scholarly journals Effect of Fiber Laser Irradiation on the Shear Bond Strength between Acrylic Resin and Titanium

Scanning ◽  
2019 ◽  
Vol 2019 ◽  
pp. 1-11
Author(s):  
Fatih Mehmet Korkmaz ◽  
Selin Aycan

Objectives. The aim of this study is to investigate the shear bond strength of an acrylic resin to titanium after different surface treatment methods. Material and Methods. A total of seventy-two disc-shaped specimens (10 mm×10 mm×2 mm) were prepared from titanium alloy. The specimens were randomly allocated to six equal groups: Group S (sandblasting), Group MP (metal primer), Group 10W (fiber laser 10 W), Group 20W (fiber laser 20 W), Group 10WMP (fiber laser 10 W+metal primer), and Group 20WMP (fiber laser 20 W+metal primer). All of the specimens were thermocycled up to 5000 cycles. After thermal cycling, a shear bond strength test was conducted. The shear bond strength data were analyzed with one-way ANOVA and Tukey’s post hoc pairwise comparisons (p<0.05). Results. While the highest values were determined in Group MP, the lowest values were observed in Group S. Additionally, Group MP exhibited significantly higher shear bond strength values than any of the other groups (p<0.05) except Group 10WMP. Similar results were observed between Group MP and Group 10WMP (p>0.05). The groups in which a metal primer was applied (Group MP, 10WMP, and 20WMP) showed significantly higher values than Group S. The shear bond strength values of Group 10W and Group 20W were similar. Conclusions. The application of a metal primer significantly improved the bond strength of acrylic resin to titanium. Fiber laser application may be an alternative method to sandblasting for improving the bond strength of acrylic resin to titanium.

2012 ◽  
Vol 2012 ◽  
pp. 1-9 ◽  
Author(s):  
Vajihesadat Mortazavi ◽  
Mohammadhosein Fathi ◽  
Ebrahim Ataei ◽  
Niloufar Khodaeian ◽  
Navid Askari

In this laboratory study shear bond strengths of three filled and one unfilled adhesive systems to enamel and dentine were compared. Forty-eight extracted intact noncarious human mandibular molars were randomly assigned to two groups of 24 one for bonding to enamel and the other for bonding to dentine. Buccal and lingual surfaces of each tooth were randomly assigned for application of each one of filled (Prime & Bond NT (PBNT), Optibond Solo Plus (OBSP), and Clearfil SE Bond (CSEB)) and unfilled (Single Bond (SB)) adhesive systems (n=12). A universal resin composite was placed into the translucent plastic cylinders (3 mm in diameter and 2 mm in length) and seated against the enamel and dentine surfaces and polymerized for 40 seconds. Shear bond strength was determined using a universal testing machine, and the results were statistically analyzed using two-way ANOVA, one-way ANOVA,t-test, and Tukey HSD post hoc test with a 5% level of significance.There were no statistically significant differences in bond strength between the adhesive systems in enamel, but CSEB and SB exhibited significantly higher and lower bond strength to dentine, respectively, than the other tested adhesive systems while there were no statistically significant differences between PBNT and OBSP.


2011 ◽  
Vol 36 (5) ◽  
pp. 492-501 ◽  
Author(s):  
B Stawarczyk ◽  
R Hartmann ◽  
L Hartmann ◽  
M Roos ◽  
M Özcan ◽  
...  

