ANALYSIS OF MECHANICAL PROPERTIES AND MICROSTRUCTURE OF NANO-STRUCTURED NI-CO/SIC COMPOSITE PREPARED BY ELECTRODEPOSITION

2012 ◽  
Vol 05 ◽  
pp. 615-621
Author(s):  
S.M. LARI BAGHAL ◽  
M. HEYDARZADEH SOHI ◽  
A. AMADEH
Keyword(s):  
Mechanical Properties ◽  
Tensile Tests ◽  
Nano Composites ◽  
Nano Particle ◽  
X Ray Diffraction ◽  
Nano Composite ◽  
Nano Structure ◽  
X Ray ◽  
Watts Bath ◽  
Average Size

Ni - Co / SiC nano-composites were prepared by electrodeposition in modified watts bath. The average size of SiC particles was 50 nm. In this study the effect of nano-particle incorporation, Co 2+ and saccharin concentration in electroplating bath on morphology and mechanical properties of Ni - Co / SiC nano-composites were investigated. The electrodeposits were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM), Vickers micro-hardness and tensile tests. The results indicate that an increase in Co 2+ and saccharin concentration in electrolyte lead to a decrease in size of SiC agglomerates and grain size refining of matrix and improvement in mechanical properties. The hardness, tensile and yield strengths of the nano-composite material with nano-structure matrixes were higher than those for microcrystalline ones.

Effect of Nitrogen Addition on Mechanical Property of Ti-Cr-Sn Alloy

2010 ◽  
Vol 654-656 ◽  
pp. 2126-2129 ◽  
Author(s):  
Yuichi Nakahira ◽  
Tomonari Inamura ◽  
Hiroyasu Kanetaka ◽  
Shuichi Miyazaki ◽  
Hideki Hosoda
Keyword(s):  
Mechanical Properties ◽  
Room Temperature ◽  
Tensile Tests ◽  
Nitrogen Addition ◽  
N Addition ◽  
X Ray Diffraction ◽  
Solution Hardening ◽  
X Ray ◽  
Bcc Phase ◽  
Cold Workability

Effect of nitrogen (N) addition on mechanical properties of Ti-Cr-Sn alloy was investigated in this study. Ti-7mol%Cr-3mol%Sn was selected and less than 0.5wt% of N were systematically added. The alloys were characterized by optical microscopy, X-ray diffraction analysis and tensile tests at room temperature. The apparent phase was β (bcc) phase, whereas the presence of precipitates was confirmed in 0.5wt%N-added alloy only which did not exhibit sufficient cold workability. The grain size was not largely affected by N addition being less than 0.5wt%. Tensile tests revealed that less than 0.5wt%N addition improves the strength which is due to the solution hardening by interstitial N atoms.

Effects of Extrusion on the Mechanical Properties and Damping Capacity of Mg-1.8Cu-0.5Mn Alloy

2007 ◽  
Vol 546-549 ◽  
pp. 257-260 ◽  
Author(s):  
Zhen Yan Zhang ◽  
Li Ming Peng ◽  
Xiao Qin Zeng ◽  
Lin Du ◽  
Lan Ma ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Tensile Properties ◽  
Room Temperature ◽  
Tensile Tests ◽  
Optical Microscope ◽  
Damping Capacity ◽  
X Ray Diffraction ◽  
Dynamic Mechanical Analyzer ◽  
X Ray ◽  
Solute Atoms

Effects of extrusion on mechanical properties and damping capacity of Mg-1.8wt.%Cu -0.5wt.%Mn (MCM1805) alloy have been investigated. Tensile tests and dynamic mechanical analyzer were respectively used to measure tensile properties and damping capacity at room temperature of as-cast and as-extruded MCM1805 alloy. The microstructure was studied using optical microscope, X-ray diffraction and scanning electron microscope with an energy dispersive X-ray spectrometer. Granato-Lücke model was used to explain the influences of extrusion on damping capacity of MCM1805 alloy. The results showed that extrusion dramatically decreases the grain size but has little influence on phase composition and solute atoms concentration of MCM1805 alloy, and the grain refinement was the dominant reason for the obvious increase of tensile properties and decrease of internal friction of MCM1805 alloy.

