scholarly journals Superficial Effects of Different Finishing and Polishing Systems on the Surface Roughness and Color Change of Resin-Based CAD/CAM Blocks

Author(s):  
Numan Aydın ◽  
Serpil Karaoğlanoğlu ◽  
Elif Aybala Oktay ◽  
Bilge Ersöz

Objective: CAD/CAM blocks are widely used in dental restorations around the world. This study aimed to investigate the effects of different polishing and finishing systems on surface roughness and color change of resin-based CAD/CAM blocks. Material and Methods: In this study, material samples of 2×7×12mm were prepared. In three different experimental groups, surface polishing was carried out with one-step, two-step and multi-step polishing systems. The samples in one subgroup of each experimental group were polished with the diamond paste. Once the initial roughness and color values of the samples were measured using a profilometer and a spectrophotometer, the samples were immersed in coffee. Surface roughness and color change (∆E00) results were statistically analyzed using two-way variance analysis (ANOVA). Results: Finishing and polishing systems created significantly different levels of surface roughness on the hybrid ceramic block (Vita Enamic) but not on the composites block (Brilliant Crios, Grandio Blocs). While the two-step and multi-step finishing and polishing systems produced the lowest color change on hybrid ceramic blocks, one-step and two-step systems achieved this on composite blocks (p<0.05). In all test groups, the supplementary polishing performed after regular polishing procedures helped us reduce the surface roughness and color change on CAD/CAM blocks.  Conclusions: The findings obtained in this study suggest that one and two-step polishing systems are more suitable for resin-based composite CAD/CAM blocks; for hybrid ceramic CAD/CAM blocks, on the other hand, two and multi-step finishing and polishing systems seem to be more efficient concerning lower surface roughness and resistance to color changes.

Author(s):  
Sara Mohammad Al Taweel ◽  
Afnan F Alfouzan ◽  
Hanan N. Al-Otaibi ◽  
Nawaf Labban ◽  
Huda A Alshehri

Abstract The aim of the present study was to evaluate and compare the effect of thermal-cycling, mechanical brushing and beverage storage on the color changes and surface roughness of conventional heat-polymerized and CAD/CAM PMMA used to fabricate complete dentures. A total of 100 specimens measuring 10 mm in diameter and 3 mm in thickness were fabricated from conventional PMMA resin (Heat-cured, Major. Base.20, Moncalieri, Italy) and CAD/CAM blocks (Opera system, Principauté de Monaco, French). The specimens were subjected to a combined surface treatment involving thermo-cycling, mechanical brushing, and immersed in either artificial saliva (AS), coffee, tea, Coca-Cola, or lemon juice. Colour differences (∆E) and surface roughness (Ra) was determined using a spectrophotometer and non-contact profilometer, respectively. The data were analyzed using IBM SPSS v.20 (α=0.05). Factorial ANOVA showed that independent factors, namely material, beverages, and the interaction between independent factors, significantly influenced ΔE (F=76.862; p<0.001) and surface roughness (F=71.685; p<0.001). The overall highest and lowest colour differences was obtained for CAD/CAM PMMA (∆E=1.93 ± 1.29) and conventional PMMA (∆E=1.41 ± 1.39) resins, respectively (p=0.061). Conventional PMMA (1.22±0.20) demonstrated significantly increased roughness compared to CAD/CAM PMMA (0.91±0.17) (p <0.001). Pearson correlation showed a low degree of correlation, which was non-significant for both the PMMA (r=0.015; p=0.917) and C-PMMA materials (r=0.097; p=0.505). CAD/CAM milled PMMA resins demonstrated greater colour change and lower surface roughness compared to conventional heat-polymerized PMMA resins. Specimens in tea and coffee demonstrated maximum colour changes and were perceivable by the human eye. On the contrary, specimens immersed in low pH acidic beverages namely Coca-Cola and lemon juice demonstrated maximum surface roughness.