SUMMARY This study tested the impact of Gluma Desensitizer on the shear bond strength (SBS) of two conventional (RelyX ARC, Panavia 21) and two self-adhesive (RelyX Unicem, G-Cem) resin luting cements after water storage and thermocycling. Human third molars (N=880) were embedded in acrylic resin. The buccal dentin was exposed. Teeth were randomly divided into four main groups, and the following cements were adhered: 1) RelyX ARC, 2) Panavia 21, 3) RelyX Unicem, and 4) G-Cem. In half of the teeth in each group, dentin was treated with Gluma Desensitizer. In the conventional cement groups, the corresponding etchant and adhesive systems were applied. SBS of the cements was tested after 1 hour (initial); at 1, 4, 9, 16, and 25 days of water storage; and at 1, 4, 9, 16, and 25 days of thermocycling. SBS data were analyzed by one-way analysis of variance (ANOVA); this was followed by the post hoc Scheffé test and a t-test. Overall, the highest mean SBS (MPa) was obtained by RelyX ARC (ranging from 14.6 ± 3.9 to 17.6 ± 5.2) and the lowest by Panavia 21 in combination with Gluma Desensitizer (ranging from 0.0 to 2.9 ± 1.0). All tested groups with and without desensitizer showed no significant decrease after aging conditions compared with baseline values (p&gt;0.05). Only the Panavia 21/Gluma Desensitizer combination showed a significant decrease after 4 days of thermocyling compared with initial values and 1 day thermocycling. Self-adhesive cements with Gluma Desensitizer showed increased SBS after aging conditions (ranging from 7.4 ± 1.4 to 15.2 ± 3) compared with groups without desensitizer (ranging from 2.6 ± 1.2 to 8.8 ± 2.9). No cohesive failures in dentin were observed in any of the test groups. Although self-adhesive cements with and without desensitizer presented mainly adhesive failures after water storage (95.8%) and thermocyling (100%), conventional cement (RelyX ARC) showed mainly mixed failures (90.8% and 89.2%, after water storage and thermocyling, respectively). Application of the Gluma Desensitizer to dentin before cementation had a positive effect on the SBS of self-adhesive cements.


2016 ◽  
Vol 18 (2) ◽  
pp. 109
Author(s):  
M.T. Muñoz MSc ◽  
E. Reales DDS ◽  
L.H.M. Prates DDS, MSc, PhD ◽  
C.A.M. Volpato DDS, MSc, PhD

The aim of this study was to compare the shear bond strength between acrylic resin teeth and autopolymerizing acrylic resin repairs after different surface treatments. Seventy-two upper anterior acrylic resin denture teeth (MFT, Vita, Germany) were selected. Specimens were randomly assigned into six groups (n=12): G1-C, without surface treatment (control); G2-M, methylmetacrylate monomer (Jet, Clássico, Brazil) application; G3-A treatment with methylmetacrylate and metiletilcetone-based bonding agent (Vitacoll, Vita, Germany). The surface of G4-OA, G5-OAM and G6-OAA was airborne-particle abraded with aluminum oxide (Polidental, Wilson, Brazil); being repeated the treatments respectively of groups G1-C, G2-M e G3-A. All groups were then repaired with autopolymerizing acrylic resin (Jet, Clássico, Brazil). Shear bond strength test was performed using an universal testing machine (Instron 4444). Two-way ANOVA and post hoc Tukey’s analysis (p<0,05) were used for statistical comparison. The shear bond strengths of groups G4-OA, G5-OAM and G6-OAA were significantly higher (p<0,05) than that of groups G1-C, G2-M and G3-A. The shear bond strength of Group G3-A were significantly higher (p<0,05) than that of groups G1-C and G2-M. In conclution, chemical treatments in combination with bondig agents showed significant improvements in bond strength without aluminum oxide treatment. More significantly, surface treatment with aluminum oxide particles resulted in the highest bond strength values for acrylic resin teeth repaired with autopolymerizing acrylic resin. 


2017 ◽  
Vol 16 ◽  
pp. 1-7
Author(s):  
Bruna Lorena dos Santos Oliveira ◽  
Ana Rosa Costa ◽  
Américo Bortolazzo Correr ◽  
Marcus Vinicius Crepaldi ◽  
Lourenço Correr-Sobrinho ◽  
...  

