scholarly journals The influence of normal stress and sliding velocity on the frictional behaviour of calcite at room temperature: insights from laboratory experiments and microstructural observations

2016 ◽  
Vol 205 (1) ◽  
pp. 548-561 ◽  
Author(s):  
B.M. Carpenter ◽  
C. Collettini ◽  
C. Viti ◽  
A. Cavallo

Abstract The presence of calcite in and near faults, as the dominant material, cement, or vein fill, indicates that the mechanical behaviour of carbonate-dominated material likely plays an important role in shallow- and mid-crustal faulting. To better understand the behaviour of calcite, under loading conditions relevant to earthquake nucleation, we sheared powdered gouge of Carrara Marble, >98 per cent CaCO3, at constant normal stresses between 1 and 100 MPa under water-saturated conditions at room temperature. We performed slide-hold-slide tests, 1–3000 s, to measure the amount of static frictional strengthening and creep relaxation, and velocity-stepping tests, 0.1–1000 μm s–1, to evaluate frictional stability. We observe that the rates of frictional strengthening and creep relaxation decrease with increasing normal stress and diverge as shear velocity is increased from 1 to 3000 μm s–1 during slide-hold-slide experiments. We also observe complex frictional stability behaviour that depends on both normal stress and shearing velocity. At normal stresses less than 20 MPa, we observe predominantly velocity-neutral friction behaviour. Above 20 MPa, we observe strong velocity-strengthening frictional behaviour at low velocities, which then evolves towards velocity-weakening friction behaviour at high velocities. Microstructural analyses of recovered samples highlight a variety of deformation mechanisms including grain size reduction and localization, folding of calcite grains and fluid-assisted diffusion mass transfer processes promoting the development of calcite nanograins in the highly deformed portions of the experimental fault. Our combined analyses indicate that calcite fault gouge transitions from brittle to semi-brittle behaviour at high normal stress and slow sliding velocities. This transition has important implications for earthquake nucleation and propagation on faults in carbonate-dominated lithologies.

2006 ◽  
Vol 326-328 ◽  
pp. 1709-1712 ◽  
Author(s):  
Hai Bo Li ◽  
Hai Peng Feng ◽  
Bo Liu ◽  
Jun Ru Li

In order to study the strength and deformation properties of rock joint under different shear velocities, normal stresses and undulation angles, series testes are conducted by a RMT-150C testing machines with artificial concrete rock joint samples in the present paper. Base on the experimental results, it can be found that the peak shear strengths decrease with the increment of shear velocity, and the decreasing rates tend to decrease with the increasing shear velocity. The shear strength of rock joints increase with the increasing undulation angles, and linearly increase with the increment of normal stress. It is also indicated that the shear stiffness increase with the increasing normal stress, undulation angle as well as the shear velocity with a decreasing tendency.


2020 ◽  
Author(s):  
Hanaya Okuda ◽  
Ikuo Katayama ◽  
Hiroshi Sakuma ◽  
Kenji Kawai

Abstract. We report the results of friction experiments on brucite under both dry and water-saturated (wet) conditions under various normal stresses (10–60 MPa). The steady-state friction coefficients of brucite were determined to be 0.40 and 0.26 for the dry and wet cases, respectively, independent of the normal stress. Under dry conditions, velocity-weakening behavior was observed in all experiments at various normal stresses. Under wet conditions, velocity weakening was observed at low normal stress (10 and 20 MPa), whereas velocity strengthening was determined at a higher applied normal stress. The microstructural observations on recovered experimental samples indicate localized deformation within the narrow shear band, implying that a small volume of brucite can control the bulk strength in an ultramafic setting and significantly change the frictional properties. Brucite is found to be the only mineral that has a low friction coefficient and exhibits unstable frictional behavior under hydrated mantle wedge conditions, explaining the occurrence of slow earthquakes in the mantle wedge.


2002 ◽  
Vol 124 (3) ◽  
pp. 146-153 ◽  
Author(s):  
John R. Smith ◽  
Jeffrey B. Lund ◽  
Robert K. Galloway

The impact of frictional forces on the overall forces when drilling with a PDC bit has previously been implied by models and by single cutter and bit tests. This report describes new experiments to measure friction between three different bit surface materials and two different rocks over a wide range of normal stresses in up to four different fluids. Polished PDC cutters are shown to have lower frictional forces on the face of the cutter than standard cutters in both water and mineral oil. The measured friction coefficients were generally higher than reported in previous studies.


