Mechanical Properties of Wear Tested LIGA Nickel

2004 ◽  
Vol 841 ◽  
Author(s):  
N. R. Moody ◽  
J. M. Jungk ◽  
M. S. Kennedy ◽  
S. V. Prasad ◽  
D. F. Bahr ◽  
...  

ABSTRACTStrength, friction, and wear are dominant factors in the performance and reliability of materials and devices fabricated using nickel based LIGA and silicon based MEMS technologies. However, the effects of frictional contacts and wear on the mechanical performance of microdevices are not well-defined. To address these effects on performance of LIGA nickel, we have begun a program employing nanoscratch and nanoindentation. Nanoscratch techniques were used to generate wear patterns using loads of 100, 200, 500, and 990 μN with each load applied for 1, 2, 5, and 10 passes. Nanoindentation was then used to measure properties in each wear pattern correcting for surface roughness. The results showed a systematic increase in hardness with applied load and number of nanoscratch passes. The results also showed that the work hardening coefficient determined from indentation tests within wear patterns follows the work hardening behavior established from tensile tests, supporting use of a nanomechanics-based approach for studying mechanical properties of wear tested material.

Author(s):  
Murat Bakirov ◽  
Sergei Chubarov ◽  
Igor Frolov ◽  
Joerg Gastrock

Ever-increasing requirements for reliability and safety of equipment in nuclear power plants (NPP) dictate a necessity to obtain reliable and validated information about the condition of materials in the most safety-relevant and economically vital systems structures and components (SSC). Thus it is a state of science and technology approach to use one method, one methodic and one methodology to facilitate these goals with the purpose of keeping NPPs operating safely by virtue of knowing the state of ageing they are in (with respect to design limits and margins). Method of the control/measurement/testing - how to conduct measurements; methodic - how to interpret the results of measurement; methodology - the program of the control/inspection and testing programmes: localities to conduct the tests, how often, and to follow evolution of test results with the aim of acting before a failure occurs. Such methodology should be based on the use of specimen-free nondestructive method of the inspection (control), which could be used successfully at all stages of life cycle of the equipment: manufacturing, construction, installation of NPP, operation and during the NPP operation through integration into the Plant Life Management (PLiM) programme [1]. It will facilitate a real picture of change (degradation) of a SSC material’s condition in the zones subjected to the harschest stressors (neutron irradiation, erosion-corrosion/flow, thermal fatigue, vibration etc). Currently, there are various approaches used in the world to follow NPP ageing degradation, but until now, no specific methodology is used that could supply all the necessary information [2]. Therefore, there is no way to use various results. Thanks to considerable advances over the last 20 years or so, the science of hardness testing offers an elegant, non-destructive way to obtain vital materials properties — even in-situ on operating SSC [3–6]. In particular, the material’s elastic-plastic condition may be measured, giving indications on tensile yield stress elevation due to hardening and also loss in ductility. The work-hardening index may be easily obtained, giving information on the ability of the material (e.g. pressure vessel steel and weld) to deform plastically without brittle fracture. Taking into account the experience of the Center of Material Science and Lifetime Management Ltd. (CMSLM Ltd.) in the use of methods of hardness testing for the inspection of the equipment of NPP of Russian manufacture in Russia, Germany, Czech, Slovakia, Bulgaria [7], and also similar successful works in this direction in USA (Oakridge) [8], to Czech (NRI Rez) and other countries, it can be seen that the most promising direction in the field of specimen-free inspection of mechanical properties by use of hardness and hardness-related characteristics is use of the kinetic indentation method (KIM, ABIT). This method is based on recording the process of elastoplastic deformation caused by the indentation of a ball indenter. This method allows one to obtain, besides hardness values, tensile properties, elongation, work hardening coefficient, true-stress/true strain diagrammes which normally required the destructive testing of small specimens. However, till now there is no universal method of interpreting the information obtained, although it is generally known that irradiation causes a loss in ductility and increase in hardness and lowering of the work-hardening coefficient. Thus, it is necessary to develop a uniform methodology of using KIM, ABIT with reference to the inspection of materials which will allow to unify the inspection of materials of various classes of the equipment of NPP over all stages of life cycle. With the purpose of introduction of such a methodology it is necessary to develop and realize the program in the frames of IAEA with the above name.


Holzforschung ◽  
2009 ◽  
Vol 63 (4) ◽  
Author(s):  
Stefanie Stanzl-Tschegg ◽  
Wilfried Beikircher ◽  
Dieter Loidl

Abstract Thermal modification is a well established method to improve the dimensional stability and the durability for outdoor use of wood. Unfortunately, these improvements are usually accompanied with a deterioration of mechanical performance (e.g., reduced strength or higher brittleness). In contrast, our investigations of the hardness properties in the longitudinal direction of beech wood revealed a significant improvement with thermal modification. Furthermore, we applied instrumented indentation tests on different hierarchical levels of wood structure (growth ring and cell wall level) to gain closer insights on the mechanisms of thermal treatment of wood on mechanical properties. This approach provides a variety of mechanical data (e.g., elastic parameters, hardness parameters, and viscoelastic properties) from one single experiment. Investigations on the influence of thermal treatment on the mechanical properties of beech revealed similar trends on the growth ring as well as the on the cell wall level of the wood structure.


Materials ◽  
2021 ◽  
Vol 14 (19) ◽  
pp. 5856
Author(s):  
Pragya Mishra ◽  
Pia Åkerfeldt ◽  
Farnoosh Forouzan ◽  
Fredrik Svahn ◽  
Yuan Zhong ◽  
...  

