On the Primary X-Ray Analyzer

1965 ◽  
Vol 9 ◽  
pp. 508-514 ◽  
Author(s):  
Shizuo Kimoto ◽  
Masayuki Sato ◽  
Hitoshi Kamada ◽  
Takuzi Ui

AbstractThe primary X-ray analyzer is used for nondestructive spectrochemical analysis of solid specimens. Accelerated electron beams bombard the specimen surface directly and generate primary X-rays which are measured in a vacuum spectrometer. The method of primary X-ray spectroscopy is superior to the fluorescence X-ray spectroscopy because (1) detectable sensitivity for such light elements as magnesium and aluminum is very high, and (2) the correction of the measured value for self-absorption of X-rays by the specimen itself is low. The performance of the instrument and applications are reported.

1984 ◽  
Vol 28 ◽  
pp. 137-144 ◽  
Author(s):  
Tomoya Arai ◽  
Takashi Shoji ◽  
Richard W. Ryon

Spectrographic analysis of light elements by soft and ultrasoft fluorescent x-rays has become a useful technique for many applications of elemental analysis, using single crystals, soap multilayers and a combination of total reflection and filtering.Instead of the wavelength dispersive method based on Bragg reflection which provides high resolution combined with low reflecting intensity, monochromatization combining total reflection by a selected mirror and an appropriate filter offered an alternative approach in order to increase measurable intensity with reasonable spectral resolution.Recently, the use of synthetic multilayers, which are prepared by sputter/evaporation techniques, has been introduced for the detection of soft and ultrasoft x-rays. Studies on the use of these new wavelength dispersing devices have been conducted and it has been found that the reflectivity of these devices is very high compared with single crystals and soap multilayers and that their resolving power is fairly good.


1991 ◽  
Vol 01 (03) ◽  
pp. 251-258 ◽  
Author(s):  
M. TERASAWA

K, L, and M X-rays in the wavelengths between 6Å and 130Å generated by the bombardment of 200 keV protons and other heavy ions were measured by means of a wavelength dispersive Bragg’s spectrometer. The X-ray peak intensity was fairly high in general, while the background was very low. The technique was favorably applied to a practical analysis of several light elements (Be, B, C, N, O, and F). Use of moderate-energy heavy ions considering the wavelength selectivity in X-ray generation was effective for the element analysis. The high-resolution spectrometry in the analytical application of ion-induced X-ray generation was found to be useful for the study of fine electronic structure, e.g. satellite and hypersatellite X-ray study, and of the chemical state of materials.


Proceedings ◽  
2019 ◽  
Vol 17 (1) ◽  
pp. 9
Author(s):  
Ka-Wah Wong ◽  
Rodrigo S. Nemmen ◽  
Jimmy A. Irwin ◽  
Dacheng Lin

The nearby M87 hosts an exceptional relativistic jet. It has been regularly monitored in radio to TeV bands, but little has been done in hard X-rays ≳10 keV. For the first time, we have successfully detected hard X-rays up to 40 keV from its X-ray core with joint Chandra and NuSTAR observations, providing important insights to the X-ray origins: from the unresolved jet or the accretion flow. We found that the hard X-ray emission is significantly lower than that predicted by synchrotron self-Compton models introduced to explain very-high-energy γ -ray emission above a GeV. We discuss recent models to understand these high energy emission processes.


1986 ◽  
Vol 30 ◽  
pp. 213-223
Author(s):  
Tomoya Arai

The development of X-ray spectrographic analysis of light elements, which are O, C and B, has bee n performed for many applications using an end-window type X-ray tube with Rh-target and thin Be-window, wavelength dispersing devices, which are synthetic multilayers or total reflection mirror (with a specific filter) and a gas flow proportional counter with a thin film window. In Fig. 1 factors related to the intensity measurements in X-ray fluorescence analysis are shown. The excitation efficiency in the soft and ultrasoft X-ray region is very low because of the lower intensity of primary X-rays and low fluorescence yield of light elements. Instead of the wavelength dispersive method of Bragg reflection, having high resolution and low reflectivity, monochromatization combining total reflection by a selected mirror and an appropriate filter offered an alternate approach in order to increase measured intensity with reasonable optical resolution. Synthetic multilayers which have higher resolution and lower intensity compared with the performance of the mirror method have become popular for the detection of soft and ultrasoft X-ray region.


2021 ◽  
Vol 11 (22) ◽  
pp. 10768
Author(s):  
Ye Chen ◽  
Frank Brinker ◽  
Winfried Decking ◽  
Matthias Scholz ◽  
Lutz Winkelmann

