scholarly journals Ultrastrong nanotwinned pure nickel with extremely fine twin thickness

2021 ◽  
Vol 7 (27) ◽  
pp. eabg5113
Author(s):  
Fenghui Duan ◽  
Yan Lin ◽  
Jie Pan ◽  
Lei Zhao ◽  
Qiang Guo ◽  
...  
Keyword(s):  
Critical Size ◽  
Alternative Pathway ◽  
High Strength ◽  
Dislocation Motion ◽  
Pure Nickel ◽  
Coarse Grained ◽  
Strengthening Mechanisms ◽  
Ultrahigh Strength ◽  
Twin Thickness ◽  
Excellent Stability

The strength of nanocrystalline and nanotwinned metals stops increasing or even starts decreasing when their grain size or twin thickness is below a critical size—a phenomenon known as Hall-Petch breakdown—which hinders the attainment of ultrahigh strength. Here, we report continuous strengthening in nanotwinned pure Ni with twin thicknesses ranging from 81.0 to 2.9 nm. An unprecedented strength of 4.0 GPa was achieved at extremely fine twin thickness of 2.9 nm, which is about 12 times stronger than that of conventional coarse-grained nickel. This ultrahigh strength arises from the excellent stability of twin boundaries and their strong impedance to dislocation motion. In particular, we find that secondary nanotwins are activated to sustain plastic deformation, which also contribute to the high strength. These results not only advance the understanding of the strengthening mechanisms in nanotwinned metals but also offer an alternative pathway to develop engineering materials with ultrahigh strength.

Effect of the Welding Thermal Cycles Based on Simulated Heat Affected Zone of S1300 Ultrahigh Strength Steel

2021 ◽  
Vol 890 ◽  
pp. 33-43
Author(s):  
Judit Kovács ◽  
János Lukács
Keyword(s):  
Mechanical Properties ◽  
Heat Affected Zone ◽  
Research Work ◽  
High Strength Steels ◽  
High Strength ◽  
Optical Microscope ◽  
Coarse Grained ◽  
Ultrahigh Strength ◽  
Ultrahigh Strength Steel ◽  
Strength And Toughness

In the automotive industry there is an increasing demand for the wider application of high strength steels due to their favourable mechanical properties. The steel producers continuously developing new generations of high strength steels to insure higher strength and toughness properties. Since in most cases these steels are joined in welded structures, great attention must be taken to their weldability. The weldability of high strength steels has still challenges which are as follows: cold cracking sensitivity; reduction of strength and toughness of heat affected zone (HAZ); filler metal selection. Because the mechanical properties of ultrahigh strength steels are provided by using various alloying elements, micro alloys, and by different metallurgical methods, the steels may lose their outstanding properties during welding. In real welded joints the critical parts of the HAZ have small extent so their properties can be limitedly analysed by conventional material testing methods. With the help of physical simulators, the different parts of the heat affected zone can be produced in an adequate size for subsequent tests. In our research work the weldability, especially the HAZ properties of an ultrahigh strength structural steel (Rp0.2 = 1300 MPa) were investigated on thermal simulated samples with the help of Gleeble 3500 physical simulator. Three relevant technological variants for gas metal arc welding (GMAW), t8/5 = 5 s, 15 s and 30 s were applied during the HAZ simulations in the selected coarse-grained (CGHAZ), intercritical (ICHAZ) and intercritically reheated coarse-grained (ICCGHAZ) zones. Both the microstructure was studied by optical microscope and the mechanical properties were analysed by Vickers hardness tests and Charpy V-notch impact tests at -40 °C. According to the results the investigated ultrahigh strength steel was softened on account of the welding heat cycles, besides that the strength of the investigated ultrahigh strength steel can be better with the application of shorter t8/5 cooling time.

USS 18-8S and 18-8L

Alloy Digest ◽  
1975 ◽  
Vol 24 (2) ◽  
Keyword(s):  
Fracture Toughness ◽  
High Strength ◽  
Heat Treating ◽  
Cryogenic Temperatures ◽  
United States Steel Corporation ◽  
Temperature Performance ◽  
Aisi Type ◽  
Shock Resistance ◽  
Type 304 ◽  
Excellent Stability

Abstract USS 18-8S (AISI Type 304) and USS 18-8I (AISI Type 304L) are austenitic chromium-nickel steels that are easy to fabricate and weld. They combine high strength with excellent stability and shock resistance, even at cryogenic temperatures. This datasheet provides information on composition, physical properties, hardness, elasticity, and tensile properties as well as fracture toughness, creep, and fatigue. It also includes information on low temperature performance and corrosion resistance as well as forming, heat treating, and joining. Filing Code: SS-305. Producer or source: United States Steel Corporation.

