Microstructure and characteristic properties of dogfish skin gelatin gels prepared by freeze/spray-drying methods

2020 ◽  
Vol 162 ◽  
pp. 1-10
Author(s):  
Ali Salem ◽  
Nahed Fakhfakh ◽  
Mourad Jridi ◽  
Ola Abdelhedi ◽  
Moncef Nasri ◽  
...  
Keyword(s):  
Spray Drying ◽  
Drying Methods ◽  
Gelatin Gels

scholarly journals Optimization of inulin production process parameters using response surface methodology

2020 ◽  
Vol 6 (1) ◽  
Author(s):  
Wasim Akram ◽  
Navneet Garud
Keyword(s):  
Response Surface ◽  
Spray Drying ◽  
Product Yield ◽  
Drying Methods ◽  
Process Variables ◽  
Drying Process ◽  
Uniform Size ◽  
Drying Temperature ◽  
Yield Value ◽  
Internal Configuration

Abstract Background Chicory is one of the major source of inulin. In our study, Box–Behnken model/response surface analysis (RSM) was used for the optimization of spray drying process variables to get the maximum inulin yield from chicory (Cichorium intybus L.). For this investigation, the investigational plan utilized three process variables drying temperature (115–125 °C), creep speed (20–24 rpm), and pressure (0.02–0.04 MPa). Result The optimal variables established by applying the Box–Behnken model were as follows: drying temperature 119.20 °C, creep speed 21.64 rpm, and pressure 0.03 MPa. The obtained powdered inulin by spray drying was investigated for the yield value, identification, size, and surface morphology of the particle. The inulin obtained from the spray drying process consists of a fine molecule-sized white powder. Instead, the drying methods shows a significant effect on the morphology and internal configuration of the powdered inulin, as the inulin obtained from spray drying was of a widespread and uniform size and shape, with a rough surface on increase in temperature and smoother surface while increasing the creep speed. The findings indicate that the spray drying with optimum parameters resulted in maximum product yield. Conclusion The outcomes of the study concluded that the product yield through spray drying technique under optimized condition is optimal as compared to other drying technique. Hence, this technique may be applied at commercial scale for the production of inulin.

scholarly journals Comparison of crystallized coconut sugar produced by traditional method and amorphous coconut sugar formed by two drying methods: vacuum drying and spray drying

2018 ◽  
Vol 21 (1) ◽  
pp. 2339-2354 ◽  
Author(s):  
Bambang Nurhadi ◽  
Nandi Sukri ◽  
Wahyu Kristian Sugandi ◽  
Annisa Puteri Widanti ◽  
Resi Restiani ◽  
...  
Keyword(s):  
Spray Drying ◽  
Traditional Method ◽  
Vacuum Drying ◽  
Drying Methods

The Preparation and Characterization of Redispersible Polymer Powder with Core-Shell Structure

2013 ◽  
Vol 687 ◽  
pp. 88-93
Author(s):  
Jian Xu ◽  
Zhong Jun Feng ◽  
Le Feng Fu ◽  
Bai Cun Zheng
Keyword(s):  
Electron Microscopy ◽  
Spray Drying ◽  
Shell Morphology ◽  
Core Shell ◽  
Drying Methods ◽  
Seeded Emulsion Polymerization ◽  
Transition Electron Microscopy ◽  
Polymer Powder ◽  
Particle Size Analyzer ◽  
Redispersible Polymer Powder

Acrylate polymer emulsion was synthesized by semi-continuous seeded emulsion polymerization with methacrylic acid (MAA) as the hydrophilic shell monomer. The redispersible polymer powder was prepared by spray drying method. The effects of the amount of MAA, styrene (St) stoichiometry equivalents to methyl methacrylate, and two kinds of spray drying methods on size distribution of the redispersible polymer powder were further systematically investigated. The Malvern laser particle size analyzer, transition electron microscopy (TEM), scanning electron microscopy (SEM) and differential scanning calorimeter were employed to characterize the redispersible polymer powder. Results showed that the redispersible polymer powder obtained by pneumatic spray drying with excellent re-dispersibility could be synthesized at 10 % of MAA, 50 % of St stoichiometry equivalents. The final copolymer emulsion with “perfect” core-shell morphology was approved by TEM, and the comparable film forming ability of the redispersible polymer powder with the original emulsion was observed by SEM, which could form a dense and smooth membrane.