Structure and properties of poly(3-hydroxybutyrate-co-3-hydroxyhexanoate)/poly(L-lactic acid) quasi core/sheath melt-electrospun microfibers

2018 ◽  
Vol 89 (9) ◽  
pp. 1770-1781 ◽  
Author(s):  
Huaizhong Xu ◽  
Benedict Bauer ◽  
Masaki Yamamoto ◽  
Hideki Yamane
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Lactic Acid ◽  
Tensile Tests ◽  
Processing Parameters ◽  
Structure And Properties ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Diffraction Patterns

A facile route was proposed to fabricate core–sheath microfibers, and the relationships among processing parameters, crystalline structures and the mechanical properties were investigated. The compression molded poly(3-hydroxybutyrate-co-3-hydroxyhexanoate) (PHBH)/poly(L-lactic acid) (PLLA) strip enhanced the spinnability of PHBH and the mechanical properties of PLLA as well. The core–sheath ratio of the fibers was determined by the prefab strip, while the PLLA sheath component did not completely cover the PHBH core component due to the weak interfacial tension between the melts of PHBH and PLLA. A rotational target was applied to collect aligned fibers, which were further drawn in a water bath. The tensile strength and the modulus of as-spun and drawn fibers increased with increasing the take-up velocities. When the take-up velocity was above 500 m/min, the jet became unstable and started to break up at the tip of the Taylor cone, decreasing the mechanical properties of the fibers. The drawing process facilitated the crystallization of PLLA and PHBH, and the tensile strength and the modulus increased linearly with the increasing the draw ratio. The crystal information displayed from wide-angle X-ray diffraction patterns and differential scanning calorimetry heating curves supported the results of the tensile tests.

Synthesis and Characterization of 3Y-TZP by Gel Solid-State Method

2011 ◽  
Vol 412 ◽  
pp. 61-64
Author(s):  
Xiao Bo Wu ◽  
Da Zhi Sun ◽  
Dan Yu Jiang ◽  
Hai Fang Xu ◽  
De Xin Huang ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Solid State ◽  
Sintering Behavior ◽  
X Ray Diffraction ◽  
Solid State Method ◽  
X Ray ◽  
Powder Particles ◽  
State Method ◽  
Average Size

3Y-TZP powder has been successfully synthesized by gel solid-state method. The structural phases of powder particles were analyzed by X-ray diffraction and the morphology was analyzed by scanning electron microscopy. The average size of grains was 230 nm. The sintering behavior, mechanical properties and microstructure of 3Y-TZP ceramics sintered by this powder were investigated. The experiment results showed that the mechanical properties of ceramics were excellent.

Microstructures and Mechanical Properties of Ti-43Al-5V-4Nb-Y Alloy Consolidated by Spark Plasma Sintering

2016 ◽  
Vol 704 ◽  
pp. 183-189
Author(s):  
Yong Jun Su ◽  
Yi Feng Zheng ◽  
De Liang Zhang ◽  
Fan Tao Kong
Keyword(s):  
Mechanical Properties ◽  
Spark Plasma Sintering ◽  
Tial Alloy ◽  
Tensile Tests ◽  
X Ray Diffraction ◽  
X Ray ◽  
Plasma Sintering ◽  
Short Period ◽  
Spark Plasma ◽  
Fully Lamellar

TiAl alloy with a composition of Ti-43Al-5V-4Nb-Y (at.%) was prepared by spark plasma sintering (SPS). The TiAl powders were sintered between 650°C and 1300°C for 5 min under different loads. With the increasing of the temperature, the diffusion of the elements can be observed. Full compaction is achieved in a short period of time and the overall processing duration does not exceed 30 min. A fully lamellar structure was seen in the TiAl alloy after heat treatment. The microstructures of the samples were determined by X-ray diffraction and scanning electron microscopy. Their mechanical properties were evaluated by tensile tests performed at room temperature

Influence of Temperature of Accumulative Roll Bonding on the Microstructure and Mechanical Properties of AA5251 Aluminum Alloy

2014 ◽  
Vol 59 (1) ◽  
pp. 127-131 ◽  
Author(s):  
J. Bogucka
Keyword(s):  
Mechanical Properties ◽  
Ambient Temperature ◽  
Accumulative Roll Bonding ◽  
Bonding Temperature ◽  
Tensile Tests ◽  
Structure Evolution ◽  
X Ray Diffraction ◽  
Roll Bonding ◽  
X Ray ◽  
Microstructure And Mechanical Properties

Abstract The influence of bonding temperature on microstructure and mechanical properties of AA5251 alloy sheets have been analyzed in the paper. The alloy was deformed with the method of accumulative roll bonding (ARB) in various temperature conditions i.e. at ambient temperature up to 5th cycle (ε = 4.0) and using pre-heating of sheet packs at 200°C and 300°C up to 10 cycles (ε = 8.0). The deformed material was subjected to structural observations using TEM, measurements of crystallographic texture with the technique of X-ray diffraction and tensile tests. It was established that the temperature of roll-bonding had a significant effect on the structure evolution and the observed changes of mechanical properties. High refinement of microstructure and optimum mechanical properties were obtained for the material processed at lower temperatures, i.e. at ambient temperature and pre-heating at 200°C. Recovery structure processes occurring during deformation were observed in the alloy bonded with pre-heating at 300°C and therefore mechanical properties were lower than for the alloy bonded at lower temperatures.

scholarly journals Interfacial premelting of ice in nano composite materials

2019 ◽  
Vol 21 (7) ◽  
pp. 3734-3741 ◽  
Author(s):  
Hailong Li ◽  
Markus Bier ◽  
Julian Mars ◽  
Henning Weiss ◽  
Ann-Christin Dippel ◽  
...  
Keyword(s):  
Experimental Data ◽  
Composite Materials ◽  
Quantitative Description ◽  
High Energy ◽  
Model Systems ◽  
Nano Composites ◽  
X Ray Diffraction ◽  
Nano Composite ◽  
X Ray

We present a quantitative description of ice premelting in permafrost model systems. Experimental data on the interfacial premelting in ice/clay nano composites was obtained by high energy X-ray diffraction.