Effect of Microstructure on High-Strength Low-Alloy Steel Welded Joint Toughness with Simulation of Heat-Affected Zone Coarse-Grained Area

Metallurgist ◽  
2021 ◽  
Vol 64 (9-10) ◽  
pp. 875-884
Author(s):  
K. G. Vorkachev ◽  
P. P. Stepanov ◽  
L. I. Éfron ◽  
M. M. Kantor ◽  
A. V. Chastukhin ◽  
...  
Keyword(s):  
Alloy Steel ◽  
Heat Affected Zone ◽  
Welded Joint ◽  
High Strength ◽  
Coarse Grained ◽  
Low Alloy Steel ◽  
Effect Of Microstructure

Microstructural Refinement in a Commercial Aluminum Alloy Processed by ECAP Using a Die Channel Angle of 110 Degrees

2015 ◽  
Vol 1114 ◽  
pp. 3-8
Author(s):  
Nicolae Şerban ◽  
Doina Răducanu ◽  
Nicolae Ghiban ◽  
Vasile Dănuţ Cojocaru
Keyword(s):  
Grain Refinement ◽  
Cross Section ◽  
High Strength ◽  
Secondary Phase ◽  
Coarse Grained ◽  
Metallographic Analysis ◽  
Second Phase ◽  
Channel Angle ◽  
Ambient Temperatures ◽  
Fine Grained

The properties of ultra-fine grained materials are superior to those of corresponding conventional coarse grained materials, being significantly improved as a result of grain refinement. Equal channel angular pressing (ECAP) is an efficient method for modifying the microstructure by refining grain size via severe plastic deformation (SPD) in producing ultra-fine grained materials (UFG) and nanomaterials (NM). The grain sizes produced by ECAP processing are typically in the submicrometer range and this leads to high strength at ambient temperatures. ECAP is performed by pressing test samples through a die containing two channels, equal in cross-section and intersecting at a certain angle. The billet experiences simple shear deformation at the intersection, without any precipitous change in the cross-section area because the die prevents lateral expansion and therefore the billet can be pressed more than once and it can be rotated around its pressing axis during subsequent passes. After ECAP significant grain refinement occurs together with dislocation strengthening, resulting in a considerable enhancement in the strength of the alloys. A commercial AlMgSi alloy (AA6063) was investigated in this study. The specimens were processed for a number of passes up to nine, using a die channel angle of 110°, applying the ECAP route BC. After ECAP, samples were cut from each specimen and prepared for metallographic analysis. The microstructure of the ECAP-ed and as-received material was investigated using optical (OLYMPUS – BX60M) and SEM microscopy (TESCAN VEGA II – XMU). It was determined that for the as-received material the microstructure shows a rough appearance, with large grains of dendritic or seaweed aspect and with a secondary phase at grain boundaries (continuous casting structure). For the ECAP processed samples, the microstructure shows a finished aspect, with refined, elongated grains, also with crumbled and uniformly distributed second phase particles after a typical ECAP texture.

scholarly journals Heterogeneous lamella structure unites ultrafine-grain strength with coarse-grain ductility

2015 ◽  
Vol 112 (47) ◽  
pp. 14501-14505 ◽  
Author(s):  
Xiaolei Wu ◽  
Muxin Yang ◽  
Fuping Yuan ◽  
Guilin Wu ◽  
Yujie Wei ◽  
...  
Keyword(s):  
Large Scale ◽  
Low Cost ◽  
High Strength ◽  
Back Stress ◽  
Coarse Grained ◽  
Ultrafine Grain ◽  
Asymmetric Rolling ◽  
Dislocation Hardening ◽  
Ultrafine Grained ◽  
Lamella Structure

Grain refinement can make conventional metals several times stronger, but this comes at dramatic loss of ductility. Here we report a heterogeneous lamella structure in Ti produced by asymmetric rolling and partial recrystallization that can produce an unprecedented property combination: as strong as ultrafine-grained metal and at the same time as ductile as conventional coarse-grained metal. It also has higher strain hardening than coarse-grained Ti, which was hitherto believed impossible. The heterogeneous lamella structure is characterized with soft micrograined lamellae embedded in hard ultrafine-grained lamella matrix. The unusual high strength is obtained with the assistance of high back stress developed from heterogeneous yielding, whereas the high ductility is attributed to back-stress hardening and dislocation hardening. The process discovered here is amenable to large-scale industrial production at low cost, and might be applicable to other metal systems.

Effect of Welding Processes with High Heat Input on the Microstructure and Toughness of Coarse-Grained Heat-Affected Zone of a High-Strength High-Toughness Steel

2018 ◽  
Vol 937 ◽  
pp. 61-67
Author(s):  
Yu Jie Li ◽  
Jin Wei Lei ◽  
Xuan Wei Lei ◽  
Oleksandr Hress ◽  
Kai Ming Wu
Keyword(s):  
Low Temperature ◽  
Impact Toughness ◽  
Heat Affected Zone ◽  
Heat Input ◽  
High Strength ◽  
High Heat ◽  
Coarse Grained ◽  
Low Temperature Impact Toughness ◽  
The Impact ◽  
Welding Processes