2017 ◽  
Vol 18 (4) ◽  
pp. 283-288 ◽  
Author(s):  
Cleidiel AA Lemos ◽  
Silvio J Mauro ◽  
Paulo H dos Santos ◽  
André LF Briso ◽  
Ticiane C Fagundes

ABSTRACT Aim The aim of this study was to investigate the association of different degradations on the roughness, gloss, and color changes of microhybrid composites. Materials and methods Ten specimens were prepared for Charisma, Amelogen Plus, Point 4, and Opallis resins. Surfaces were polished and baseline measurements of roughness, gloss, and color were recorded. Specimens were then submitted to chemical and mechanical challenges, and the specimens were reevaluated. Roughness and gloss were analyzed by Kruskal – Wallis and Dunn's test (p < 0.05). Color change (ΔE) was analyzed by one-way analysis of variance and Tukey's tests (p < 0.05). The initial and final data were compared using the Wilcoxon test (p < 0.05). Spearman test checked the correlation between the roughness and gloss (p < 0.05). Results Regarding surface roughness and gloss, there was no difference between composites before challenges. However, all composites showed a significant increase of roughness after challenges, with highest values for Charisma. The gloss was influenced by challenges, evidencing the best gloss for Point 4. Charisma showed the highest value of color change. There was no correlation between surface roughness and gloss for the initial analysis, and after the challenges. Conclusion Composites were influenced by association of challenges, and Charisma showed the highest changes for roughness, gloss, and color. Clinical significance The type of composite resin influenced the properties of materials, which are surface roughness, gloss, and color change. The dentist should be aware of the performance of different brands, to choose the correct required composite resin for each type of patient or region to be restored. How to cite this article Lemos CAA, Mauro SJ, dos Santos PH, Briso ALF, Fagundes TC. Influence of Mechanical and Chemical Degradation in the Surface Roughness, Gloss, and Color of Microhybrid Composites. J Contemp Dent Pract 2017;18(4):283-288.


Cerâmica ◽  
2016 ◽  
Vol 62 (362) ◽  
pp. 121-127 ◽  
Author(s):  
P. P. Kist ◽  
I. L. Aurélio ◽  
M. Amaral ◽  
L. G. May

Abstract The purpose of the present study was to determine the biaxial flexural strength (BFS) of a CAD/CAM leucite reinforced glass-ceramic ground by diamond burs of different grit sizes and the influence of surface roughness on the BFS. For this, 104 plates were obtained from CAD/CAM ceramic blocks and divided into 4 groups (n = 26), according to bur grit size: extra-fine, fine, medium and coarse. Roughness parameters (Ra, RyMax) were measured, and plates were kept dry for 7 days. The flexural test was carried out and BFS was calculated. Ra, RyMax and BFS data were subjected to analysis of variance and post-hoc test. Weibull analysis was used to compare characteristic strength and Weibull modulus. Regression analysis was performed for BFS vs. Ra and RyMax. When burs with coarse grit were used, higher surface roughness values were found, causing a negative effect on the ceramic BFS (117 MPa for extra-fine, and 83 MPa for coarse). Correlation (r) between surface roughness and BFS was 0.78 for RyMax and 0.73 for Ra. Increases in diamond grit size have a significant negative effect on the BFS of leucite-reinforced glass-ceramics, suggesting that grinding of sintered glass-ceramic should be performed using burs with the finest grit possible in order to minimize internal surface flaws and maximize flexural strength.


2010 ◽  
Vol 04 (02) ◽  
pp. 118-127 ◽  
Author(s):  
Randa Hafez ◽  
Doa Ahmed ◽  
Mai Yousry ◽  
Wafa El-Badrawy ◽  
Omar El-Mowafy

Objectives: The purpose of this study was to determine color changes and surface roughness of composites when they were subjected to in-office bleaching.Methods: 12 discs 15 mm in diameter and 2 mm thick were prepared from two shades (A2 & A4) of two composites, Durafil VS (DF) and TPH3 (TPH). Specimens were polished and stored in distilled water for 24 hours at 37°C before being subjected to bleaching, staining, and re-bleaching. Each of the groups of specimens (DF-A2, DF-A4, TPH-A2 and TPH-A4) were subdivided into three subgroups (n=4) and bleached with Beyond, LumaWhite-Plus, and Opalescence-Boost. Specimens were then stained by immersing them in a coffee solution for 48 hours at 37°C, and then they were re-bleached. Colorimetric measurements were performed at baseline, after bleaching, after staining, and after rebleaching. Surface roughness was determined with environmental SEM before and after bleaching. Data were statistically-analyzed.Results: None of the bleaching systems notably changed the color of composites (delta-E<2). Coffee staining affected DF specimens more than TPH. Stained specimens showed variable responses to whitening with no significant color change observed with TPH (delta-E<2) and significant changes observed with DF. Surface roughness significantly changed with bleaching, but the degree varied according to composite shade and bleaching agent.Conclusions: Three in-office bleaching agents had no significant color changes on two composites. DF showed more color change than TPH when immersed in coffee. Stained composites showed different degrees of whitening, with DF showing more response. Bleaching may adversely affect the surface texture of composites. Dentists should take into consideration that composite restorations may not respond to bleaching in the same way that natural teeth do. (Eur J Dent 2010;4:118-127)