scholarly journals SPRAY DRYING APPROACH IN PREPARATION AND CHARACTERIZATION OF SOLID DISPERSION OF EPROSARTAN MESYLATE

2021 ◽  
Vol 10 (3) ◽  
pp. 2929-2932
Author(s):  
Sachin N Kothawade
Keyword(s):  
Spray Drying ◽  
Solid Dispersion ◽  
Water Solubility ◽  
Solid Dispersions ◽  
Weight Ratio ◽  
Water Soluble ◽  
Drying Methods ◽  
Scanning Calorimetry ◽  
Dispersion Systems ◽  
Physicochemical Features

Spray drying methods were used to make solid dispersions of the medication Eprosartan Mesylate, which is poorly water-soluble. X-ray Powder diffraction, Fourier transform infrared spectroscopy, and differential scanning calorimetry were used to characterize the products' physicochemical features as well as drug-polymer interactions. Eprosartan Mesylate was shown to be dispersed amorphously in both solid dispersion systems, with a drug to polymer weight ratio of 1:4.The drug and polymer created hydrogen bonds, according to the spectrum data. Both techniques utilized in this investigation enhanced Eprosartan Mesylate solubility. Solid dispersions, on the other hand, performed significantly better, dissolving completely in 5 minutes and at a rate that was about 20 times faster than API within the first 15 minutes. Spray drying is a good way to boost the bioavailability of drugs that are poor water solubility.

scholarly journals Effects of Storage Conditions on Degradation of Chlorophyll and Emulsifying Capacity of Thylakoid Powders Produced by Different Drying Methods

Foods ◽  
2020 ◽  
Vol 9 (5) ◽  
pp. 669
Author(s):  
Karolina Östbring ◽  
Ingegerd Sjöholm ◽  
Marilyn Rayner ◽  
Charlotte Erlanson-Albertsson
Keyword(s):  
Relative Humidity ◽  
Spray Drying ◽  
Freeze Drying ◽  
Functional Foods ◽  
Storage Conditions ◽  
Drying Methods ◽  
Drying Method ◽  
Equivalent Effect ◽  
Emulsifying Capacity

Thylakoid membranes isolated from spinach have previously been shown to inhibit lipase/co-lipase and prolong satiety in vivo. There is a need to develop thylakoid products that not only have the desired characteristics and functionality after processing, but also are stable and provide equivalent effect on appetite over the promised shelf life. The aim of the present study was therefore to evaluate how the thylakoid powders’ characteristics and functionality were affected by moisture during storage. Thylakoids produced by drum-drying, spray-drying, and freeze-drying were incubated in controlled atmosphere with different relative humidity (10 RH%, 32 RH%, 48 RH% and 61 RH%) for 8 months. The water content in all powders was increased during storage. The water absorption was moisture-dependent, and the powders were considered hygroscopic. Relative humidity showed a definite influence on the rate of chlorophyll degradation and loss of green color in thylakoid powders after storage which correlated with impaired emulsifying capacity. Spray-dried powder had the overall highest chlorophyll content and emulsifying capacity at all RH-levels investigated. Spray drying was therefore considered the most suitable drying method yielding a powder with best-maintained functionality after storage. The results can be applied towards quality control of high-quality functional foods with appetite suppressing abilities.

