High frequency wideband permittivity measurements of dielectric liquids using a new stripline structure technique

Author(s):  
M.A. Benaissa ◽  
A. Mokraoui ◽  
H. Moulai ◽  
A. Beroual
Geophysics ◽  
2018 ◽  
Vol 83 (1) ◽  
pp. MR1-MR14 ◽  
Author(s):  
Ali A. Garrouch

Dimensional analysis was performed to understand the physics of ionic dispersion in reservoir rocks and to identify the factors influencing the cation exchange capacity (CEC) of these rocks. Dimensional analysis revealed the existence of a general relation independent of the unit system between two dimensionless groups denoted as the cationic dispersion number [Formula: see text] and the conductivity number [Formula: see text]. The former group [Formula: see text] stands for the ratio of the CEC to the electrical double-layer dispersion. The latter group [Formula: see text] represents the ratio of the low-frequency ionic conductivity to the high-frequency electronic polarization. Complex dielectric permittivity measurements on 121 water-saturated sandstone and carbonate rock samples were used to validate the dimensionless groups. In retrospect, dimensional analysis was useful in identifying variables influencing the CEC of hydrocarbon rocks. In particular, these variables consist of rock porosity [Formula: see text], specific surface area, and five other parameters of the Cole-Cole function, which describes the frequency dependence of the complex permittivity of rock samples in the range 10–1300 MHz. The Cole-Cole function parameters are [Formula: see text], which is a characteristic relaxation time; [Formula: see text] is the so-called spread parameter; [Formula: see text] is the real DC conductivity of water-saturated rocks; and [Formula: see text] and [Formula: see text], which are the real numbers representing the static and the high-frequency dielectric permittivities of the water-saturated rock, respectively. A general regression neural network (GRNN) model was developed to predict the CEC of shaly sandstones and carbonate rocks as a function of the variables identified by the dimensional analysis as essential in predicting the CEC. The CEC prediction capability of the GRNN model has been tested with a blind data set, and it has been compared with the CEC prediction capability using a nonlinear regression model developed in this study and using a linear regression model available in the literature. The GRNN model outperformed both of these empirical models. With the GRNN model, it is possible to obtain reliable quantitative estimates of the CEC of shaly sandstone and carbonate rocks using nondestructive frequency-dependent dielectric permittivity measurements that are rapid, economic, and accurate. In return, accurate and fast estimates of the CEC are useful in many petroleum engineering applications. They can be used to identify clay types and can also be used to quantify the volume of hydrocarbon in shaly sands using well-log resistivity data. The results of this study represent a major advantage for formation evaluation, wellbore stability analysis, and designing stimulation jobs.


Energies ◽  
2019 ◽  
Vol 12 (6) ◽  
pp. 1063 ◽  
Author(s):  
Stefan Wolny

This paper presents research results of the loss factor of high voltage insulation samples made of aramid paper impregnated with various types of insulating oil. The analysis was carried out in the high frequency domain in the range of 50 Hz to 1 MHz. The experiments were carried out for three impregnation types: mineral oil, synthetic ester and natural ester. The influence of temperature in the range of 20 °C to 100 °C, which is typical when using this type of insulation in power transformers, was taken into account. In addition, the process of influence of initial aging of aramid paper was simulated by heat soaking the samples before their impregnation at a temperature of 250 °C in multiple time intervals. Based on the analyses of dispersion characteristics of insulation sample loss factors, conclusions and recommendations for further diagnostics of aramid-oil insulations using the method described were delineated.


Sensors ◽  
2020 ◽  
Vol 20 (17) ◽  
pp. 4684
Author(s):  
Rafael Pérez-Campos ◽  
José Fayos-Fernández ◽  
Antonio José Lozano-Guerrero ◽  
Antonio Martínez-González ◽  
Juan Monzó-Cabrera ◽  
...  

Permittivity of materials is of utmost importance for microwave applicators’ design and to predict high-frequency dielectric heating of materials. In the case of aromatic plant biomass, however, there are few data that help researchers design microwave applicators for microwave-assisted extraction. In this work, the permittivity of cypress and rockrose biomass samples were measured versus temperature, density, and moisture content. A resonant technique based on a coaxial bi-reentrant microwave cavity was employed to obtain the complex permittivity of biomass samples as a function of those magnitudes around the 2.45 GHz ISM frequency. The obtained measurements show that large variations for permittivity values can be found with moisture content and density changes for both cypress and rockrose biomass. Temperature also has effects in a lesser degree, although it has an important influence on the cypress biomass loss factor. Polynomial expressions fitting the experimental data were provided in order to facilitate the estimation of intermediate values, which were not explicitly arranged in this work. As a general trend, the permittivity of cypress and rockrose biomass increases with increasing values of moisture content and density, whereas the biomass loss factor increases when temperature rises.