2012 ◽  
Vol 576 ◽  
pp. 559-562 ◽  
Author(s):  
W.Y.H. Liew ◽  
Sebastian Dayou ◽  
M. Azlan Bin Ismail ◽  
Nancy J. Siambun ◽  
Jedol Dayou

This paper examines the friction behaviour of AlCrN and TiN PVD coatings in atmospheric air and vacuum using a ball-on-disc and a reciprocating tribotesters. Comparative study on the coating sliding in air and in high vacuum environment provides important insight on the effect of oxidation on the friction behaviour of the coatings. Other important factors such as load, sliding velocity, temperature effects on the frictional behaviour of these coatings were also investigated. In the ball-on-disc tests carried out in vacuum, (i) TiN gave lower coefficient of friction (COF) than AlCrN, indicating that TiN was more lubricous, (ii) higher speed resulted in lower COF, and (iii) the COF of both coatings were lower than that produced in air. In ambient air, (i) AlCrN gave lower COF than TiN with high wear debris retention on the sliding interface due to the effect of oxidation, and (ii) higher speed resulted in lower COF, similar to that observed in vacuum. In the reciprocating tests, at low load, increasing the temperature from room temperature to 150 °C resulted in a reduction in the COF. However, at high load, the temperature virtually did not affect the COF. Higher nominal load resulted in lower COF while higher speed resulted in higher COF.


Author(s):  
Henki Ødegaard ◽  
Bjørn Nilsen

AbstractTo avoid hydraulic failure of unlined pressure tunnels, knowledge of minimum principal stress is needed. Such knowledge is only obtainable from in situ measurements, which are often time-consuming and relatively costly, effectively limiting the number of measurements typically performed. In an effort to enable more stress measurements, the authors propose a simplified and cost-effective stress measuring method; the Rapid Step-Rate Test (RSRT), which is based on existing hydraulic testing methods. To investigate the ability of this test to measure fracture normal stresses in field-like conditions, a true triaxial laboratory test rig has been developed. Hydraulic jacking experiments performed on four granite specimens, each containing a fracture, have been performed. Interpretation of pressure-, flow- and acoustic emission (AE) data has been used to interpret fracture behaviour and to assess fracture normal stresses. Our experimental data suggest that the proposed test method, to a satisfactory degree of reliability, can measure the magnitude of fracture normal stress. In addition, a clear correlation has been found between fracture closure and sudden increase in AE rate, suggesting that AE monitoring during testing can serve as a useful addition to the test. The rapid step-rate test is also considered relevant for field-scale measurements, with only minor adaptions. Our findings suggest that the RSRT can represent a way to get closer to the ideal of performing more testing along the entire length of pressure tunnel, and not only at key locations, which requires interpolation of stress data with varying degree of validity.


Geofluids ◽  
2017 ◽  
Vol 2017 ◽  
pp. 1-13 ◽  
Author(s):  
Fengshou Zhang ◽  
Yi Fang ◽  
Derek Elsworth ◽  
Chaoyi Wang ◽  
Xiaofeng Yang

We explore the evolution of friction and permeability of a propped fracture under shear. We examine the effects of normal stress, proppant thickness, proppant size, and fracture wall texture on the frictional and transport response of proppant packs confined between planar fracture surfaces. The proppant-absent and proppant-filled fractures show different frictional strength. For fractures with proppants, the frictional response is mainly controlled by the normal stress and proppant thickness. The depth of shearing-concurrent striations on fracture surfaces suggests that the magnitude of proppant embedment is controlled by the applied normal stress. Under high normal stress, the reduced friction implies that shear slip is more likely to occur on propped fractures in deeper reservoirs. The increase in the number of proppant layers, from monolayer to triple layers, significantly increases the friction of the propped fracture due to the interlocking of the particles and jamming. Permeability of the propped fracture is mainly controlled by the magnitude of the normal stress, the proppant thickness, and the proppant grain size. Permeability of the propped fracture decreases during shearing due to proppant particle crushing and related clogging. Proppants are prone to crushing if the shear loading evolves concurrently with the normal loading.


