scholarly journals Digital image correlation-based point-wise inverse characterization of heterogeneous material properties of gallbladder in vitro

Author(s):  
Katia Genovese ◽  
Luciana Casaletto ◽  
Jay D. Humphrey ◽  
Jia Lu

Continuing advances in mechanobiology reveal more and more that many cell types, especially those responsible for establishing, maintaining, remodelling or repairing extracellular matrix, are extremely sensitive to their local mechanical environment. Indeed, it appears that they fashion the extracellular matrix so as to promote a ‘mechanical homeostasis’. A natural corollary, therefore, is that cells will try to offset complexities in geometry and applied loads with heterogeneous material properties in order to render their local environment mechanobiologically favourable. There is a pressing need, therefore, for hybrid experimental–computational methods in biomechanics that can quantify such heterogeneities. In this paper, we present an approach that combines experimental information on full-field surface geometry and deformations with a membrane-based point-wise inverse method to infer full-field mechanical properties for soft tissues that exhibit nonlinear behaviours under finite deformations. To illustrate the potential utility of this new approach, we present the first quantification of regional mechanical properties of an excised but intact gallbladder, a thin-walled, sac-like organ that plays a fundamental role in normal digestion. The gallbladder was inflated to a maximum local stretch of 120% in eight pressure increments; at each pressure pause, the entire three-dimensional surface was optically extracted, and from which the surface strains were computed. Wall stresses in each state were predicted from the deformed geometry and the applied pressure using an inverse elastostatic method. The elastic properties of the gallbladder tissue were then characterized locally using point-wise stress–strain data. The gallbladder was found to be highly heterogeneous, with drastically different stiffness between the hepatic and the serosal sides. The identified material model was validated through forward finite-element analysis; both the configurations and the local stress–strain patterns were well reproduced.

2021 ◽  
Author(s):  
Luigi Bruno ◽  
Santo Canto ◽  
Luciano Luciani

Abstract In the present work, authors have demonstrated how a localized induction heat treatment can be advantageously applied, controlled and mechanically characterized on a specific part – i.e. on steel hose fittings for hydraulic applications. More specifically, the study shows how this specific type of heat treatment facilitates the acquisition of significant localization effects on mechanical properties, and how such a treatment could act as a powerful tool for material optimization in diverse applications. The instrumented micro-indentation test was adopted as the investigation method for mechanical characterization and, due to the reduced amount of material required for the test, has the double advantage of retrieving potential spatial gradients of the mechanical properties without causing permanent damage to the entirety of analyzed parts. The measurement of both the Vickers hardness and plastic work required to make the indentation that would be necessary to quantify the strength and ductility capability of the parts’ material. In addition, a customized tensile test, based on the strains measurement obtained through an optical full-field method – i.e. Digital Image Correlation (DIC) – was developed with the aim of identifying and quantifying the correlation between the material properties attainable through a conventional tensile test and those measured by the instrumented micro-indentation test. Finally, it was demonstrated that the proposed customized tensile test, due to the localized heat treatment, is capable of retrieving potential spatial gradients of material properties.


2020 ◽  
pp. 1-17
Author(s):  
W.-c. Xie ◽  
X.-l. Wang ◽  
D.-p. Duan ◽  
J.-w. Tang ◽  
Y. Wei

ABSTRACT Stratospheric airships are promising aircraft, usually designed as a non-rigid airship. As an essential part of the non-rigid airship, the envelope plays a significant role in maintaining its shape and bearing the external force load. Generally, the envelope material of a flexible airship consists of plain-weave fabric, composed of warp and weft fibre yarn. At present, biaxial tensile experiments are the primary method used to study the stress–strain characteristics of such flexible airship materials. In this work, biaxial tensile testing of UN-5100 material was carried out. The strain on the material under unusual stress and the stress ratio were obtained using Digital Image Correlation (DIC) technology. Also, the stress–strain curve was corrected by polynomial fitting. The slope of the stress–strain curve at different points, the Membrane Structures Association of Japan (MSAJ) standard and the Radial Basis Function (RBF) model were compared to identify the stress–strain characteristics of the materials. Some conclusions on the mechanical properties of the flexible airship material can be drawn and will play a significant role in the design of such envelopes.


2015 ◽  
Vol 137 (4) ◽  
Author(s):  
Baptiste Coudrillier ◽  
Jacek Pijanka ◽  
Joan Jefferys ◽  
Thomas Sorensen ◽  
Harry A. Quigley ◽  
...  

