An investigation on the influence of sintering temperature on microstructural, physical and mechanical properties of Cu-SiC composites

2021 ◽  
Vol ahead-of-print (ahead-of-print) ◽  
Author(s):  
Nalin Somani ◽  
Y. K. Tyagi ◽  
Nitin Kumar Gupta

Purpose The purpose of this study is to investigate the effect of the sintering temperature on the microstructural, mechanical and physical properties of Cu-SiC composites. Design/methodology/approach The powder metallurgy route was used to fabricate the samples. Cold compaction of powders was conducted at 250 MPa which was followed by sintering at 850°C–950°C at the interval of 50 °C in the open atmospheric furnace. SiC was used as a reinforcement and the volumetric fraction of the SiC was varied as 10%, 15% and 20%. The processed samples were metallurgically characterized by the scanning electron microscope (SEM). Mechanical characterization was done using tensile and Vickers’ micro-hardness testing to check the hardness and strength of the samples. Archimedes principle and Four-point collinear probe method were used to measure the density and electrical resistivity of the samples. Findings SEM micrograph reveals the uniform dispersion of the SiC particles in the Cu matrix element. The results revealed that the Hardness and tensile strength were improved due to the addition of SiC and were maximum for the samples sintered at 950 °C. The addition of SiC has also increased the electrical resistivity of the Cu-SiC composite and was lowest for Cu 100% while the relative density has shown the reverse trend. Further, it was found that the maximum hardness of 91.67 Hv and ultimate tensile strength of 312.93 MPa were found for Cu-20% SiC composite and the lowest electrical resistivity of 2.017 µ- Ω-cm was found for pure Cu sample sintered at 950 °C, and this temperature was concluded as the optimum sintering temperature. Research limitations/implications The powder metallurgy route for the fabrication of the composites is a challenging task as the trapping of oxygen cannot be controlled during the compaction process as well as during the sintering process. So, a more intensive study is required to overcome these kinds of limitations. Originality/value As of the author’s best knowledge, no work has been reported on the effect of sintering temperature on the properties of the Cu-SiC composites which has huge potential in the industries.

Author(s):  
M. A. Salem ◽  
I. G. El-Batanony ◽  
M. Ghanem ◽  
Mohamed Ibrahim Abd ElAal

Different Al-SiC metal matrix composites (MMCs) with a different matrix, reinforcement sizes, and volume fractions were fabricated using ball milling (BM) and powder metallurgy (PM) techniques. Al and Al-SiC composites with different volume fractions were milled for 120 h. Then, the Al and Al-SiC composites were pressed under 125 MPa and finally sintered at 450 °C. Moreover, microsize and combination between micro and nano sizes Al-SiC samples were prepared by the same way. The effect of the Al matrix, SiC reinforcement sizes and the SiC volume fraction on the microstructure evolution, physical and mechanical properties of the produced composites was investigated. The BM and powder metallurgy techniques followed by sintering produce fully dense Al-SiC composite samples with different matrix and reinforcement sizes. The SiC particle size was observed to have a higher effect on the thermal conductivity, electrical resistivity, and microhardness of the produced composites than that of the SiC volume fraction. The decreasing of the Al and SiC particle sizes and increasing of the SiC volume fraction deteriorate the physical properties. On the other hand, the microhardness was enhanced with the decreasing of the Al, SiC particle sizes and the increasing of the SiC volume fraction.


2013 ◽  
Vol 58 (1) ◽  
pp. 43-48 ◽  
Author(s):  
B. Leszczynska-Madej

Attempts have been made to describe the influence of sintering temperature on the microstructure and properties of Al - SiC composites. Mixtures of 100%Al and Al - 5% SiC, Al - 10% SiC were produced by tumbling for 30 minutes in the Turbula T2F mixer. The powders were subsequently cold pressed at pressure 300MPa in a rigid die on a single action press. The green compacts were sintered in nitrogen at 580°C and 620°C for one hour. The main objective of this work was to determine influence of chemical composition and the manufacturing parameters on microstructure and properties of Al - SiC composites produced by powder metallurgy technology.


2019 ◽  
Vol 11 (2) ◽  
pp. 277-285
Author(s):  
Rajesh Kumar Bhushan ◽  
Deepak Sharma

Purpose Sound microstructure components are necessary for reliability and safety; hence, these components are used in aircraft, satellite, automobiles and ships, where many commercial alloys are not suitable. The paper aims to discuss this issue. Design/methodology/approach AA6082/Si3N4 and AA6082/SiC composites were fabricated using the stir-casting process considering 5, 10 and 15 vol.% of reinforcement particles. Density and porosity of AA6082/Si3N4 and AA6082/SiC composites were calculated. Characterization was done using an X-ray (EDX) detector, attached to SEM. The effect of addition of Si3N4 and SiC particulates in the AA6082 was investigated. Findings Results showed that Si3N4 and SiC particulates had good wettability with AA6082 and were uniformly distributed in AA6082 matrix. No adverse effects of reactions were noticed in the microstructure of AA6082/Si3N4 and AA6082/SiC composites. Research limitations/implications AA6082 with more than 15 vol.% of Si3N4 and AA6082/SiC reinforcement particles do not find industrial application where high hardness and tensile strength are required. Practical implications Components made from AA6082/Si3N4 and AA6082/SiC composites find their application where high hardness with better tensile strength is required. Social implications Naturally and locally available materials are utilized for fabrication. Originality/value Little work is available in the literature on fabrication and characterization of AA6082/Si3N4 and AA6082/SiC composites. The authors have identified the process parameters at which proper fabrication is done and sound microstructure is obtained.


