Elastic and Plastic Anisotropy in a Refractory High Entropy Alloy utilizing Combinatorial Instrumented Indentation and Electron Backscatter Diffraction

2021 ◽  
pp. 162902
Author(s):  
Abheepsit Raturi ◽  
Krishanu Biswas ◽  
N.P. Gurao
2017 ◽  
Vol 23 (5) ◽  
pp. 905-915 ◽  
Author(s):  
Leo T.H. de Jeer ◽  
Václav Ocelík ◽  
Jeff T.M. De Hosson

AbstractA detailed microstructural evaluation was executed on the crystallographic texture as well as the mechanisms for nucleation, phase transformation, and grain growth in a Al0.7CoCrFeNi high-entropy alloy. The microstructure and crystallographic orientations were characterized by electron backscatter diffraction, and the chemical composition variations by energy-dispersive X-ray spectroscopy. The cast Al0.7CoCrFeNi alloy started in the BCC phase and partially transformed into the FCC phase. It was found that the Pitsch orientation relationship (OR) dominates the nucleation mechanism of the FCC phase; however, deviations with respect to the Pitsch OR are observed and are attributed to the differently sized atoms forming an ordered B2 phase in the alloy causing lattice distortions. The dual phase BCC–FCC microstructure contains FCC Widmanstätten plates oriented parallel to the {110}BCC planes of the parent grain. It was found that the crystal orientation distribution after the BCC–FCC phase transformation is confined and is explained as a product of the governing mechanisms.


Entropy ◽  
2019 ◽  
Vol 21 (9) ◽  
pp. 880 ◽  
Author(s):  
Ali Arab ◽  
Yansong Guo ◽  
Qiang Zhou ◽  
Pengwan Chen

High entropy alloys (HEAs) are usually fabricated using arc melting which has the disadvantages of diseconomy, and the limitations in the shape and size of final products. However, recently, quite a large amount of research has been carried out to find the fabrication techniques for HEAs with better properties such as mechanical alloying and rapid solidification. In this paper, an AlCoCrFeNi high entropy alloy was successfully fabricated by the shock consolidation technique. In this method, the starting powders were mixed by mechanical alloying and then the shock wave was imposed to the compacted powders by explosion. High levels of residual stress existed in samples fabricated by the shock consolidation method. Due to this, after fabrication of the sample, heat treatment was used to eliminate the residual stress and improve the mechanical properties. The microstructure of the samples before and after heat treatment were examined by XRD, SEM and electron backscatter diffraction (EBSD). The shock consolidated sample and sample with heat treatment both showed the nano-structure. After heat treatment the hardness of the sample was decreased from 715 HV to the 624 HV, however the failure strength increased, and as expected the ductility of the sample was improved after heat treatment.


Author(s):  
Frank Altmann ◽  
Jens Beyersdorfer ◽  
Jan Schischka ◽  
Michael Krause ◽  
German Franz ◽  
...  

Abstract In this paper the new Vion™ Plasma-FIB system, developed by FEI, is evaluated for cross sectioning of Cu filled Through Silicon Via (TSV) interconnects. The aim of the study presented in this paper is to evaluate and optimise different Plasma-FIB (P-FIB) milling strategies in terms of performance and cross section surface quality. The sufficient preservation of microstructures within cross sections is crucial for subsequent Electron Backscatter Diffraction (EBSD) grain structure analyses and a high resolution interface characterisation by TEM.


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