Influence of Heat Treatment on Dental Prostheses Produced by Additive Technology

Author(s):  
Viktoria Rajt'ukova ◽  
Lubos Chromy ◽  
Alena Findrik Balogova ◽  
Gabriela Izarikova ◽  
Andrea Sincak Konecna ◽  
...  
2019 ◽  
Vol 104 ◽  
pp. 01010 ◽  
Author(s):  
Vladimir Dub ◽  
Pavel Medvedev ◽  
Konstantin Kudrin ◽  
Aliy Delov ◽  
Stepan Stepanov ◽  
...  

This article shows the possibility of additive technology applied to medical implants. It’s shown the difference of physical properties such as elastic module of bones, implants made of traditional technology and implants made of additive technology. Porous structure has been chosen for future implants through designing its and further calculation of its mechanical properties using software such as Solid Works, Logos and Ansys. To confirm the right choice of design of structure we manufactured samples with using Rosatom 3D printer, made heat treatment and tested them.


2019 ◽  
Vol 58 (1) ◽  
pp. 218-225
Author(s):  
Damian S. Nakonieczny ◽  
Agata Sambok ◽  
Magdalena Antonowicz ◽  
Marcin Basiaga ◽  
Zbigniew K. Paszenda ◽  
...  

Abstract Purpose: This part of the study focuses on the influence of zirconia heat treatment for surface morphology, phase composition and mechanical properties Methods: Zirconia samples was prepared with ISO 13356:2013 and ISO 14704:2008 recommendations. X-ray diffraction, observations (SEM) and (AFM), microhardness (Olivera & Phara method), and static bending test (4PBT) were taken. Results: characterization of YSZ and high temperature heat treatment has clearly shown that the aging process influences the change in phase composition of the material, significantly worsening the topography. In turn, re-treatment of the high temperature made after the artificial aging process results in reverse transformation of the desired tetragonal phase, but does not affect the improvement of surface morphology. Conclusions: The research made it possible to assess the negative impact of the zirconium oxide aging simulation process. Because of the failure to achieve the intended results, it was also proved that the high-temperature re-processing was not appropriate.


2019 ◽  
Author(s):  
Marina Yu. Panchenko ◽  
Valentina A. Moskvina ◽  
Sergey V. Astafurov ◽  
Galina G. Maier ◽  
Evgenii V. Melnikov ◽  
...  

Materials ◽  
2021 ◽  
Vol 14 (15) ◽  
pp. 4159
Author(s):  
Marina Gushchina ◽  
Gleb Turichin ◽  
Olga Klimova-Korsmik ◽  
Konstantin Babkin ◽  
Lyubov Maggeramova

Additive manufacturing of titanium alloys is one of the fastest growing areas of 3D metal printing. The use of AM methods for parts production in the aviation industry is especially promising. During the deposition of products with differently sized cross-sections, the thermal history changes, which leads to non-uniformity of the structure and properties. Such heterogeneity can lead to failure of the product during operation. The structure of deposited parts, depending on the thermal cycle, may consist of α’, α + α’ + β’, and α + β in different ratios. This problem can be solved by using heat treatment (HT). This paper presents research aimed towards the determination of optimal heat treatment parameters that allows the reception of the uniform formation of properties in the after-treatment state, regardless of the initial structure and properties, using the example of a deposited Ti-6Al-4V gas turbine blade.


2021 ◽  
Vol 2094 (4) ◽  
pp. 042037
Author(s):  
A M Khakimov ◽  
K V Nikitin ◽  
S S Zhatkin

Abstract This paper presents the development of stable modes of additive technology of direct laser growing, using the starting material - a metal powder made of heat-resistant EP648 alloy of Russian production. The subsequent heat treatment of the manufactured samples was tested in order to avoid the formation of cracks in the structure of the material formed as a result of the presence of internal stresses after surfacing. Recommendations for further research are given.


Author(s):  
Oksana Savvova ◽  
Oleksii Fesenko ◽  
Hennadii Voronov ◽  
Emin Salekh Ohly Bairamov

