scholarly journals Discrimination of defective dry-cured Iberian ham determining volatile compounds by non-destructive sampling and gas chromatography

LWT ◽  
2021 ◽  
pp. 112785
Author(s):  
Andrés Martín-Gómez ◽  
M. Pilar Segura-Borrego ◽  
Rocío Ríos-Reina ◽  
M. José Cardador ◽  
Raquel M. Callejón ◽  
...  
2011 ◽  
Author(s):  
M Ormsby ◽  
T Barrett ◽  
J. B. Lang ◽  
J. Mazurek ◽  
M. Schilling

<p>Gelatin sizing was a key ingredient during the handpapermaking era. The gelatin concentration in historical papers has never been well documented, however, because measuring the gelatin content required destructive sampling. In this project we developed a non-destructive method using near infrared (NIR) spectroscopy. Gelatin concentrations of 40 historical papers from the 15<sup>th</sup>-18<sup>th</sup> centuries were determined from amino acid (AA) concentrations by using gas chromatography/mass spectroscopy. These values were combined with NIR spectra from the same papers to generate a model for predicting concentrations of unknowns. If a NIR measurement predicted a gelatin concentration in the range 0-6 percent then there is a 95% probability that the difference between the NIR model value and a destructive AA measurement would be between -1.6 and +1.3 percentage points. For 6-8 percent there is a 95% probability the difference would be between -2.0 and +1.5 percentage points, and for 8-12 percent the difference is between -3.0 and +2.0 percentage points. In a study of 159 specimens from books, loose leaves, and artworks printed from 1460-1791, the means for all papers were quite high in the 15<sup>th</sup> century and dropped an average of 20% every 50 years. Possible explanations for the decline are offered.</p>


Author(s):  
Rini Rini ◽  
Daimon Syukri ◽  
Fauzan Azima

Rendang is a traditional-specific food in Indonesia. Rendang is generally made with beef, coconut milk, and spices. There are two types of rendang according to its time processing. Rendang “kalio” is a final product of rendang that needs a short heating period while dried rendang is produced by the longer heating period. In the present study, the profile of the volatile compounds that most obtained from spices was analyzed by gas chromatography-mass spectrometry (GC-MS) to characterize the influence of the cooking period on the flavor characteristic of two available types of rendang. There were dozens of volatile compounds identified including carboxylic, aromatic, carbonyl, and alcohols where carboxylic and aromatics were the predominant volatile fractions. The results indicated that the cooking period affected the profile of volatile compounds between "kalio" rendang and dried rendang. Carboxylic and aromatics were less in the dried rendang compared to the rendang “kalio” where others were opposites. The increase of carbonyls and alcohol during the cooking process has suggested can play a crucial role in the flavor of dried rendang.


Foods ◽  
2021 ◽  
Vol 10 (6) ◽  
pp. 1180
Author(s):  
Xiaoyu Yin ◽  
Qian Chen ◽  
Qian Liu ◽  
Yan Wang ◽  
Baohua Kong

Smoking is mainly used to impart desirable flavour, colour and texture to the products. Various food smoking methods can be divided into traditional and industrial methods. The influences of three different smoking methods, including traditional smouldering smoke (TSS), industrial smouldering smoke (ISS) and industrial liquid smoke (ILS), on quality characteristics, sensory attributes and flavour profiles of Harbin red sausages were studied. The smoking methods had significant effects on the moisture content (55.74–61.72 g/100 g), L*-value (53.85–57.61), a*-value (11.97–13.15), b*-value (12.19–12.92), hardness (24.25–29.17 N) and chewiness (13.42–17.32). A total of 86 volatile compounds were identified by headspace solid phase microextraction combined with comprehensive two-dimensional gas chromatography mass spectrometry (GC × GC-qMS). Among them, phenolic compounds were the most abundant compounds in the all sausages. Compared with sausages smoked with smouldering smoke, the ILS sausages showed the highest content of volatile compounds, especially phenols, alcohols, aldehydes and ketones. Principal component analysis showed that the sausages smoked with different methods had a good separation based on the quality characteristics and GC × GC-qMS data. These results will facilitate optimising the smoking methods in the industrial production of smoked meat products.


2016 ◽  
Vol 97 (7) ◽  
pp. 1479-1482 ◽  
Author(s):  
Thomas J. Ashton ◽  
Meriem Kayoueche-Reeve ◽  
Andrew J. Blight ◽  
Jon Moore ◽  
David M. Paterson

Accurate discrimination of two morphologically similar species of Patella limpets has been facilitated by using qPCR amplification of species-specific mitochondrial genomic regions. Cost-effective and non-destructive sampling is achieved using a mucus swab and simple sample lysis and dilution to create a PCR template. Results show 100% concurrence with dissection and microscopic analysis, and the technique has been employed successfully in field studies. The use of highly sensitive DNA barcoding techniques such as this hold great potential for improving previously challenging field assessments of species abundance.


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