Sub-ångström working regime refers to a working state of free-electron lasers which allows the generation of hard X-rays at a photon wavelength of 1 ångström and below, that is, a photon energy of 12.5 keV and above. It is demonstrated that the accelerators of the European X-ray Free-Electron Laser can provide highly energetic electron beams of up to 17.5 GeV. Along with long variable-gap undulators, the facility offers superior conditions for exploring self-amplified spontaneous emission (SASE) in the sub-ångström regime. However, the overall FEL performance relies quantitatively on achievable electron beam qualities through a kilometers-long accelerator beamline. Low-emittance electron beam production and the associated start-to-end beam physics thus becomes a prerequisite to dig in the potentials of SASE performance towards higher photon energies. In this article, we present the obtained results on electron beam qualities produced with different accelerating gradients of 40 MV/m–56 MV/m at the cathode, as well as the final beam qualities in front of the undulators via start-to-end simulations considering realistic conditions. SASE studies in the sub-ångström regime, using optimized electron beams, are carried out at varied energy levels according to the present state of the facility, that is, a pulsed mode operating with a 10 Hz-repetition 0.65 ms-long bunch train energized to 14 GeV and 17.5 GeV. Millijoule-level SASE intensity is obtained at a photon energy of 25 keV at 14 GeV electron beam energy using a gain length of about 7 m. At 17.5 GeV, half-millijoule lasing is achieved at 40 keV. Lasing at up to 50 keV is demonstrated with pulse energies in the range of a few hundreds and tens of microjoules with existing undulators and currently achievable electron beam qualities.


Nukleonika ◽  
2016 ◽  
Vol 61 (2) ◽  
pp. 161-167 ◽  
Author(s):  
Władysław Surała ◽  
Marek J. Sadowski ◽  
Roch Kwiatkowski ◽  
Lech Jakubowski ◽  
Jarosław Żebrowski

Abstract The paper reports results of the recent experimental studies of pulsed electron beams and soft X-rays in plasma-focus (PF) experiments carried out within a modified PF-360U facility at the NCBJ, Poland. Particular attention was focused on time-resolved measurements of the fast electron beams by means of two different magnetic analyzers, which could record electrons of energy ranging from about 41 keV to about 715 keV in several (6 or 8) measuring channels. For discharges performed with the pure deuterium filling, many strong electron signals were recorded in all the measuring channels. Those signals were well correlated with the first hard X-ray pulse detected by an external scintillation neutron-counter. In some of the analyzer channels, electron spikes (lasting about dozens of nanoseconds) and appearing in different instants after the current peculiarity (so-called current dip) were also recorded. For several discharges, fast ion beams, which were emitted along the z-axis and recorded with nuclear track detectors, were also investigated. Those measurements confirmed a multibeam character of the ion emission. The time-integrated soft X-ray images, which were taken side-on by means of a pinhole camera and sensitive X-ray films, showed the appearance of some filamentary structures and so-called hot spots. The application of small amounts of admixtures of different heavy noble gases, i.e. of argon (4.8% volumetric), krypton (1.6% volumetric), or xenon (0.8% volumetric), decreased intensity of the recorded electron beams, but increased intensity of the soft X-ray emission and showed more distinct and numerous hot spots. The recorded electron spikes have been explained as signals produced by quasi-mono-energetic microbeams emitted from tiny sources (probably plasma diodes), which can be formed near the observed hot spots.


In an attempt to fill up the gap between the shortest ultra-violet light waves hitherto produced and the longest X-ray waves known, Hughes recently made a study of the characteristic X-rays emitted by carbon and by boron when bombarded by electrons. In this investigation the energy of the bombarding electrons was increased by steps, and the critical values were determined that were necessary and just sufficient to cause the bombarded element to emit its characteristic radiations with measurable intensities. These characteristic radiations were detected, and their intensities measured, by their photo-electric action on an insulated electrode of nickel or of silver. The method followed by Hughes in recording his results was to plot curves with the values of the accelerating potentials of the electrons as abscissæ and the measures of the photo-electric effect divided by the corresponding electronic currents as ordinates. At certain critical accelerating voltages it was found that these curves showed marked and abrupt kinks or changes of curvature, and these changes were taken to connote the beginning of the emission by the bombarded element of its characteristic radiations.


2021 ◽  
Vol 28 (5) ◽  
Author(s):  
Hsiang Hsin Chen ◽  
Shun-Min Yang ◽  
Kai-En Yang ◽  
Ching-Yu Chiu ◽  
Chia-Ju Chang ◽  
...  

The new Brain Imaging Beamline (BIB) of the Taiwan Photon Source (TPS) has been commissioned and opened to users. The BIB and in particular its endstation are designed to take advantage of bright unmonochromatized synchrotron X-rays and target fast 3D imaging, ∼1 ms exposure time plus very high ∼0.3 µm spatial resolution. A critical step in achieving the planned performances was the solution to the X-ray induced damaging problems of the detection system. High-energy photons were identified as their principal cause and were solved by combining tailored filters/attenuators and a high-energy cut-off mirror. This enabled the tomography acquisition throughput to reach >1 mm3 min−1, a critical performance for large-animal brain mapping and a vital mission of the beamline.


1981 ◽  
Vol 25 ◽  
pp. 45-48
Author(s):  
M. A. Short ◽  
T. G. Gleason

Two recent improvements in energy dispersive spectrometry are the development of time variant amplifiers and the introduction of pulsed X-ray sources. Either pulsed X-ray tubes or electron beams with fast beam blanking may be used.Time variant amplifiers designed by Kandiah (1 ,2) used control logic to co-ordinate charge restoration of the detector preamplifier, pole-zero cancellation and baseline restoration. In the pulse shaping circuit, time constants are switched during the processing of each pulse to optimize throughput, baseline stability and pileup rejection. Pulse processing techniques have been discussed by Statham (3) .


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