The objective of this study was to measure the collagen fiber structure and estimate the material properties of 7 human donor scleras, from age 53 to 91. The specimens were subjected to inflation testing, and the full-field displacement maps were measured by digital image correlation. After testing, the collagen fiber structure was mapped using wide-angle X-ray scattering. A specimen-specific inverse finite element method was applied to calculate the material properties of the collagen fibers and interfiber matrix by minimizing the difference between the experimental displacements and model predictions. Age effects on the fiber structure and material properties were estimated using multivariate models accounting for spatial autocorrelation. Older age was associated with a larger matrix stiffness (p = 0.001), a lower degree of fiber alignment in the peripapillary sclera (p = 0.01), and a lower mechanical anisotropy in the peripapillary sclera (p = 0.03).


2011 ◽  
Vol 70 ◽  
pp. 135-140 ◽  
Author(s):  
G. Le Louëdec ◽  
M.A. Sutton ◽  
Fabrice Pierron

Welding is one of the most popular joining technologies in industry. Depending on the materials to be joined, the geometry of the parts and the number of parts to be joined, there is a wide variety of methods that can be used. These joining techniques share a common feature: the material in the weld zone experiences different thermo-mechanical history, resulting in significant variations in material microstructure and spatial heterogeneity in mechanical properties. To optimize the joining process, or to refine the design of welded structures, it is necessary to identify the local mechanical properties within the different regions of the weld. The development of full-field kinematic measurements (digital image correlation, speckle interferometry, etc.) helps to shed a new light on this problem. The large amount of experimental information attained with these methods makes it possible to visualize the spatial distribution of strain on the specimen surface. Full-field kinematic measurements provide more information regarding the spatial variations in material behaviour. As a consequence, it is now possible to quantify the spatial variations in mechanical properties within the weld region through a properly constructed inverse analysis procedure. High speed tensile tests have been performed on FSW aluminium welds. The test was performed on an MTS machine at a cross-head speed of up to 76 mm/s. Displacement fields were measured across the specimen by coupling digital image correlation with a high-speed camera (Phantom V7.1) taking 1000 frames per second. Then, through the use of the virtual fields method it is possible to retrieve the mechanical parameters of the different areas of the weld from the strain field and the loading. The elastic parameters (Young’s modulus and Poisson’s ratio) are supposed to be constant through the weld. Their identification was carried out using the virtual fields method in elasticity using the data of the early stage of the experiment. Assuming that the mechanical properties (elastic and plastic) of the weld are constant through the thickness, the plastic parameters were identified on small sections through the specimen, using a simple linear hardening model. This method leads to a discrete identification of the evolution of the mechanical properties through the weld. It allows the understanding of the slight variations of yield stress and hardening due to the complexity of the welding process.


2012 ◽  
Vol 19 (5) ◽  
pp. 765-785 ◽  
Author(s):  
Peter Avitabile ◽  
Pawan Pingle

Dynamic response is an important consideration for design of structures due to operating or occasional loadings. The resulting dynamic stress strain is also of concern for fatigue and structural health monitoring. Typically, the actual loading and structural condition (boundary conditions, environmental condition, geometry, mechanical properties, etc.) are not necessarily known. Much effort is expended in attempting to identify the loads and appropriate model for prediction of these types of events. At best, the forces and actual boundary conditions are approximate and have an effect on the overall predicted response and resulting stress-strain that is identified for subsequent evaluation.Experimental data can only be obtained from limited sets of points, such as those typically collected with accelerometers. These are normally used in the evaluation the state of a structure in service condition. More recently, Digital Image Correlation (DIC) and Dynamic Photogrammetry (DP) have become very important techniques to measure the surface response. These are non-contact and full-field techniques, which allow that much more simultaneous data to be measure. The sets of limited surface data that are collected can be used in conjunction with an expansion algorithm to obtain full field information. The finite element model mass and stiffness matrices are used to obtain the normal constitutive relations as well as the modal characteristics. This information is used to develop the expansion algorithm and for the stress recovery during the back substitution process typically employed.


2014 ◽  
Vol 627 ◽  
pp. 305-308 ◽  
Author(s):  
Tomasz Brynk ◽  
Barbara Romelczyk ◽  
Zbigniew Pakiela ◽  
Tomasz Kurzynowski ◽  
Edward Chlebus

Mini-samples technique was utilized to determine mechanical properties of technically pure titanium produced by means of selective laser melting (SLM). Full-field digital image correlation (DIC) measurements and inverse method were applied for crack tip position and stress intensity factors calculations in the case of fatigue crack growth rate tests. DIC was also used for strain measurement during tensile tests on sub sized samples. There was studied the influence of samples orientation on the mechanical properties of mini-samples. Samples were cut out from rectangular cubes and were oriented with 0°, 45° or 90° angle to the direction of laser beam travel. There were also tested samples directly produced via SLM. Additionally microstructure observations were performed to verify the quality of SLM processed materials and explain mechanical properties variations.


