scholarly journals Doping Effect of Lead(II) on Structural and Optical Properties of Chromium Oxide Nanoparticles

2020 ◽  
Vol 32 (12) ◽  
pp. 3002-3006
Author(s):  
N. Kalaiselvi ◽  
K.U. Madhu
Keyword(s):  
Optical Properties ◽  
Chromium Oxide ◽  
Morphological Properties ◽  
Oxide Nanoparticles ◽  
X Ray Diffraction ◽  
Structural And Optical Properties ◽  
X Ray ◽  
Prepared Nanoparticles ◽  
Chromium Oxide Nanoparticles ◽  
Pure Chromium

In this work, the effects of doping post transition metal (Pb2+) on the structural, morphological, elemental and optical properties of pure chromium oxide nanoparticles are reported. The structural and morphological properties were examined by X-ray diffraction and scanning electron microscopy (SEM). The elemental composition of the prepared nanoparticles were estimated from energy dispersive X-ray (EDX) absorption spectra. The band gap energies of the prepared nanoparticles (4.72-3.78 eV) obtained from UV-vis absorption spectroscopy is higher than that of bulk Cr2O3 (3.3 eV), which ensures that the prepared nanoparticles were successfully synthesized in the nano-region.

Structural and optical properties of Tin Oxide and Indium doped SnO2 thin films deposited by thermal evaporation technique

2016 ◽  
Vol 12 (3) ◽  
pp. 4394-4399
Author(s):  
Sura Ali Noaman ◽  
Rashid Owaid Kadhim ◽  
Saleem Azara Hussain
Keyword(s):  
Thin Films ◽  
Optical Properties ◽  
Tin Oxide ◽  
Thermal Evaporation ◽  
Pure Sno2 ◽  
X Ray Diffraction ◽  
Structural And Optical Properties ◽  
X Ray ◽  
Evaporation Technique ◽  
Sno2 Thin Films

Tin Oxide and Indium doped Tin Oxide (SnO2:In) thin films were deposited on glass and Silicon  substrates  by  thermal evaporation technique.  X-ray diffraction pattern of  pure SnO2 and SnO2:In thin films annealed at 650oC and the results showed  that the structure have tetragonal phase with preferred orientation in (110) plane. AFM studies showed an inhibition of grain growth with increase in indium concentration. SEM studies of pure  SnO2 and  Indium doped tin oxide (SnO2:In) ) thin films showed that the films with regular distribution of particles and they have spherical shape.  Optical properties such as  Transmission , optical band-gap have been measured and calculated.

scholarly journals Structural and optical properties of SnO2–Al2O3 nanocomposite synthesized via sol-gel route

2015 ◽  
Vol 33 (4) ◽  
pp. 714-718 ◽  
Author(s):  
Neeraj K. Mishra ◽  
Chaitnaya Kumar ◽  
Amit Kumar ◽  
Manish Kumar ◽  
Pratibha Chaudhary ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Optical Properties ◽  
Sol Gel ◽  
Physical Interaction ◽  
X Ray Diffraction ◽  
Structural And Optical Properties ◽  
X Ray ◽  
Sensing Applications ◽  
Scanning Electron

AbstractA nanocomposite of 0.5SnO2–0.5Al2O3 has been synthesized using a sol-gel route. Structural and optical properties of the nanocomposite have been discussed in detail. Powder X-ray diffraction and scanning electron microscopy with energy-dispersive X-ray diffraction spectroscopy confirm the phase purity and the particle size of the 0.5SnO2–0.5Al2O3 nanocomposite (13 to 15 nm). The scanning electron microscopy also confirms the porosity in the sample, useful in sensing applications. The FT-IR analysis confirms the presence of physical interaction between SnO2 and Al2O3 due to the slight shifting and broadening of characteristic bands. The UV-Vis analysis confirms the semiconducting nature because of direct transition of electrons into the 0.5SnO2–0.5Al2O3 nanocomposites.