Utilizing submerged arc welding under heat input 50 kJ/cm on 60 mm thick marine engineering structure plate F550, the effect of preheating and post welding heat treatment on the microstructure and impact toughness of coarse-grained heat-affected zone (CGHAZ) has been investigated. The original microstructure of the steel plate is tempered martensite. The yield and tensile strength is 610 and 660 MPa, respectively. The impact absorbed energy at low temperature (-60 °C) at transverse direction reaches about 230~270 J. Welding results show that the preheating at 100 °C did not have obvious influence on the microstructure and toughness; whereas the tempering at 600 °C for 2.5 h after welding could significantly reduce the amount of M-A components in the coarse-grained heat-affected zone and thus improved the low temperature impact toughness.

scholarly journals Multi-strengthening-mechanisms in a novel titanium alloy with (TiHf)5Si3 particle-reinforcement

2020 ◽  
Vol 321 ◽  
pp. 11078
Author(s):  
Yan Du ◽  
Jinwen Lu ◽  
Wei Zhang ◽  
Yusheng Zhang
Keyword(s):  
Dislocation Motion ◽  
Heat Treatments ◽  
Triple Junctions ◽  
Strengthening Mechanisms ◽  
Particle Reinforcement ◽  
Solid Solution Strengthening ◽  
Long Period ◽  
Solution Strengthening ◽  
Dislocation Strengthening ◽  
Particle Strengthening

The microstructure and mechanical properties of Ti-2Si-2Nb-2Fe-1Hf-1Ta-1W alloy with (TiHf)5Si3 particle-reinforcement and their underlying relations have been studied. Electron microscope observations and correlative statistical analysis have been made to analyze microstructure evolution with heat treatments. The (TiHf)5Si3 particles with 800 nm in diameter were found uniformly distributed at α/β boundaries and triple junctions and turned out to be stable even after heat treatments at high temperature for a long period, inhibiting grain growth and dislocation motion. In addition, multi-strengthening-mechanisms including particle strengthening, solid-solution strengthening, grain boundary strengthening and dislocation strengthening have been discussed.

scholarly journals Quantitative tests revealing hydrogen enhanced dislocation motion in α-iron

2021 ◽  
Author(s):  
Long-Chao Huang ◽  
Dengke Chen ◽  
De-Gang Xie ◽  
Suzhi Li ◽  
Ting Zhu ◽  
...  
Keyword(s):  
Hydrogen Embrittlement ◽  
High Strength Steels ◽  
High Strength ◽  
Dislocation Motion ◽  
Atomistic Simulations ◽  
Vacuum Degassing ◽  
Nucleation Barrier ◽  
Free Behavior ◽  
Individual Dislocation ◽  
Energy Transportation

Abstract Hydrogen embrittlement jeopardizes the use of high-strength steels as critical load-bearing components in energy, transportation, and infrastructure applications. However, our understanding of hydrogen embrittlement mechanism is still obstructed by the uncertain knowledge of how hydrogen affects dislocation motion, due to the lack of quantitative experimental evidence. Here, by studying the well-controlled, cyclic, bow-out movements of individual screw dislocations, the key to plastic deformation in α-iron, we find that the critical stress for initiating dislocation motion in a 2 Pa electron-beam-excited H2 atmosphere is 27~43% lower than that under vacuum conditions, proving that hydrogen lubricates screw dislocation motion. Moreover, we find that aside from vacuum degassing, dislocation motion facilitates the de-trapping of hydrogen, allowing the dislocation to regain its hydrogen-free behavior. Atomistic simulations reveal that the observed hydrogen-enhanced dislocation motion arises from the hydrogen-reduced kink nucleation barrier. These findings at individual dislocation level can help hydrogen embrittlement modelling in steels.

In-Situ TEM Study of Plastic Stress Relaxation Mechanisms and Interface Effects in Metallic Films

2005 ◽  
Vol 875 ◽  
Author(s):  
Marc Legros ◽  
Gerhard Dehm ◽  
T. John Balk
Keyword(s):  
Thin Films ◽  
High Strength ◽  
Dislocation Motion ◽  
Dislocation Nucleation ◽  
Film Stress ◽  
In Situ Tem ◽  
Metallic Films ◽  
Cross Sectional ◽  
Thin Foils

AbstractTo investigate the origin of the high strength of thin films, in-situ cross-sectional TEM deformation experiments have been performed on several metallic films attached to rigid substrates. Thermal cycles, comparable to those performed using laser reflectometry, were applied to thin foils inside the TEM and dislocation motion was recorded dynamically on video. These observations can be directly compared to the current models of dislocation hardening in thin films. As expected, the role of interfaces is crucial, but, depending on their nature, they can attract or repel dislocations. When the film/interface holds off dislocations, experimental values of film stress match those predicted by the Nix-Freund model. In contrast, the attracting case leads to higher stresses that are not explained by this model. Two possible hardening scenarios are explored here. The first one assumes that the dislocation/interface attraction reduces dislocation mobility and thus increases the yield stress of the film. The second one focuses on the lack of dislocation nucleation processes in the case of attracting interfaces, even though a few sources have been observed in-situ.

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