Aim: To evaluate, in vitro, the effect of adhesive and bonding materials on the shear bond strength (SBS) of metallic brackets bonded to bovine teeth. Methods: Bovine teeth were embedded with acrylic resin, etched with 35% phosphoric acid for 20 s, rinsed, dried for 20 s and divided into 8 groups (n=20), according to the bonding materials and adhesive: Groups 1 and 5 – Transbond XT; Groups 2 and 6 – Fill Magic; Groups 3 and 7 – Biofix; and, Groups 4 and 8 – Orthocem. One layer of adhesive 3 M Unitek (Group 1), and one layer of Single Bond Universal Adhesive (Groups 2, 3 and 4) were applied and light-cured with LED for 10 s. Brackets were bonded to the buccal surface with four bonding materials and light-cured with LED for 40 s. SBS was carried out after 24 h and thermocycling (7,000 cycles - 5°/55 °C). Data were submitted to two way ANOVA and Tukey’s post hoc test (α=0.05). The Adhesive Remaining Index (ARI) was evaluated at 8×. Results: The adhesive was effective in increasing the SBS for all bonding materials (p<0.05). Significant difference (p<0.05) on the SBS was observed between bonding materials with or without adhesive. The ARI showed a predominance of scores 0 for all groups. Conclusions: The adhesive improved significantly the SBS of the brackets to teeth. Different SBS values occurred among the bonding materials. ARI index showed predominance of score 0 for all groups.


Author(s):  
Fatma Ayse Sanal DDS, PhD ◽  
Derya Guler DDS, PhD

Purpose: The purpose of the present research was to evaluate the effectiveness of self-adhesive composites in amalgam repair as time-saving alternatives to universal bonding-universal composite materials, with or without the usage of Alloy Primer in terms of shear bond strength. Materials and Methods: Forty-two disc-shaped amalgam samples were prepared by condensing into 6×2 mm holes in acrylic resin blocks, sandblasted with 50 μm Al2O3 and randomly divided into 6 groups according to repair material [Constic (Group C), Fusio Liquid Dentin (Group FLD), Universal bonding+Universal composite (Group Control), Alloy Primer+Constic (Group APC), Alloy Primer+Fusio Liquid Dentin (Group APFLD), Alloy Primer+Universal bonding+Universal composite (Group APControl)]. After shear bond strength test, the fracture modes were determined under a digital microscope. Statistical analysis was performed using one-way analysis of variance and Tukey's post hoc test. Results: The highest shear bond strength values were obtained for Fusio Liquid Dentin, among the three repair materials when Alloy Primer was not applied (p<0.05). Usage of Alloy Primer increased shear bond strength values of the investigated repair materials to amalgam, except Fusio Liquid Dentin. Conclusion: Within the limitations of the present research, it can be concluded that; the investigated self-adhesive composite materials could be time-saving alternatives to the Universal bonding+Universal composite for the purpose of amalgam repair, in terms of shear bond strength. The clinicians could prefer Fusio Liquid Dentin self-adhesive composite material without Alloy Primer application for the purpose of amalgam repair in non-cooperative patients.


2011 ◽  
Vol 36 (5) ◽  
pp. 478-485 ◽  
Author(s):  
R Brum ◽  
R Mazur ◽  
J Almeida ◽  
G Borges ◽  
D Caldas

SUMMARY In vitro studies to assess bond strength between resins and ceramics have used surfaces that have been ground flat to ensure standardization; however, in patients, ceramic surfaces are irregular. The effect of a polished and unpolished ceramic on bond strength needs to be investigated. Sixty ceramic specimens (20×5×2 mm) were made and divided into two groups. One group was ground with 220- to 2000-grit wet silicon carbide paper and polished with 3-, 1-, and ¼-μm diamond paste; the other group was neither ground nor polished. Each group was divided into three subgroups: treated polished controls (PC) and untreated unpolished controls (UPC), polished (PE) and unpolished specimens (UPE) etched with hydrofluoric acid, and polished (PS) and unpolished specimens (UPS) sandblasted with alumina. Resin cement cylinders were built over each specimen. Shear bond strength was measured, and the fractured site was analyzed. Analysis of variance (ANOVA) and Tukey post hoc tests were performed. PE (44.47 ± 5.91 MPa) and UPE (39.70 ± 5.46 MPa) had the highest mean bond strength. PS (31.05 ± 8.81 MPa), UPC (29.11 ± 8.11 MPa), and UPS (26.41 ± 7.31 MPa) were statistically similar, and PC (24.96 ± 8.17 MPa) was the lowest. Hydrofluoric acid provides the highest bond strength regardless of whether the surface is polished or not.