Structural and Optical Properties of Al Co-Doped ZnCoO Thin Film

2014 ◽  
Vol 989-994 ◽  
pp. 656-659
Author(s):  
Ping Cao ◽  
Yue Bai
Keyword(s):  
Thin Film ◽  
Optical Properties ◽  
Sol Gel ◽  
X Ray Diffraction ◽  
Structural And Optical Properties ◽  
Al Doping ◽  
X Ray ◽  
Uv Emission ◽  
Uv Absorption Spectroscopy ◽  
Co Doped

Al co-doped ZnCoO thin film has been prepared by a sol-gel method. The structural and optical properties of the sample were investigated. X-ray diffraction and UV absorption spectroscopy analyses indicate that Al3+ and Co2+ substitute for Zn2+ without changing the wurtzite structure. With the Al doping, the visible emission increased and the UV emission decreased, which is attributed to the increase of O vacancies and Zn interstitials.

scholarly journals Laser induced plasma of cadmium oxide: structural, morphological and optical properties

2021 ◽  
Vol 2114 (1) ◽  
pp. 012012
Author(s):  
Tamara S. Hussein ◽  
Ala F. Ahmed
Keyword(s):  
Optical Properties ◽  
Energy Gap ◽  
Cadmium Oxide ◽  
X Ray Diffraction ◽  
Structural And Optical Properties ◽  
Optical Energy Gap ◽  
X Ray ◽  
Laser Induced Plasma ◽  
Atomic Force ◽  
Doping Ratio

Abstract In this study, the effect of grafting with Iron (Fe) ratios (0.1, 0.3 and 0.5) on the structural and optical properties of cadmium oxide films (CdO) was studied, as these films were prepared on glass bases using the method of pulse laser deposition (PLD). The crystallization nature of the prepared films was examined by X-ray diffraction technique (XRD), which showed that the synthesis of the prepared films is polycrystalline, and Atomic Force Microscope (AFM) images also showed that the increased vaccination with Iron led to an increase in the crustal size ratio and a decrease in surface roughness, The absorption coefficient was calculated and the optical energy gap for the prepared thin films. It was found the absorption decreases and the energy gap decreases with the increase of doping ratio.

scholarly journals Influence of Different Annealing Temperatures on the Structural and Optical Properties of TiO2 Nanoparticles Synthesized via Sol-Gel Method: Potential Application as UV Sensor

2021 ◽  
Vol 21 (2) ◽  
pp. 279
Author(s):  
Nur Munirah Safiay ◽  
Rozina Abdul Rani ◽  
Najwa Ezira Ahmed Azhar ◽  
Zuraida Khusaimi ◽  
Fazlena Hamzah ◽  
...  
Keyword(s):  
Optical Properties ◽  
Anatase Phase ◽  
Sol Gel ◽  
Band Gap Energy ◽  
X Ray Diffraction ◽  
Structural And Optical Properties ◽  
Tio2 Thin Films ◽  
Xrd Pattern ◽  
X Ray ◽  
Annealing Temperatures

In this research, TiO2 thin films were prepared using a simple sol-gel spin coating process. The films were characterized using Field Emission Scanning Electron Microscopy (FE-SEM), Energy Dispersive Ray (EDX), X-ray diffraction (XRD) and Ultraviolet–visible Spectrophotometer in order to investigate the influence of different annealing temperatures to the structural and optical properties of TiO2. The surface morphology images from FE-SEM display a uniform layer of nanoparticles with a sample of 500 °C possess the most uniform and the visible spherical grain of TiO2 nanoparticles. EDX spectra confirm the presence of Ti and O elements in the samples. The structural properties from the XRD pattern demonstrate that the films are crystalline at a temperature of 500 and 600 °C and the peak (101) intensity was increased as the annealing temperature increased. They exist in the anatase phase at the preferred plane orientation of (101). The calculated crystallite size for 500 and 600 °C samples is 19.22 and 28.37 nm, respectively. The films also possessed excellent absorption in the ultraviolet (UV) region with optical band gap energy ranging from 3.32 to 3.43 eV. These results can be fundamental for the fabrication of a UV sensing device.

