Application of the 3ω Hot Wire Technique for Measurement of Fluid Thermophysical Properties

Author(s):  
Brandon W. Olson ◽  
Ali Fahham

The popular 3ω method of measuring thermophysical properties of solids is adapted for the simultaneous measurement of thermal conductivity and heat capacity in both liquids and gases. This technique is experimentally simple and has a lower susceptibility to random experimental noise, bulk fluid motion, radiation losses, and non-linear effects than other transient hot wire measurement methods. The compactness of the 3ω hotwire allows it to be used with different fluids in a variety of circumstances with very little specialized experimental equipment. Both the experimental setup and theoretical model are detailed. Experimental 3ω measurements were made in a variety of common fluids (air, water, and mineral oil) using commercially drawn 10μm platinum and 5μm tungsten hot wires which serve as both heating element and resistance thermometer. Measurements taken over a range of frequencies are numerically reduced to provide both thermal conductivity and heat capacity information. Experimental measurements and the corresponding analytical model are presented in terms of impedance or thermal resistance; a more physically meaningful and intuitive basis of comparison. Fluid properties are determined by curve-fitting an analytical model to experimental data using a least-squares approach. This technique allows both thermal conductivity and heat capacity (or thermal diffusivity) to be uniquely determined from a single measurement sequence.

2004 ◽  
Vol 18 (10n11) ◽  
pp. 1489-1502 ◽  
Author(s):  
V. GIARETTO ◽  
M. F. TORCHIO

A prototype apparatus that uses two platinum wires for the simultaneous estimation of the thermal conductivity and specific heat capacity of liquids is described. The first wire is used both as a hot wire and a resistance thermometer, while the second one is used as a resistance thermometer. The aim of the work was to experimentally verify the advantages of employing a second wire to improve the reliability of the estimation of the properties. Three different liquids: water, propylene glycol, and a mixture of these are considered. An analytical solution with a changing heat flux is adopted. The thermal conductivity and the specific heat capacity are simultaneously estimated with a nonlinear regression (Maximum Likelihood) of the experimental data, using two-wire measurements or only hot-wire measurements. A comparison between these two approaches is reported and discussed.


Author(s):  
D.Ya. Barinov ◽  
◽  
S.Yu. Shorstov ◽  
M.G. Razmahov ◽  
A.I. Gulyaev ◽  
...  

When designing advanced samples of aviation and rocket and space technology, during the operation of which the temperature on the surface of the material can exceed the temperature of destruction, it is important to have an understanding of the values of thermophysical properties. The work investigates the thermophysical properties of fiberglass in the initial state and after the binder is burned out in a muffle furnace. The temperature dependences of thermal effects, heat capacity, thermal diffusivity and thermal conductivity were determined, density was measured, and thermogravimetric analysis was carried out. Using a stereomicroscope, the microstructure of the lateral cut of the samples was examined and its evolution was determined during the burning of the binder.


2017 ◽  
Vol 21 (3) ◽  
pp. 1195-1202 ◽  
Author(s):  
Andrej Stanimirovic ◽  
Emila Zivkovic ◽  
Nenad Milosevic ◽  
Mirjana Kijevcanin

Transient hot wire method is considered a reliable and precise technique for measuring the thermal conductivity of liquids. The present paper describes a new transient hot wire experimental set-up and its initial testing. The new apparatus was tested by performing thermal conductivity measurements on substances whose reference thermophysical properties data existed in literature, namely on pure toluene and double distilled deionized water. The values of thermal conductivity measured in the temperature range 25 to 45 ?C deviated +2.2% to +3% from the literature data, while the expanded measurement uncertainty was estimated to be ?4%.


2019 ◽  
Vol 2019 ◽  
pp. 1-9 ◽  
Author(s):  
Ľuboš Krišťák ◽  
Rastislav Igaz ◽  
Ivan Ružiak

The results of using the EDPS (extended dynamic plane source) method to determine thermophysical properties of solid wood of coniferous trees growing in Slovakia with 0% and 12% equilibrium moisture content are presented in the paper. Solid wood of two different tree species: Norway spruce (Picea abies L.) and Scots pine (Pinus sylvestris L.) was used in the research. The research was carried out independently in three anatomical planes. Coefficients of thermal conductivity, thermal diffusivity, and specific heat capacity were determined following the research. Comparing the research results to the values determined by other authors and already published models to calculate individual parameters, the fact that the data gathered using the EDPS method can be accepted in case of all studied thermophysical properties can be stated.