2006 ◽  
Vol 17 (1) ◽  
pp. 39-43 ◽  
Author(s):  
Guilherme Carpena Lopes ◽  
Paula C. Cardoso ◽  
Luiz Clovis Cardoso Vieira ◽  
Luiz N. Baratieri ◽  
Karina Rampinelli ◽  
...  

The aim of this study was to assess the shear bond strength of four acetone-based one-bottle adhesive systems to enamel and dentin, and compare to that of an ethanol-based system used as control. Fifty human molars were bisected mesiodistally and the buccal and lingual surfaces were embedded in acrylic resin using PVC cylinders. The buccal surfaces were ground to obtain flat dentin surfaces, while the lingual surfaces were ground to obtain flat enamel surfaces. All specimens were polished up to 600-grit sandpapers and randomly assigned to 5 groups (n=20; 10 dentin specimens and 10 enamel specimens), according to the adhesive system used: One-Step (Bisco); Gluma One Bond (Heraeus Kulzer); Solobond M (Voco); TenureQuik w/F (Den-Mat) and OptiBond Solo Plus (Kerr) (control). Each adhesive system was applied according to the manufacturers' instructions. The respective proprietary hybrid composite was applied in a gelatin capsule (d=4.3mm) and light-cured for 40 s. The specimens were tested in shear strength with an Instron machine at a crosshead speed of 5 mm/min. Bond strengths means were analyzed statistically by one-way ANOVA and Duncan's post-hoc (p£0.05). Shear bond strength means (MPa) (±SD) to enamel and dentin were: Enamel: One-Step=11.3(±4.9); Gluma One Bond=16.3(±10.1); Solobond M=18.9(±4.5); TenureQuik w/F=18.7(±4.5) and OptiBond Solo Plus=16.4(±3.9); Dentin: One-Step=6.4(±2.8); Gluma One Bond=3.0(±3.4); Solobond M=10.6(±4.9); TenureQuik w/F=7.8(±3.9) and OptiBond Solo Plus=15.1(±8.9). In enamel, the adhesive systems had statistically similar bond strengths to each other (p>0.05). However, the ethanol-based system (OptiBond Solo Plus) showed significantly higher bond strength to dentin than the acetone-based systems (p£0.0001). In conclusion, the solvent type (acetone or ethanol) had no influence on enamel bond strength, but had great influence on dentin bonding, which should be taken into account when choosing the adhesive system.


2021 ◽  
Vol 10 (16) ◽  
pp. e195101623481
Author(s):  
Tainah Oliveira Rifane ◽  
Ítalo Hudson Tavares Maia ◽  
Andressa Silva de Oliveira ◽  
Ranyele Elis Alexandre Rodrigues ◽  
Francisbênia Alves Silvestre ◽  
...  