Research on the Microstructure and Mechanical Properties of Spray-Deposited 8009 Heat Resistant Aluminum Alloy

2014 ◽  
Vol 543-547 ◽  
pp. 3733-3736
Author(s):  
Rong Hua Zhang ◽  
Biao Wu ◽  
Xiao Ping Zheng
Keyword(s):  
Mechanical Properties ◽  
Aluminum Alloy ◽  
Tensile Tests ◽  
Test Results ◽  
Secondary Phases ◽  
X Ray Diffraction ◽  
X Ray ◽  
Heat Resistant ◽  
Microstructure And Mechanical Properties ◽  
Transmission Electron

In this study, 8009 heat resistant aluminum alloy was synthesized by the spray atomization and deposition technique. The microstructure and mechanical properties of the alloy were studied using transmission electron microscopy, X-ray diffraction, and tensile tests. The secondary phases in the microstructure of the spray-deposited alloy were examined. The tensile test results indicate that the spray-deposited 8009 alloy both at room and elevated temperature displays superior tensile strength due to the presence of the thermally stable Al12(Fe,V)3Si particles.

Synthesis and Characterization of TiO2Nanoparticles with Polycarbonate and Investigation of its Mechanical Properties

2017 ◽  
Vol 16 (05n06) ◽  
pp. 1750012 ◽  
Author(s):  
Farhad Jahantigh ◽  
Mehdi Nazirzadeh
Keyword(s):  
Mechanical Properties ◽  
Weight Fraction ◽  
Xrd Analysis ◽  
Tensile Tests ◽  
Nanocomposite Films ◽  
Micro Hardness ◽  
X Ray Diffraction ◽  
X Ray ◽  
Thermal Stability Of

In this project, nanocomposite films were prepared with different Titanium dioxide (TiO2) percentages. Properties of polycarbonate (PC) and PC–TiO2nanocomposite films were studied by X-ray diffraction (XRD) analysis and Fourier transform infrared (FTIR) spectroscopy. The structure of samples was studied by XRD. The mechanical properties of PC–TiO2nanocomposite films were investigated by conducting tensile tests and hardness measurements. Thermal stability of the nanocomposites was studied by thermogravimetric analysis (TGA) method. The elastic modulus of the composite increased with increasing weight fraction of nanoparticles. The microhardness value increases with increasing TiO2nanoparticles. The results of tensile testing were in agreement with those of micro-hardness measurements. In addition, TGA curves showed that nanocomposite films have higher resistance to thermal degradation compared to polycarbonate. There are many reports related to the modification of polycarbonate films, but still a systematic study of them is required.

scholarly journals Microstructural and Mechanical Characterization of a Custom-Built Implant Manufactured in Titanium Alloy by Direct Metal Laser Sintering

2014 ◽  
Vol 6 ◽  
pp. 945819 ◽  
Author(s):  
Maria Aparecida Larosa ◽  
André Luiz Jardini ◽  
Cecília Amélia de Carvalho Zavaglia ◽  
Paulo Kharmandayan ◽  
Davi Reis Calderoni ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Tensile Tests ◽  
Laser Sintering ◽  
Direct Metal Laser Sintering ◽  
X Ray Diffraction ◽  
Medical Field ◽  
X Ray ◽  
Craniomaxillofacial Surgery ◽  
The One

Custom-built implants manufacture has always presented difficulties which result in high cost and complex fabrication, mainly due to patients’ anatomical differences. The solution has been to produce prostheses with different sizes and use the one that best suits each patient. Additive manufacturing technology, incorporated into the medical field in the late 80's, has made it possible to obtain solid biomodels facilitating surgical procedures and reducing risks. Furthermore, this technology has been used to produce implants especially designed for a particular patient, with sizes, shapes, and mechanical properties optimized, for different areas of medicine such as craniomaxillofacial surgery. In this work, the microstructural and mechanical properties of Ti6Al4V samples produced by direct metal laser sintering (DMLS) are studied. The microstructural and mechanical characterizations have been made by optical and scanning electron microscopy, X-ray diffraction, and microhardness and tensile tests. Samples produced by DMLS have a microstructure constituted by hexagonal α′ martensite with acicular morphology. An average microhardness of 370 HV was obtained and the tensile tests showed ultimate strength of 1172 MPa, yield strength of 957 MPa, and elongation at rupture of 11%.

Sign in / Sign up

Export Citation Format

Share Document