Microstructural stability of TMS-238TM Ni-base superalloy during long-term exposure at high temperature

Author(s):  
Roman Sowa ◽  
Thomas Goehler ◽  
Lisa Dankl ◽  
Anna Kirzinger ◽  
Andrzej Budziak ◽  
...  
Author(s):  
R. E. Franck ◽  
J. A. Hawk ◽  
G. J. Shiflet

Rapid solidification processing (RSP) is one method of producing high strength aluminum alloys for elevated temperature applications. Allied-Signal, Inc. has produced an Al-12.4 Fe-1.2 V-2.3 Si (composition in wt pct) alloy which possesses good microstructural stability up to 425°C. This alloy contains a high volume fraction (37 v/o) of fine nearly spherical, α-Al12(Fe, V)3Si dispersoids. The improved elevated temperature strength and stability of this alloy is due to the slower dispersoid coarsening rate of the silicide particles. Additionally, the high v/o of second phase particles should inhibit recrystallization and grain growth, and thus reduce any loss in strength due to long term, high temperature annealing.The focus of this research is to investigate microstructural changes induced by long term, high temperature static annealing heat-treatments. Annealing treatments for up to 1000 hours were carried out on this alloy at 500°C, 550°C and 600°C. Particle coarsening and/or recrystallization and grain growth would be accelerated in these temperature regimes.


2015 ◽  
Vol 658 ◽  
pp. 14-18
Author(s):  
Tanaporn Rojhirunsakool ◽  
Duangkwan Thongpian ◽  
Nutthita Chuankrerkkul ◽  
Panyawat Wangyao

Nickel-base superalloys have been used as high temperature materials in land-base gas turbine application. When subjected to long term, high temperature service, large crack propagation was observed. Typical refurbishment method of these turbines is carried out by using TIG welding followed by post-weld standard heat treatment. However, new crack initiation is found in the heat-affected zone after TIG welding. Pre-weld heat treatment has been discovered to improves final γ + γ’ microstructure. This study focuses on the effect of pre-weld heat treatment temperature on final γ + γ’ microstructure. Seven different conditions of pre-weld heat treatment temperature were investigated. Scanning electron microscopy studies were carried out after pre-weld and post-weld heat treatments to compare the γ + γ’ microstructure and capture microcracks. The best pre-weld heat treatment temperature produces uniform distribution of finely dispersed γ’ precipitates in the γ matrix without post-weld crack.


2015 ◽  
Vol 816 ◽  
pp. 523-528 ◽  
Author(s):  
Zhi Hong Zhong ◽  
Yue Feng Gu ◽  
Yong Yuan ◽  
Zhan Shi ◽  
Yu Cheng Wu

A low-cost, high-creep strength wrought Fe‒Ni-base superalloy for 700 °C advanced ultra-supercritical coal-fired power plant applications has been developed. The microstructural stability of this alloy during long-term exposures at 700 °C‒750 °C for up to 10000 h was investigated by SEM and TEM. The correlation between the microstructure evolution and the mechanical properties was studied. The experimental results showed that the major precipitates in the alloy were spherical γ′, MC and discrete M23C6 after the long-term exposure at 700 °C and 750 °C and no harmful phases, such as σ phase and η phase, were observed. The amount of M23C6 increased with exposure time at 700 °C while it decreased at 750 °C. During thermal exposure γ′ coarsened with increasing the exposure time and exposure temperature. Alloy showed good oxidation resistance due to the formation of external layer of Cr2O3. The yield strength of the alloy increased at first and then decreased with increasing exposure time at 700 °C, but it decreased gradually with increasing exposure time at 750 °C. The relationship between yield strength and the dominant deformation mechanisms of the alloy was discussed.