2020 ◽  
Vol 10 (01n02) ◽  
pp. 2060019
Author(s):  
Sidek Khasbulatov ◽  
Suleiman Kallaev ◽  
Haji Gadjiev ◽  
Zairbek Omarov ◽  
Abumuslim Bakmaev ◽  
...  

The paper presents the results of a comprehensive study of the thermophysical properties (thermal conductivity, thermal diffusivity, heat capacity) of high-temperature multiferroic BiFeO3 modified with rare-earth elements (REEs) (La, Pr, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Lu). The regularities of the formation of the mentioned characteristics were established. The assumptions about the nature of the observed phenomena were suggested.


2021 ◽  
Vol 2119 (1) ◽  
pp. 012135
Author(s):  
D A Samoshkin ◽  
A Sh Agazhanov ◽  
S V Stankus

Abstract The heat capacity and the thermal diffusivity of NP2 brand nickel were investigated in the temperature interval 296–1000…1375 K of the solid-state, including the region of the magnetic phase transformation. Measurements were carried out on samples from one initial ingot by laser flash technique and method of differential scanning calorimetry using LFA-427 and DSC 404 F1 setups, respectively. The thermal conductivity was calculated based on the measured thermophysical properties. The estimated errors of the obtained results were 2–4%, 3–5%, and 2–3% for thermal diffusivity, thermal conductivity, and heat capacity, respectively. For investigated thermophysical properties the fitting equations and the reference table have been received.


2021 ◽  
pp. 44-48
Author(s):  
S.I. Bananyarli ◽  

The termophisical properties, namely, the temperature dependence of thermal conductivity, thermal resistance and heat capacity of the allays compositions (2Bi2O3∙B2O3)100-x (2Bi2O3∙3GeO2)x in the (300–600) K temperature range have ligated been invest. An increase in thermal conductivity χ(T) above 500 K is probably associated with the softening of alloys and the presence of blurred phase transitions, which are accompanied by partial breaking of chemical bonds. It was revealed that the heat capacity in alloys of the compositions (2Bi2O3∙B2O3)100-x (2Bi2O3∙3GeO2)x increases with an increase in the GeO2 concentration. In the studied samples, that showed their own disorder during solidification, the thermal conductivity is strongly reduced due to the enhancement of the anharmonicity of phonon – phonon interactions. İn turn a small "disorder" introduced by defects due to the difference in masses is not noticeable against the background of the huge "disorder" inherent in oxide substances


Author(s):  
B. W. Zhao ◽  
Y. Zhao ◽  
H. Liu ◽  
Y. Q. Li ◽  
K. X. Duan ◽  
...  

Soil thermophysical properties are the key factors affecting the internal heat balance of soil. In this paper, biochars (BC300, BC500 and BC700) were produced with wheat straw at the temperatures of 300, 500 and 700°, respectively. The effects of biochar amendment at the rates of 0%, 1%, 3%, and 5% on the thermophysical properties (thermal conductivity, heat capacity, and thermal diffusivity) of a loessial soil were investigated with and without water content respectively. Although the bulk density of soil significantly decreased with biochar amendment, due to enhancing soil porosity and organic matter content, the thermophysical properties of soil did not change largely with biochar amendment rate and pyrolysis temperature. Water content exhibited significant effects on the thermophysical properties of soils added with biochars, where the thermal conductivity and heat capacity of soil were linearly proportional to water content, the thermal diffusivity initially increased and then decreased with the increase of water content. In the meanwhile, there was no significant correlation between the biochar amendment rate or pyrolysis temperature and thermophysical properties. The results show that water content should be mainly concerned as a factor when the internal heat balance of loess soil is evaluated, even though the soil is amended with biochar.


Author(s):  
A.V. Zuev ◽  
◽  
Yu.P. Zarichnyak ◽  
D.Ya. Barinov ◽  
L.L. Krasnov ◽  
...  

The paper presents the results of measuring thermal conductivity and heat capacity of a flexible thermal insulation. Flexible thermal insulation is a highly porous fibrous material, a construction that includes felt, covered on all sides with fabric. The whole structure is stitched with a thread. The fibrous core, fabric and sewing thread are composed of silica fibers. Thermal conductivity was measured by the stationary method on flat samples. The heat capacity was determined using a NT-1000 calorimeter. The calculation of heat transfer was carried out for the conditions characteristic of those in effect when the spacecraft entered the orbit.


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