2021 ◽  
Vol 32 (4) ◽  
pp. 19-30
Author(s):  
Nayara Rodrigues Nascimento Oliveira Tavares ◽  
Alexia da Mata Galvão ◽  
Lia Dietrich ◽  
Roberta Furtado Carvalho ◽  
Robinson Sabino Silva ◽  
...  

Abstract: This study investigated the bleaching effectiveness and the physicochemical effects on enamel of violet light and ozone, associate or not to hydrogen peroxide, compared to 35%-hydrogen peroxide. Enamel-dentin blocks from human molars were randomly allocated to receive one of the following bleaching protocols (n=15): (HP) 35%-hydrogen peroxide, (VL) violet light, (OZ) ozone, the association between hydrogen peroxide with ozone (OZ+HP) or violet light (VL+HP). All protocols were performed in two sessions with a 48h interval. Color (spectrophotometer) and mineral composition (Raman spectroscopy) were measured before and after the bleaching. Color changes were calculated by ΔEab, ΔE00, and whitening index (WI). The surface roughness was measured with an atomic force microscope. Data were analyzed by One-way or Two-way repeated measure ANOVA followed by the Tukey’s test (α = 0.05). The lowest color change values (either measured by WI, ΔEab, or ΔE00) were observed for VL and OZ used with no HP. Violet light associate with HP was unable to improve the color changes observed for the peroxide alone, in combination with OZ and HP, the highest color changes were verified. Regardless of bleaching protocol, the bleached enamel presented higher contents of PO4 and CO3 -2 than those observed at baseline. All bleaching protocols resulted in similar enamel surface roughness. Both the VL and the OZ caused reduced effects on the enamel color change when used alone. The ozone therapy improved the bleaching effect in the group that received the association of HP.


2019 ◽  
Vol 44 (3) ◽  
pp. E122-E132 ◽  
Author(s):  
L St-Pierre ◽  
C Martel ◽  
H Crépeau ◽  
MA Vargas

SUMMARY Objectives: The objective of this in vitro study was to compare, with a threshold value of 200 nm, the surface roughness obtained when using 12 different polishing systems on four different composite resins (microfill, nanofill, and two nanohybrids). Methods and Materials: A total of 384 convex specimens were made using Durafill VS, Filtek Supreme Ultra, Grandio SO, and Venus Pearl. After sandblasting and finishing with a medium-grit finishing disc, initial surface roughness was measured using a surface roughness tester. Specimens were polished using 12 different polishing systems: Astropol, HiLuster Plus, D♦Fine, Diacomp, ET Illustra, Sof-Lex Wheels, Sof-Lex XT discs, Super-Snap, Enhance/Pogo, Optrapol, OneGloss and ComposiPro Brush (n=8). The final surface roughness was measured, and data were analyzed using two-way analysis of variance. Pairwise comparisons were made using protected Fisher least significant difference. Results: There were statistical differences in the final surface roughness between polishing systems and between composite resins (p&lt;0.05). The highest surface roughness was observed for all composite resins polished with OneGloss and ComposiPro Brush. Enhance/Pogo and Sof-Lex Wheels produced a mean surface roughness greater than the 200-nm threshold on Filtek Supreme Ultra, Grandio SO, and Venus Pearl. Data showed that there was an interaction between the composite resins and the polishing systems. Conclusions: A single polishing system does not perform equally with all composite resins. Except for Optrapol, multi-step polishing systems performed generally better than one-step systems. Excluding Enhance/Pogo, diamond-impregnated polishers led to lower surface roughness. Durafill VS, a microfill composite resin, may be polished more predictably with different polishers.


Author(s):  
Ana Leticia Franklin Silva ◽  
Rocio Geng‐Vivanco ◽  
Rafaella Tonani‐Torrieri ◽  
Fernanda de Carvalho Panzeri Pires‐de‐Souza

2016 ◽  
Vol 19 (1) ◽  
pp. 88
Author(s):  
Sabrina Alves Feitosa ◽  
Isabela Gomes Moura ◽  
Pedro Henrique Corazza ◽  
Cesar Dalmolin Bergolli ◽  
Clóvis Pagani ◽  
...  