Author(s):  
M. Larsen ◽  
R.G. Rowe ◽  
D.W. Skelly

Microlaminate composites consisting of alternating layers of a high temperature intermetallic compound for elevated temperature strength and a ductile refractory metal for toughening may have uses in aircraft engine turbines. Microstructural stability at elevated temperatures is a crucial requirement for these composites. A microlaminate composite consisting of alternating layers of Cr2Nb and Nb(Cr) was produced by vapor phase deposition. The stability of the layers at elevated temperatures was investigated by cross-sectional TEM.The as-deposited composite consists of layers of a Nb(Cr) solid solution with a composition in atomic percent of 91% Nb and 9% Cr. It has a bcc structure with highly elongated grains. Alternating with this Nb(Cr) layer is the Cr2Nb layer. However, this layer has deposited as a fine grain Cr(Nb) solid solution with a metastable bcc structure and a lattice parameter about half way between that of pure Nb and pure Cr. The atomic composition of this layer is 60% Cr and 40% Nb. The interface between the layers in the as-deposited condition appears very flat (figure 1). After a two hour, 1200 °C heat treatment, the metastable Cr(Nb) layer transforms to the Cr2Nb phase with the C15 cubic structure. Grain coarsening occurs in the Nb(Cr) layer and the interface between the layers roughen. The roughening of the interface is a prelude to an instability of the interface at higher heat treatment temperatures with perturbations of the Cr2Nb grains penetrating into the Nb(Cr) layer.


Alloy Digest ◽  
2010 ◽  
Vol 59 (1) ◽  

Abstract Kubota KNC-03 is a grade with a combination of high strength and excellent resistance to oxidation. These properties make this alloy suitable for long-term service at temperature up to 1250 deg C (2282 deg F). This datasheet provides information on physical properties, hardness, elasticity, tensile properties, and compressive strength as well as creep. It also includes information on high temperature performance as well as casting and joining. Filing Code: Ni-676. Producer or source: Kubota Metal Corporation, Fahramet Division. See also Alloy Digest Ni-662, April 2008.


Alloy Digest ◽  
2020 ◽  
Vol 69 (8) ◽  

Abstract ATI 6-2-4-2 is a near-alpha, high strength, titanium alloy that exhibits a good combination of tensile strength, creep strength, toughness, and long-term stability at temperatures up to 425 °C (800 °F). Silicon up to 0.1% frequently is added to improve the creep resistance of the alloy. This datasheet provides information on composition, physical properties, hardness, and tensile properties as well as creep. It also includes information on high temperature performance as well as forming, heat treating, machining, and joining. Filing Code: Ti-169. Producer or Source: ATI.


Proceedings ◽  
2021 ◽  
Vol 56 (1) ◽  
pp. 41
Author(s):  
Lida Khajavizadeh ◽  
Anita Lloyd Spetz ◽  
Mike Andersson

In order to investigate the necessary device improvements for high-temperature CO sensing with SiC metal insulator semiconductor field effect transistor (MISFET)-based chemical gas sensors, devices employing, as the gas-sensitive gate contact, a film of co-deposited Pt/Al2O3 instead of the commonly used catalytic metal-based contacts were fabricated and characterized for CO detection at elevated temperatures and different CO and O2 levels. It can be concluded that the sensing mechanism at elevated temperatures correlates with oxygen removal from the sensor surface rather than the surface CO coverage as observed at lower temperatures. The long-term stability performance was also shown to be improved compared to that of previously studied devices.


2018 ◽  
Vol 924 ◽  
pp. 854-857
Author(s):  
Ming Hung Weng ◽  
Muhammad I. Idris ◽  
S. Wright ◽  
David T. Clark ◽  
R.A.R. Young ◽  
...  

A high-temperature silicon carbide power module using CMOS gate drive technology and discrete power devices is presented. The power module was aged at 200V and 300 °C for 3,000 hours in a long-term reliability test. After the initial increase, the variation in the rise time of the module is 27% (49.63ns@1,000h compared to 63.1ns@3,000h), whilst the fall time increases by 54.3% (62.92ns@1,000h compared to 97.1ns@3,000h). The unique assembly enables the integrated circuits of CMOS logic with passive circuit elements capable of operation at temperatures of 300°C and beyond.


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