The relevance of the problem of improving the quality of life and protecting human health in the context of the successful development of the modern society was presented. A literary review of well-known modern technologies for the design and manufacture of dental prostheses was carried out, as well as the leading domestic and foreign companies that were engaged in this were given. The history of the development of materials for obtaining clinical restorations (crowns, inlays, onlays, etc.) was considered and the main directions of the development of innovative ceramic materials for dental prosthetics were outlined. Based on the analysis of the properties of various types of materials for dental prosthetics, the prospects of using glass-ceramic materials in the development of dental prostheses have been substantiated. The chemical compositions of lithium silicate glasses for the synthesis of the glass matrix have been developed and the technological parameters for the production of glass-ceramic dental prostheses have been selected (Тgl. melting = 1350–1400 °С, Тheat treatment = 600–650 °С). Preliminary heat treatment before the formation of products ensures the formation of the required number of the nucleus of crystalline phase and the prerequisites for creating a volume crystallized structure under conditions of short-term heat treatment. The glass-ceramic prosthesis with a formed interpenetrating sitallized structure was obtained by the method of hot pressing with a short exposure (18-20 min). It was found that the obtained glass-ceramic material containing lithium disilicate as a crystalline phase in an amount of 40-60 vol. %, had high values of bending strength (σ = 400 MPa) and fracture toughness. The indicated mechanical properties of the developed materials, along with the approximate values of their modulus of elasticity to natural teeth, will significantly extend the service life of products under conditions of significant alternating loads that arise during the chewing cycle. A comparative assessment of the competitiveness of the developed dental prostheses based on lithium disilicate with world analogues was carried out, in particular the products of Ivoclar Vivadent and Vita Zahnfabrik, in terms of the main operational parameters. The positive effect of the introduction of domestic developed glass-ceramic dental prostheses to reduce import dependence has been determined.


Author(s):  
R. M. Anderson

Aluminum-copper-silicon thin films have been considered as an interconnection metallurgy for integrated circuit applications. Various schemes have been proposed to incorporate small percent-ages of silicon into films that typically contain two to five percent copper. We undertook a study of the total effect of silicon on the aluminum copper film as revealed by transmission electron microscopy, scanning electron microscopy, x-ray diffraction and ion microprobe techniques as a function of the various deposition methods.X-ray investigations noted a change in solid solution concentration as a function of Si content before and after heat-treatment. The amount of solid solution in the Al increased with heat-treatment for films with ≥2% silicon and decreased for films <2% silicon.


Author(s):  
E. Bischoff ◽  
O. Sbaizero

Fiber or whisker reinforced ceramics show improved toughness and strength. Bridging by intact fibers in the crack wake and fiber pull-out after failure contribute to the additional toughness. These processes are strongly influenced by the sliding and debonding resistance of the interfacial region. The present study examines the interface in a laminated 0/90 composite consisting of SiC (Nicalon) fibers in a lithium-aluminum-silicate (LAS) glass-ceramic matrix. The material shows systematic changes in sliding resistance upon heat treatment.As-processed samples were annealed in air at 800 °C for 2, 4, 8, 16 and 100 h, and for comparison, in helium at 800 °C for 4 h. TEM specimen preparation of as processed and annealed material was performed with special care by cutting along directions having the fibers normal and parallel to the section plane, ultrasonic drilling, dimpling to 100 pm and final ionthinning. The specimen were lightly coated with Carbon and examined in an analytical TEM operated at 200 kV.


Author(s):  
A.H. Advani ◽  
L.E. Murr ◽  
D. Matlock

Thermomechanically induced strain is a key variable producing accelerated carbide precipitation, sensitization and stress corrosion cracking in austenitic stainless steels (SS). Recent work has indicated that higher levels of strain (above 20%) also produce transgranular (TG) carbide precipitation and corrosion simultaneous with the grain boundary phenomenon in 316 SS. Transgranular precipitates were noted to form primarily on deformation twin-fault planes and their intersections in 316 SS.Briant has indicated that TG precipitation in 316 SS is significantly different from 304 SS due to the formation of strain-induced martensite on 304 SS, though an understanding of the role of martensite on the process has not been developed. This study is concerned with evaluating the effects of strain and strain-induced martensite on TG carbide precipitation in 304 SS. The study was performed on samples of a 0.051%C-304 SS deformed to 33% followed by heat treatment at 670°C for 1 h.


Author(s):  
R. Padmanabhan ◽  
W. E. Wood

Intermediate high temperature tempering prior to subsequent reaustenitization has been shown to double the plane strain fracture toughness as compared to conventionally heat treated UHSLA steels, at similar yield strength levels. The precipitation (during tempering) of metal carbides and their subsequent partial redissolution and refinement (during reaustenitization), in addition to the reduction in the prior austenite grain size during the cycling operation have all been suggested to contribute to the observed improvement in the mechanical properties. In this investigation, 300M steel was initially austenitized at 1143°K and then subjected to intermediate tempering at 923°K for 1 hr. before reaustenitizing at 1123°K for a short time and final tempering at 583°K. The changes in the microstructure responsible for the improvement in the properties have been studied and compared with conventionally heat treated steel. Fig. 1 shows interlath films of retained austenite produced during conventionally heat treatment.


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