Laser powder bed fusion (L-PBF) has attracted great interest in the aerospace and medical sectors because it can produce complex and lightweight parts with high accuracy. Austenitic stainless steel alloy 316 L is widely used in many applications due to its good mechanical properties and high corrosion resistance over a wide temperature range. In this study, L-PBF-processed 316 L was investigated for its suitability in aerospace applications at cryogenic service temperatures and the behavior at cryogenic temperature was compared with room temperature to understand the properties and microstructural changes within this temperature range. Tensile tests were performed at room temperature and at −196 °C to study the mechanical performance and phase changes. The microstructure and fracture surfaces were characterized using scanning electron microscopy, and the phases were analyzed by X-ray diffraction. The results showed a significant increase in the strength of 316 L at −196 °C, while its ductility remained at an acceptable level. The results indicated the formation of ε and α martensite during cryogenic testing, which explained the increase in strength. Nanoindentation revealed different hardness values, indicating the different mechanical properties of austenite (γ), strained austenite, body-centered cubic martensite (α), and hexagonal close-packed martensite (ε) formed during the tensile tests due to mechanical deformation.


2019 ◽  
Vol 221 ◽  
pp. 01019
Author(s):  
Lev Zuev

The generality of localization of plastic deformation, which is observed at the stage of linear work hardening for HCP, BCC and FCC monoand polycrystals of pure metals and alloys, is considered. It was found previously that the motion rate of localized flow autowave is related to the reciprocal value of the work hardening coefficient by a linear law, which is universal in character. This is further substantiated by the results of the given study. The waves of plastic flow localization are found to have dispersion law. It has been established that in order to address the autowave of localized deformation, a quasi-particle may be introduced. The quasi-particle’s characteristics have been defined.


2001 ◽  
Vol 16 (8) ◽  
pp. 2283-2292 ◽  
Author(s):  
Masatoshi Futakawa ◽  
Takashi Wakui ◽  
Yuji Tanabe ◽  
Ikuo Ioka

This paper describes a novel technique for determining the constitutive equation of elastic–plastic materials by the indentation technique using plural indenters with different apex angles. Finite element method (FEM) analyses were carried out to evaluate the effects of yield stress, work hardening coefficient, work hardening exponent, and the apex angle of indenter on the load–depth curve obtained from the indentation test. As a result, the characterized curves describing the relationship among the yield stress, work hardening coefficient, and the work hardening exponent were established. Identification of the constants of a constitutive equation was made on the basis of the relationship between the characterized curves and the hardness given by the load–depth curve. This technique was validated through experiments on Inconel 600 and aluminum alloy. The determined constitutive equation was applied to the FEM analyses to simulate the deformation including necking behavior under uniaxial tension. The analytical results are in good agreement with experimental results.


Author(s):  
Steffany N. Cerda-Avila ◽  
Hugo I. Medellín-Castillo ◽  
Dirk F. de Lange

The prediction of the mechanical properties of AM parts is very important in order to design and fabricate parts not only of any geometrical shape but also with variable or customized mechanical properties. A limited number of investigations have focused on the analysis and prediction of the mechanical properties of AM parts using theoretical and numerical approaches such as the Finite Element Method (FEM); nevertheless, their results have been not accurate yet. Thus, more research work is needed in order to develop reliable prediction models able to estimate the mechanical performance of AM parts before fabrication. In this paper the analysis and numerical simulation of the mechanical performance of FDM samples with variable infill values is presented. The aim is to predict the mechanical performance of FDM components using numerical models. Thus, several standard tensile test specimens were fabricated in an FDM system using different infill values, a constant layer thickness, one shell perimeter, and PLA material. These samples were measured and modelled in a CAD system before performing the experimental tensile tests. Numerical models and simulations based on the FEM method were then developed and carried out in order to predict the structural performance of the specimens. Finally the experimental and numerical results were compared and conclusions drawn.


Science ◽  
2018 ◽  
Vol 362 (6414) ◽  
pp. eaau1925 ◽  
Author(s):  
Zhao Cheng ◽  
Haofei Zhou ◽  
Qiuhong Lu ◽  
Huajian Gao ◽  
Lei Lu

Gradient structures exist ubiquitously in nature and are increasingly being introduced in engineering. However, understanding structural gradient–related mechanical behaviors in all gradient structures, including those in engineering materials, has been challenging. We explored the mechanical performance of a gradient nanotwinned structure with highly tunable structural gradients in pure copper. A large structural gradient allows for superior work hardening and strength that can exceed those of the strongest component of the gradient structure. We found through systematic experiments and atomistic simulations that this unusual behavior is afforded by a unique patterning of ultrahigh densities of dislocations in the grain interiors. These observations not only shed light on gradient structures, but may also indicate a promising route for improving the mechanical properties of materials through gradient design.


2000 ◽  
Vol 653 ◽  
Author(s):  
Olivier Couteau ◽  
Corinne Charbonnier ◽  
Tomas Kruml ◽  
Jean-Luc Martin

AbstractRepeated stress-relaxation experiments are used to characterize the deformation parameters in 3 types of single crystals (Cu, Ni3Al and Ge) in which different dislocation mechanisms are known to operate. Mobile dislocation exhaustion rates and the amplitude of the yield point at reloading after stress-relaxation are measured. These two parameters are discussed in terms of the work-hardening coefficient in monotonic tests.


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