TIG cladding in-situ nano vanadium carbide reinforced Fe-based ultra-fine grain layers under water cooling condition

2018 ◽  
Vol 352 ◽  
pp. 222-230 ◽  
Author(s):  
Hui Zhang ◽  
Kai Chong ◽  
Guangchun Xiao ◽  
Zhiping Sun ◽  
Wei Zhao
Author(s):  
Dudley M. Sherman ◽  
Thos. E. Hutchinson

The in situ electron microscope technique has been shown to be a powerful method for investigating the nucleation and growth of thin films formed by vacuum vapor deposition. The nucleation and early stages of growth of metal deposits formed by ion beam sputter-deposition are now being studied by the in situ technique.A duoplasmatron ion source and lens assembly has been attached to one side of the universal chamber of an RCA EMU-4 microscope and a sputtering target inserted into the chamber from the opposite side. The material to be deposited, in disc form, is bonded to the end of an electrically isolated copper rod that has provisions for target water cooling. The ion beam is normal to the microscope electron beam and the target is placed adjacent to the electron beam above the specimen hot stage, as shown in Figure 1.


2014 ◽  
Vol 602-603 ◽  
pp. 438-442
Author(s):  
Lei Yu ◽  
Jian Yang ◽  
Tai Qiu

Fully dense (ZrB2+ZrC)/Zr3[Al (Si)]4C6 composites with ZrB2 content varying from 0 to 15 vol.% and fixed ZrC content of 10 vol.% were successfully prepared by in situ hot-pressing in Ar atmosphere using ZrH2, Al, Si, C and B4C as raw materials. With the increase of ZrB2 content, both the bending strength and fracture toughness of the composites increase and then decrease. The synergistic action of ZrB2 and ZrC as reinforcements shows significant strengthening and toughing effect to the Zr3[Al (Si)]4C6 matrix. The composite with 10 vol.% ZrB2 shows the optimal mechanical properties: 516 MPa for bending strength and 6.52 MPa·m1/2 for fracture toughness. With the increase of ZrB2 content, the Vickers hardness of the composites shows a near-linear increase from 15.3 GPa to 16.7 GPa. The strengthening and toughening effect can be ascribed to the unique mechanical properties of ZrB2 and ZrC reinforcements, the differences in coefficient of thermal expansion and modulus between them and Zr3[Al (Si)]4C6 matrix, fine grain strengthening and uniform microstructure derived by the in situ synthesis reaction.


2021 ◽  
Vol 47 (1) ◽  
pp. 953-964
Author(s):  
Liujie Xu ◽  
Fangfang Wang ◽  
Yucheng Zhou ◽  
Xi Wang ◽  
Chong Chen ◽  
...  

Materials ◽  
2020 ◽  
Vol 13 (23) ◽  
pp. 5319
Author(s):  
Haofei Zhu ◽  
Jun Liu ◽  
Yi Wu ◽  
Qing Zhang ◽  
Qiwei Shi ◽  
...  

Isothermal compression tests of in-situ TiB2/7050Al composites fabricated by powder metallurgy were performed at 300–460 °C with the strain rate varying from 0.001 s−1 to 1 s−1. The Arrhenius constitutive equation and hot processing map of composites were established, presenting excellent hot workability with low activation energies and broad processing windows. Dramatic discontinuous/continuous dynamic recrystallization (DDRX/CDRX) and grain boundary sliding (GBS) take place in composites during deformation, depending on the Zener-Hollomon parameter (Z) values. It is found that initially uniform TiB2 particles and fine grain structures are beneficial to the DDRX, which is the major softening mechanism in composites at high Z values. With the Z value decreasing, dynamic recovery and CDRX around particles are enhanced, preventing the occurrence of DDRX. In addition, fine grain structures in composites are stable at elevated temperature thanks to the pinning of dense nanoparticles, which triggers the occurrence of GBS and ensures good workability at low Z values.