Author(s):  
R. Miralbes ◽  
D. Ranz ◽  
D. Zouzias

AbstractExpanded polystyrene foams are a petroleum-origin material that is usually used in some applications such as motorcyclist helmets. Despite it notably mechanical properties, it low density and its capability to absorb energy during an impact, it is necessary to find a renewable-origin substitute material. Thus, it has been studied the use of a sawdust and mycelium composite material under quasi-static and dynamic efforts. Sawdust is a waste material that has very small grains that are totally disaggregated so it has very low material properties. The use of oyster mushroom mycelium generates an internal structure that joins grains and, consequently, the resultant material has notably high mechanical properties. Then it has been compared the resultant properties (stress-strain curve, absorbed energy, decelerations, etc.) with the different densities EPS ones and it has been concluded that this composite material, despite it high density, it could be a suitable substitute material and in some cases it has better properties.


2020 ◽  
Vol 10 (2) ◽  
pp. 468 ◽  
Author(s):  
Zhifeng Qi ◽  
Zhongqiang Shan ◽  
Weihao Ma ◽  
Linan Li ◽  
Shibin Wang ◽  
...  

Nanoscale silicon film electrodes in Li-ion battery undergo great deformations leading to electrochemical and mechanical failures during repeated charging-discharging cycles. In-situ experimental characterization of the stress/strain in those electrodes still faces big challenges due to remarkable complexity of stress/strain evolution while it is still hard to predict the association between the electrode cycle life and the measurable mechanical parameters. To quantificationally investigate the evolution of the mechanical parameters, we develop a new full field 3D measurement method combining digital image correlation with laser confocal profilometry and propose a strain criterion of the failure based on semi-quantitative analysis via mean strain gradient (MSG). The experimental protocol and results illustrate that the revolution of MSG correlates positively with battery capacity decay, which may inspire future studies in the field of film electrodes.


2014 ◽  
Vol 14 (06) ◽  
pp. 1440010
Author(s):  
AHMET C. CILINGIR

Soft tissues (e.g., tendon, skin, cartilage) change their dimensions and properties in response to applied mechanical stress/strain, which is called remodeling. Experimental studies using tissue cultures were performed to understand the biomechanical properties of collagen fascicles under mechanical loads. Collagen fascicles were dissected from sheep Achilles tendons and loaded under 1, 2, and 3 kg for 2, 4, and 6 days under culture. The mechanical properties of collagen fascicles after being loaded into the culture media were determined using tensile tester, and resultant stress–strain curves, tangent modulus, tensile strength, and strain at failure values were compared with those in a non-loaded and non-cultured control group of fascicles. The tangent modulus and tensile strength of the collagen fascicles increased with the increasing remodeling load after two days of culture. However, these values gradually decreased with the increasing culture period compared with the control group. According to the results obtained in this study, the mechanical properties of collagen fascicles were improved by loading at two days of culture, most likely due to the remodeling of collagen fibers. However, after a period of remodeling, local strains on the collagen fibrils increased, and finally, the collagen fibrils broke down, decreasing the mechanical properties of the tissue.


Author(s):  
Pradeep Lall ◽  
Geeta Limaye ◽  
Sandeep Shantaram ◽  
Jeff Suhling

Industry migration to lead-free solders has resulted in a proliferation of a wide variety of solder alloy compositions. The most popular amongst these are the Tin-Silver-Copper (Sn-Ag-Cu or SAC) family of alloys like SAC105, SAC305 etc. Recent studies have highlighted the detrimental effects of isothermal aging on the material properties of these alloys. SAC alloys have shown up to 50% reduction in their initial elastic modulus and ultimate tensile strength within a few months of elevated temperature aging. This phenomenon has posed a severe design challenge across the industry and remains a road-block in the migration to Pb-free. Multiple compositions with additives to SAC have been proposed to minimize the effect of aging and creep while maintaining the melting temperatures, strength and cost at par with SAC. Innolot is a newly developed high-temperature, high-performance lead-free substitute by InnoRel™ targeting the automotive electronics segment. Innolot contains Nickel (Ni), Antimony (Sb) and Bismuth (Bi) in small proportions in addition to Sn, Ag and Cu. The alloy has demonstrated enhanced reliability under thermal cycling as compared to SAC alloys. In this paper, the high strain rate material properties of Innolot have been evaluated as the alloy ages at an elevated temperature of 50°C. The strain rates chosen are in the range of 1–100 per-second which are typical at second level interconnects subjected to drop-shock environments. The strain rates and elevated aging temperature have been chosen also to correspond to prior tests conducted on SAC105 and SAC305 alloys at this research center. This paper presents a comparison of material properties and their degradation in the three alloys — SAC105, SAC305 and Innolot. Full field strain measurements have been accomplished with the use of high speed imaging in conjunction with Digital Image Correlation (DIC). Ramberg-Osgood non-linear model parameters have been determined to curve-fit through the experimental data. The parameters have been implemented in Abaqus FE model to obtain full-field stresses which correlates with contours obtained experimentally by DIC.


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