Author(s):  
Leslie Y. Yeo ◽  
Dimitri Lastochkin ◽  
Hsueh-Chia Chang

A new high-frequency (> 10 kHz) AC electrospray phenomenon which behaves distinctly to DC electrosprays is investigated. Unlike DC electrosprays, the drops do not emanate from the usual well-defined Taylor cone-jet and carry no net charge. Instead, the meniscus vibrates at a resonant frequency associated with its capillary-inertia vibration time, periodically ejecting drops with dimensions of order 10 μm under the action of the Maxwell-Wagner electric stress at the meniscus tip. Above a crossover frequency, the polarization and direction of the Maxwell force reverses and an apparent electrowetting effect is observed. A simple lubrication model is used to generate spatio-temporal evolution profiles for the stretched liquid meniscus tip as a function of the Maxwell-Wagner stress and a capillary number. From a self-similar scaling technique, the meniscus is shown to advance as t1/2.


Author(s):  
W. E. Lee ◽  
A. H. Heuer

IntroductionTraditional steatite ceramics, made by firing (vitrifying) hydrous magnesium silicate, have long been used as insulators for high frequency applications due to their excellent mechanical and electrical properties. Early x-ray and optical analysis of steatites showed that they were composed largely of protoenstatite (MgSiO3) in a glassy matrix. Recent studies of enstatite-containing glass ceramics have revived interest in the polymorphism of enstatite. Three polymorphs exist, two with orthorhombic and one with monoclinic symmetry (ortho, proto and clino enstatite, respectively). Steatite ceramics are of particular interest a they contain the normally unstable high-temperature polymorph, protoenstatite.Experimental3mm diameter discs cut from steatite rods (∼10” long and 0.5” dia.) were ground, polished, dimpled, and ion-thinned to electron transparency using 6KV Argon ions at a beam current of 1 x 10-3 A and a 12° angle of incidence. The discs were coated with carbon prior to TEM examination to minimize charging effects.


Author(s):  
G. Y. Fan ◽  
J. M. Cowley

It is well known that the structure information on the specimen is not always faithfully transferred through the electron microscope. Firstly, the spatial frequency spectrum is modulated by the transfer function (TF) at the focal plane. Secondly, the spectrum suffers high frequency cut-off by the aperture (or effectively damping terms such as chromatic aberration). While these do not have essential effect on imaging crystal periodicity as long as the low order Bragg spots are inside the aperture, although the contrast may be reversed, they may change the appearance of images of amorphous materials completely. Because the spectrum of amorphous materials is continuous, modulation of it emphasizes some components while weakening others. Especially the cut-off of high frequency components, which contribute to amorphous image just as strongly as low frequency components can have a fundamental effect. This can be illustrated through computer simulation. Imaging of a whitenoise object with an electron microscope without TF limitation gives Fig. 1a, which is obtained by Fourier transformation of a constant amplitude combined with random phases generated by computer.


Author(s):  
M. T. Postek ◽  
A. E. Vladar

Fully automated or semi-automated scanning electron microscopes (SEM) are now commonly used in semiconductor production and other forms of manufacturing. The industry requires that an automated instrument must be routinely capable of 5 nm resolution (or better) at 1.0 kV accelerating voltage for the measurement of nominal 0.25-0.35 micrometer semiconductor critical dimensions. Testing and proving that the instrument is performing at this level on a day-by-day basis is an industry need and concern which has been the object of a study at NIST and the fundamentals and results are discussed in this paper.In scanning electron microscopy, two of the most important instrument parameters are the size and shape of the primary electron beam and any image taken in a scanning electron microscope is the result of the sample and electron probe interaction. The low frequency changes in the video signal, collected from the sample, contains information about the larger features and the high frequency changes carry information of finer details. The sharper the image, the larger the number of high frequency components making up that image. Fast Fourier Transform (FFT) analysis of an SEM image can be employed to provide qualitiative and ultimately quantitative information regarding the SEM image quality.


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