Effect of drying methods (electrospraying, freeze drying and spray drying) on survival and viability of microencapsulated Lactobacillus rhamnosus ATCC 7469

2018 ◽  
Vol 40 ◽  
pp. 391-399 ◽  
Author(s):  
Mahsa Moayyedi ◽  
Mohammad Hadi Eskandari ◽  
Amir Hossein Elhami Rad ◽  
Esmaeil Ziaee ◽  
Mohammad Hossein Haddad Khodaparast ◽  
...  
Keyword(s):  
Spray Drying ◽  
Freeze Drying ◽  
Lactobacillus Rhamnosus ◽  
Drying Methods

scholarly journals Effects of Vacuum Freeze-Drying and Vacuum Spray-Drying on Biochemical Properties and Functionalities of Myofibrillar Proteins from Silver Carp

2019 ◽  
Vol 2019 ◽  
pp. 1-8
Author(s):  
Jianzhen Niu ◽  
Binfan Zhao ◽  
Xiujin Guo ◽  
Tao Yin
Keyword(s):  
Spray Drying ◽  
Freeze Drying ◽  
Silver Carp ◽  
Biochemical Properties ◽  
Molecular Structures ◽  
Drying Methods ◽  
Myofibrillar Proteins ◽  
Fish Protein ◽  
Freeze Dried ◽  
Spray Dried

Fish protein powders were produced from silver carp myofibrillar proteins using vacuum freeze-drying and vacuum spray-drying. Biochemical properties and functionalities of freeze-dried and spray-dried powders were determined. The myofibrillar proteins were partially denatured under both the drying methods which were evidenced by the increase of free sulfhydryl content, surface hydrophobicity, and intrinsic fluorescence while the decrease of the Ca2+-ATPase activity and percentage of the α-helical structure. With respect to vacuum freeze-drying, the proteins were denatured to a higher degree by vacuum spray-drying. The spray-dried fish protein powder showed a higher water retention capacity and emulsifying stability index, but the same solubility and emulsifying activity index. The micrographs indicate that vacuum freeze-dried powder formed a spongy structure, while the powder under vacuum spray-drying mostly appeared spherical in shape with hollow inside. Thus, the two drying methods can be used to manufacture fish protein powders with varied molecular structures and functionalities.

scholarly journals Optimization of Spray-Drying Process of Jerusalem artichoke Extract for Inulin Production

Molecules ◽  
2019 ◽  
Vol 24 (9) ◽  
pp. 1674
Author(s):  
Zhenzhou Zhu ◽  
Mailing Wu ◽  
Jie Cai ◽  
Shuyi Li ◽  
Krystian Marszałek ◽  
...  
Keyword(s):  
Particle Size ◽  
Water Content ◽  
Spray Drying ◽  
Freeze Drying ◽  
Heating Temperature ◽  
Great Influence ◽  
Jerusalem Artichoke ◽  
Drying Methods ◽  
Freeze Dried ◽  
Spray Dried

Jerusalem artichoke is an important natural matrix for inulin production. In this experiment, response surface methodology (RSM) was employed to optimize the spray-drying parameters in order to determine the maximal inulin yield. For this study, three independent variables (heating temperature (Tª, 110–120 °C), creep speed (V, 18–22 rpm) and pressure (P, 0.02–0.04 MPa)) were used in the experimental design. Using the Box–Behnken design, the optimal parameters obtained were: drying temperature 114.6 °C, creep speed 20.02 rpm, and pressure: 0.03 MPa. The inulin yield, water content and particle size of inulin obtained by spray-drying and freeze-drying were compared. In this regard, the spray-dried inulin consisted of a white powder having a fine particle size, and the freeze-dried inulin had a pale-yellow fluffy floc. On the other hand, the drying methods had a great influence on the appearance and internal structure of inulin powder, since the spray-dried inulin had a complete and uniform shape and size, whereas the freeze-dried inulin had a flocculated sheet structure. The analysis showed that the spray-drying led to a higher inulin yield, lower water content and better surface structure than freeze-drying.

Sign in / Sign up

Export Citation Format

Share Document