Effect of Deposition Time on Structural and Optical Properties of ZnO Thin Films Deposited by Spray Pyrolysis

2019 ◽  
Vol 397 ◽  
pp. 81-87 ◽  
Author(s):  
Farid Khediri ◽  
Abdelkader Hafdallah ◽  
Mouna Bouhelal
Keyword(s):  
Thin Films ◽  
Optical Properties ◽  
Spray Pyrolysis ◽  
Deposition Time ◽  
Spray Pyrolysis Technique ◽  
Precursor Solution ◽  
Zno Thin Films ◽  
X Ray Diffraction ◽  
Structural And Optical Properties ◽  
X Ray

In this work Zinc oxide thin films prepared by spray pyrolysis technique. A set of ZnO thin films were deposited with various deposition times, on glass substrate at 350 °C. The precursor solution is formed with zinc acetate in distilled methanol with 0.1 molarity. The deposition time was ranged from 2 to 8 min. The structural and optical properties of those films were examined by X-ray diffraction (XRD) and ultraviolet-visible spectrometer (UV). X-ray diffraction patterns of the ZnO thin films showed polycrystalline hexagonal wurtzite structure and the preferred orientation was along (002) plane when the grain size varied between 9.66 and 16.67nm. ZnO thin films were highly transparent in the visible with the maximum transmittance of 85% and the optical band gap was found between 3.25 and 3.28 eV.

THEORETICAL AND EXPERIMENTAL STUDIES ON SILOXENE

1993 ◽  
Vol 07 (21) ◽  
pp. 1343-1364 ◽  
Author(s):  
P. DEÁK ◽  
M. STUTZMANN ◽  
M. S. BRANDT ◽  
M. ROSENBAUER ◽  
S. FINKBEINER ◽  
...  
Keyword(s):  
Experimental Data ◽  
Optical Properties ◽  
Magnetic Resonance ◽  
Quantum Chemical ◽  
Experimental Studies ◽  
X Ray Diffraction ◽  
Absorption Coefficients ◽  
Structural And Optical Properties ◽  
X Ray ◽  
Equilibrium Structures

Structural and optical properties of siloxene ( Si 6 O 3 H 6) and its derivatives obtained by chemical substitution or annealing are reviewed. The preparation of siloxene is briefly described and results of x-ray diffraction and infrared absorption are shown. The equilibrium structures of stoichiometric siloxene and the electronic properties of the corresponding 2, 1, and 0-dimensional Si-clusters are obtained from quantum chemical calculations and compared to other calculations. Experimental results concerning luminescence, luminescence excitation, absorption coefficients, magnetic resonance, and stability are presented. The origin of the optical properties of siloxene is discussed based on the accumulated experimental data and on the results of theoretical modeling.

Improvements of Structural and Optical Properties of GaN/Al0.10Ga0.9N Multi-Quantum Wells by Isoelectronic In-doping

2001 ◽  
Vol 693 ◽  
Author(s):  
Lianshan Wang ◽  
Soo Jin Chua ◽  
Wenhong Sun
Keyword(s):  
Optical Properties ◽  
Quantum Wells ◽  
Chemical Deposition ◽  
Crystal Quality ◽  
X Ray Diffraction ◽  
Structural And Optical Properties ◽  
Flow Rates ◽  
X Ray ◽  
In Doping ◽  
Metalorganic Chemical

Absratct:The effects of isoelectronic In-doping were studied on the structural and optical properties of 3-periods and 10-periods of GaN/Al0.10Ga0.90N multi quantum wells (MQWs). The GaN/Al40.10Ga0.90N MQWs were grown on u-GaN/sapphire via metalorganic chemical deposition (MOCVD) at 1050°C in H2 carrier gas. X-ray diffraction (XRD), and micro-Photoluminescence (PL) measurements revealed that In-doping into well layers improves the crystalline and optical properties of MQWs relative to those samples without In-doping. With increasing Trimethylindium (TMIn) flow rates from 4.2 mol/min to 42.6 mol/min, PL peaks from well layers obviously redshifted, due to the improvement of the strain along the interfaces between MQWS, irrespective of 3-periods or 10 periods MQWs. The improvement of the crystal quality was also confirmed by XRD.

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