2010 ◽  
Vol 47 (10) ◽  
pp. 1112-1126 ◽  
Author(s):  
Md. Akhtar Hossain ◽  
Jian-Hua Yin

Shear strength and dilative characteristics of a re-compacted completely decomposed granite (CDG) soil are studied by performing a series of single-stage consolidated drained direct shear tests under different matric suctions and net normal stresses. The axis-translation technique is applied to control the pore-water and pore-air pressures. A soil-water retention curve (SWRC) is obtained for the CDG soil from the equilibrium water content corresponding to each applied matric suction value for zero net normal stress using a modified direct shear apparatus. Shear strength increases with matric suction and net normal stress, and the failure envelope is observed to be linear. The apparent angle of internal friction and cohesion intercept increase with matric suction. A greater dilation angle is found at higher suctions with lower net normal stresses, while lower or zero dilation angles are observed under higher net normal stresses with lower suctions, also at a saturated condition. Experimental shear strength data are compared with the analytical shear strength results obtained from a previously modified model considering the SWRC, effective shear strength parameters, and analytical dilation angles. The experimental shear strength data are slightly higher than the analytical results under higher net normal stresses in a higher suction range.


2018 ◽  
Vol 12 (10) ◽  
pp. 3333-3353 ◽  
Author(s):  
Philipp Mamot ◽  
Samuel Weber ◽  
Tanja Schröder ◽  
Michael Krautblatter

Abstract. Instability and failure of high mountain rock slopes have significantly increased since the 1990s coincident with climatic warming and are expected to rise further. Most of the observed failures in permafrost-affected rock walls are likely triggered by the mechanical destabilisation of warming bedrock permafrost including ice-filled joints. The failure of ice-filled rock joints has only been observed in a small number of experiments, often using concrete as a rock analogue. Here, we present a systematic study of the brittle shear failure of ice and rock–ice interfaces, simulating the accelerating phase of rock slope failure. For this, we performed 141 shearing experiments with rock–ice–rock “sandwich”' samples at constant strain rates (10−3 s−1) provoking ice fracturing, under normal stress conditions ranging from 100 to 800 kPa, representing 4–30 m of rock overburden, and at temperatures from −10 to −0.5 ∘C, typical for recent observed rock slope failures in alpine permafrost. To create close to natural but reproducible conditions, limestone sample surfaces were ground to international rock mechanical standard roughness. Acoustic emission (AE) was successfully applied to describe the fracturing behaviour, anticipating rock–ice failure as all failures are predated by an AE hit increase with peaks immediately prior to failure. We demonstrate that both the warming and unloading (i.e. reduced overburden) of ice-filled rock joints lead to a significant drop in shear resistance. With a temperature increase from −10 to −0.5 ∘C, the shear stress at failure reduces by 64 %–78 % for normal stresses of 100–400 kPa. At a given temperature, the shear resistance of rock–ice interfaces decreases with decreasing normal stress. This can lead to a self-enforced rock slope failure propagation: as soon as a first slab has detached, further slabs become unstable through progressive thermal propagation and possibly even faster by unloading. Here, we introduce a new Mohr–Coulomb failure criterion for ice-filled rock joints that is valid for joint surfaces, which we assume similar for all rock types, and which applies to temperatures from −8 to −0.5 ∘C and normal stresses from 100 to 400 kPa. It contains temperature-dependent friction and cohesion, which decrease by 12 % ∘C−1 and 10 % ∘C−1 respectively due to warming and it applies to temperature and stress conditions of more than 90 % of the recently documented accelerating failure phases in permafrost rock walls.


Author(s):  
Eduardo Bonet-Martínez ◽  
Pedro García-Cobo ◽  
Luis Pérez-Villarejo ◽  
Eulogio Castro ◽  
Dolores Eliche-Quesada

In this research, the feasibility of using bottom ashes generated by the combustion of biomass (olive pruning and pine pruning) as a source of aluminosilicates (OPBA) has been studied, replacing the metakaolin precursor (MK) in different proportions (0, 25, 50, 75 and 100 wt. % substitution) for the synthesis of geopolymers. As alkaline activator an 8 M NaOH solution and a Na2SiO3 have been used. The geopolymers were cured 24 hours in a climatic chamber at 60 ° C in a water-saturated atmosphere, subsequently demoulded and cured at room temperature for 28 days. The results indicated that the incorporation of OPBA waste, which have 19.7 wt. % of Ca, modifies the characteristics of the products formed after alkaline activation. In general terms, the incorporation of increasing amounts of calcium-rich ashes results in geopolymers with higher bulk density. The compressive strength increases with the addition of up to 50 wt. % of OPBA with respect to the control geopolymers, contributing the composition of the residue to the acquisition of a better behaviour mechanical. The results indicate the potential use of these OPBA waste as raw material to produce unconventional cements with 28-day curing strengths greater than 10 MPa, and thermal conductivities less than 0.35 W/mK.


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