2021 ◽  
pp. 002199832110157
Author(s):  
Müslim Çelebi ◽  
Onur Güler ◽  
Aykut Çanakçı ◽  
Hamdullah Çuvalcı

In this study, ZA27-Al2O3-Gr hybrid nanocomposite materials (HNMs) were prepared by powder metallurgy method including mechanical-milling and hot-pressing (HP). The physical and mechanical properties of ZA27-Al2O3-Gr HNMs have been investigated with the primary objective of understanding the influence of the alumina (Al2O3) nanoparticle (n-Al2O3) reinforcement. The density, hardness and tensile strength tests of HNMs carried out to determine the physical and mechanical properties of ZA27-Al2O3-Gr HNMs. Scanning Electron Microscope (SEM) is used for the microstructural evolution of the HNMs. As a result of microstructure examination results, n-Al2O3 were observed around grain boundary while the graphite (Gr) nanoparticles (n-Gr) were dispersed homogeneous throughout ZA27 matrix. Relative density values decreased with the increase of nanoparticle reinforcement ratio from 1%vol to 4%vol., while an increase in porosity values was detected for HNMs. Moreover, the results showed that the addition of n-Al2O3 significantly improved the mechanical properties of the HNMs. Additionally, the HNMs reinforced with 4%vol. n-Al2O3 and 1%vol. n-Gr exhibited the highest tensile strength of about 158 MPa and hardness of 160 HB in comparison with the other HNMs reinforced with different content of n-Al2O3.


2016 ◽  
Vol 1139 ◽  
pp. 55-58 ◽  
Author(s):  
Dibyendu Dutta Majumdar ◽  
Dehi Pada Mondal ◽  
Amit Roy Chowdhury ◽  
Harish Rao ◽  
Jyotsna Dutta Majumdar

The present study concerns detailed microstructural investigation and property evaluation of titanium-cenosphere composite developed by powder metallurgy route. The main process variables for the development of titanium-cenosphere composite were cenosphere particle size, sintering time, and sintering temperature. Followed by sintering, a detailed characterization of the sintered parts in terms of density, microstructure, composition and phase has been carried out. The compressive strength of the sintered component has also been evaluated in details. The density of the sintered pellets varied with process parameters and is significantly reduced (2.5-2.11 g/cm3) as compared to as-received titanium (4.5 g/cm3). The compressive yield strength of the sintered pellet is reduced as compared to as-received Ti-6Al-4V.


Materials ◽  
2019 ◽  
Vol 12 (4) ◽  
pp. 670 ◽  
Author(s):  
Xiangyang Chen ◽  
Rui Bao ◽  
Jianhong Yi ◽  
Dong Fang ◽  
Jingmei Tao ◽  
...  

Carbon nanotube (CNT)-reinforced metal matrix composites (MMCs) face the problems of dispersion and interfacial wetting with regard to the matrix. A synergetic method of spray pyrolysis (SP) and flake powder metallurgy (FPM) is used in this paper to improve the dispersibility and interfacial bonding of CNTs in a Cu matrix. The results of the interface characterization show interface oxygen atoms (in the form of Cu2O) and a high density of dislocation areas, which is beneficial for interfacial bonding. The tensile results show that the tensile strength of the SP-CNT-Cu composites is much higher than that of the CNT-Cu composites when the mass fraction of the CNTs does not reach the critical value. This can be explained by the nanoparticles which are found on the surface of the CNTs during the SP process. These nanoparticles not only increase the tensile strength of the SP-CNT-Cu composites but also improve the dispersion of the CNTs in the Cu matrix. Thereby, uniform dispersion of CNTs, interfacial bonding between CNTs and the Cu matrix, and the enhancement of tensile strength are achieved simultaneously by the synergetic method.


2016 ◽  
Vol 697 ◽  
pp. 350-353
Author(s):  
Da Ming Du ◽  
Rui Hua Wang ◽  
Jie Guang Song ◽  
Si Yuan Yu ◽  
Yao Qi Li ◽  
...  

Metal ceramics are a important new engineering materials with the advantages of ceramics and metal materials. The Al-Al2O3 metal ceramics were prepared via the powder metallurgy methods and characterized in this paper, which lay the base for preparing the high performance cermet materials. Through the results and analysis, the conclusions are shown that the relative density is increased with a increasing forming pressure, the electrical resistivity is decreased with a increasing forming pressure. The relative density is increased with a increasing sintering temperature under 700°C, the relative density decreases with a increasing sintering temperature above 700°C, the electrical resistivity is shown the opposite tendency. Through the optimizing the technological parameter, such as the sintering temperature at 700°C, the forming pressure under 20MPa, the Al content for 75wt%, Al-Al2O3 metal ceramics are successfully prepared with the high relative density and the low electrical resistivity, the relative density is 97.52%, and the electrical resistivity is 101.34Ω·m


2013 ◽  
Vol 795 ◽  
pp. 573-577 ◽  
Author(s):  
Zuraidawani Che Daud ◽  
Shamsul Baharin Jamaludin

F-75 (Co-Cr-Mo) alloy are widely used in the production of medical implants because of their excellent strength properties, hardness and also one of the biocompatible materials that very suitable in human body environment. In this research, the effect of sintering in terms of sintering temperature and sintering time has been studied by focusing on the microstructure, physical and mechanical properties of F-75 alloy. The samples were prepared by blending the starting material at 160 rpm for 30 minutes, uniaxially pressing at 500 MPa and sintering in an argon atmosphere at two sintering temperatures (1300°C and 1350°C) for four sintering times (60, 90, 120 and 150 minutes). The results show that the grains and bulk density increased with the increasing of sintering temperature and sintering times. However, opposite results were obtained for apparent porosity, hardness and compressive strength


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