To evaluate the shear bond strength and the fracture type of orthodontic tubes bonded directly with composite resin throughout the enamel surface. 30 bovine teeth were cut into 3 slices with 5 mm each and embedded in PVC pipes with acrylic resin exposing the buccal face. Subsequently, the teeth were submitted to conventional bonding techniques. Natural Ortho resin was applied for direct bonding of Edgewise Standard orthodontic tubes (Morelli®) and light-cured for 20s. A different viscosity resin was chosen and light-cured for 40s to reinforce the tube surface. The samples were divided into the following groups: Orthodontic tube with direct bonding without reinforcement (CONTROL), Tube with Natural Ortho resin + Reinforcement (NO + NO), Tube with Natural Ortho resin + Reinforcement with Flow resin (NO + FL). These were submitted to shear bond strength; immediate and 1-year aging fracture analysis after simulated through thermocycling. In the shear bond strength test, the group of orthodontic tubes that were directly bonded with Natural Ortho resin and reinforced (NO + NO) showed greater strength results after 24 hours and 1 year with values of (p=0.0225) and (p=0.0273). It was statistically differentto the NO + FL and CONTROL reinforced groups. In the fracture analysis, the NO +NO group was classified immediately as composite cohesive, and mixed failure after aging by thermocycling. The addition of a composite resin layer on the surface of the directly bonded orthodontic tube improved bond strength. The reinforcement must be carried out in regular consistency and the use of Flow resin is not indicated.


2013 ◽  
Vol 24 (5) ◽  
pp. 513-516 ◽  
Author(s):  
Américo Bortolazzo Correr ◽  
Ana Rosa Costa ◽  
Adriana Simoni Lucato ◽  
Silvia Amélia Vedovello ◽  
Heloísa Cristina Valdrighi ◽  
...  

The aim of this study was to evaluate the shear bond strength (SBS) of metallic orthodontic brackets bonded to bovine teeth using light-activated or chemically activated composite resins. One hundred and twenty bovine mandibular incisors were divided into 6 groups (n=20), according to the bonding materials: Transbond XT (T); Enforce Dual (ED); Enforce chemical (EC); Enforce Light-activated (EL); Concise Orthodontic (C); and RelyX Unicem Capsule (UN). Metallic brackets were positioned and firmly bonded to the teeth. Light-activation for T, ED, EL and UN was carried out with four exposures on each side of the bracket with 20 s total exposure times using XL2500 (3M ESPE). EC and C were chemically cured. Next, all specimens were stored in deionized water at 37 °C for 24 h. The shear bond strength was carried out at a crosshead speed of 1.0 mm/min. Data were subjected to one-way ANOVA and Tukey's test (α=0.05). The adhesive remnant index (ARI) was evaluated at 8× magnification. C (17.72±4.45) presented significantly higher SBS means (in MPa) than the other groups (p<0.05), followed by EC (11.97±5.77) and ED (10.57±1.32). EL (5.39±1.06) and UN (4.32±1.98) showed the lowest SBS means, while T (9.09±2.56) showed intermediate values. For ARI, there was a predominance of score 0 for EC, C and UN, and score 3 for T, ED and EL. In conclusion, the activation mode influenced the SBS.


2016 ◽  
Vol 64 (2) ◽  
pp. 140-147
Author(s):  
Gilvan Cutrim TAVARES ◽  
Renan Macedo Cutrim TAVARES ◽  
Milton Edson MIRANDA ◽  
Cecilia Pedroso TURSSI ◽  
Roberta Tarkany BASTING ◽  
...  

ABSTRACT Objective This study evaluated the shear bond strength (SBS) of lithium disilicate glass (LDG) ceramic bonded to a zirconia (Y-TZP), using different cementation strategies. Methods LDG ceramic cylinders were cemented to Y-TZP structure according to the following adhesive system (AS)/resin cement (RC) (n = 15): U- self-adhesive dual-cure RC; AMBAR- AS containing phosphate monomers (PM) + dual-cure RC; group SBU: PM+Silane/AS + light-cure RC; group ALLB: PM/AS + dual-cure RC. Specimens were subjected to SBS in a universal testing machine (0.5 mm/min). Data (MPa) were subjected to one-way ANOVA and Tukey's test (α = 0,05). Results The groups SBU and ALLB had significantly higher SBS than those provided by the group U, in which the lowest values were observed. For the AMBAR group, intermediate SBS values were found, which did not differ significantly from the values observed in the other groups. Conclusion Regardless of resins cement, the use of adhesives containing phosphate monomers provided superior bond strength than self-adhesive cement.


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