<p><strong>O</strong><span lang="en-US"><strong>bjective: </strong></span><span lang="en-US">This study evaluated the effect of drying times of two total-etch &amp; rinse adhesives on the resin bond strength to a feldsphatic ceramic, before and after aging. </span><span lang="en-US"><strong>Material and Methods: </strong></span><span lang="en-US">Feldsphatic-ceramic CAD-CAM bars were cut into blocks (12×10×4 mm) with a cutting machine (N = 32). </span><span lang="en-US">Impressions were made of each ceramic block with silicone putty material and the negative space was filled with a composite resin.</span><span lang="en-US"> The bonding ceramic surface was etched with hydrofluoric acid, silanized, and the adhesive system (SB- Single Bond 2, 3M-ESPE; or PB- Prime &amp; Bond NT, Dentsply) was applied. The samples were dried at different times (5, 10 and 15 s) before the cementation. The resin and ceramic blocks were cemented by a dual cure resin cement. All samples were stored in distilled water at 37 °C for 24 h. For the μ-TBS test, the samples were sliced into microbars. Half of the bars of each block was tested after 24 h and, the other bars </span><span lang="en-US">were submitted to thermocycling (12,000×) and water storage (150 d)</span><span lang="en-US">. For the 24 h groups, the longer drying time increased (p &lt; 0.05) the bond strength of SB (water/alcohol adhesive), while reduced (p &lt; 0.05) for the PB group (acetone based adhesive). </span><span lang="en-US"><strong>Results: </strong></span><span lang="en-US">For the aged groups, the bond strength for the different drying times had no significant difference, for the both adhesives. </span><span lang="en-US"><strong>Conclusion:</strong></span><span lang="en-US"> Longer drying times increased the bond strength values of SB. Smaller drying times increased the bond strength values of PB. The aging protocol influenced the bond strength of SB groups.</span></p><p class="western"> </p><p class="western" lang="pt-BR"><span><span><span lang="en-US"><strong>Keywords:</strong></span></span></span><span><span><span lang="en-US"><span> Microtensile; Adhesion; Feldspar ceramic; Drying time; Adhesive system.</span></span></span></span></p>


2021 ◽  
Author(s):  
B Oglakci ◽  
BO Kucukyildirim ◽  
ZC Özduman ◽  
E Eliguzeloglu Dalkilic

SUMMARY The aim of this study was to evaluate the effects of different polishing systems on the surface roughness of different nanocomposite resins using various analysis methods. Three types of nanocomposite resins were investigated in this study: supra-nanohybrid (Estelite Asteria), nanohybrid (GrandioSo), and nanoceramic composite resins (Ceram-X Spheretec One). Forty-eight disc-shaped specimens (4 mm in diameter, 2 mm in thickness) were fabricated using a Teflon mold and divided into four groups according to the different polishing systems (n=12). All specimens were processed with one of the following methods: Mylar strip (control), one-step polishers (Opti1step), two-step polishers (Clearfil TwistDia), or multistep polishers (Sof-Lex XT Pop-on). The surface roughness (Ra, μm) was measured by contact profilometry (Mahr, Marsurf PS1) (n=10) and scanning electron microscopy (SEM) (Thermo Fisher Scientific, Phenom XL) at 400× magnification (n=2). The data were statistically analyzed using Kruskal-Wallis and Bonferroni correction tests (p&lt;0.05). In addition, the surface morphology and elemental content were examined by SEM and energy dispersive x-ray spectroscopy (EDS) analyses. Under SEM evaluation, in terms of the polishing systems, there were no significant differences in the surface roughness for supra-nanohybrid composite resin (p&gt;0.05). The multistep polishers created lower surface roughness than the one-step polishers for nanohybrid and nanoceramic composites. In terms of the composite resins, supra-nanohybrid composite exhibited lower surface roughness than nanohybrid composite for all polishing systems (p&lt;0.05). The SEM observations confirmed the surface roughness measurements related to the surface morphology. One-step and two-step polishers created porosity on the surface of nanohybrid and nanoceramic composites. EDS analysis indicated the elemental composition of the particles in the porous zones was quite close to diamond abrasives and glass fillers.


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