2012 ◽  
Vol 430-432 ◽  
pp. 517-520
Author(s):  
Nan Lv ◽  
Sheng Li Li ◽  
Yong Long Jin ◽  
Xin Gang Ai ◽  
Dong Wei Zhang

The production of huge rectangular ingots becomes crying needs in the condition of lots of heavy plate mills more than 5m have been in operation. In this paper, we simulate the solidification of 60t Q235 huge rectangular ingot with ProCAST in different cooling conditions such as air cooling, forced air cooling and water cooling. The results show that solidification time in forced air cooling and water cooling shortened than that in air cooling respectively by 0.9 hours and 2.2 hours; The primary fine-grain area is large in the forced air cooling and water cooling. In forced air cooling , we can obtain the largest equiaxial crystal ratio and the minimum columnar crystal ratio; The shrinkage cavity position of the ingot in forced air cooling and water cooling is closer to riser than it is in air cooling, but the volumes of shrinkage cavities respectively increased to a greater extent than in air cooling.


2017 ◽  
Vol 737 ◽  
pp. 11-15 ◽  
Author(s):  
R.E. Ibrahim ◽  
Ramli Rosmamuhamadani ◽  
Mahesh Talari ◽  
Sabrina M. Yahaya ◽  
Sreenivasan Sulaiman ◽  
...  

Aluminum-silicon (Al-Si) alloys are an important class of materials, alloys which have great interested in wide industries whether in light or heavy industries, due to their superior properties like high strength to weight ratio, corrosion resistance, and excellent castability. The mechanical strength and the effect of modifying alloys have been studied. To evaluate the strength and revealed the structural of these alloys, the Instron tensile and Shimidzu Vickers hardness tester have been employed while the fracture surfaces have been observed by Scanning electron microscope (SEM). From results obtained, the microstructure of Al-Si with TiB2 has much finer microstructure compared to unfine Al-Si alloy. It showed that the eutectic silicon microstructure in Al-Si alloy changed from needles-look or acicular to fine grain size or globular when the added of TiB2. The mechanical studies showed that the ductility of Al-Si alloy was much lower in the absence of grain refiner, TiB2. The tensile strength of unrefined Al-Si and Al-Si with 6 wt.%TiB2 as grain refinement were recorded 275 and 312 MPa respectively. The hardness value for the unrefined Al-Si alloy also shows less compared with Al-Si with grain refiner, 6 wt.%TiB2, which are 74 and 78 MPa. This showed the results were significant improvements in mechanical properties have been obtained with the use of TiB2 as grain refiner to Al-Si alloy.


1992 ◽  
Vol 7 (12) ◽  
pp. 3175-3184 ◽  
Author(s):  
Yuan-Liang Wang ◽  
Z.Q. Tan ◽  
Yimei Zhu ◽  
A.R. Moodenbaugh ◽  
M. Suenaga

A modified aerosol decomposition method was developed for producing sintered YBa2Cu3O7−δ (1-2-3) pellets having sharp superconducting transition Tc's at ∼90 K, fine grain sizes, and clean grain boundaries. This method used “precursor” powders, which were produced with an aerosol flow reactor at 550 °C, instead of in situ produced 1-2-3 powders commonly processed at 880–1000 °C. As determined by x-ray absorption and powder diffraction studies, the 1-2-3 powders produced by the modified route contain less cation disorders than the in situ produced powders. The disorder is speculated to be the cause of Tc-suppression and broadening. It cannot be removed unless high sintering temperatures were used (>950 °C), which resulted in large grains and impurities and cracks at grain boundaries.


2015 ◽  
Vol 19 (sup10) ◽  
pp. S10-44-S10-48
Author(s):  
S. Q. Zhang ◽  
T. J. Chen ◽  
P. B. Li ◽  
L. L. Li

2013 ◽  
Vol 718-720 ◽  
pp. 20-24
Author(s):  
J. Yang ◽  
X.Q. Jiao ◽  
R. Zhang ◽  
H. Zhong ◽  
Y. Shi ◽  
...  

In this work, the aluminum nitride (AlN) thin film with highly c-axis orientation was prepared successfully at water cooling condition by RF sputtering. The influence of water cooling on the crystalline quality of AlN thin film is researched. The crystalline characteristics and microstructure of AlN thin films deposited on Si (111) and Mo/Si (111) were researched by X-ray diffraction (XRD) and field emission scanning electron microscope (FESEM). The results indicated that highly c-axis AlN films can be synthetized at water cooling condition. The AlN film deposited on Mo thin film is titled to the surface, when that is perpendicular to the silicon substrate. Different models are proposed to explain the growth behaviors of AlN thin films on the two kinds of substrates.


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