scholarly journals Chemical composition of essential oil extracted from leaves of Campomanesia adamantium subjected to different hydrodistillation times

2017 ◽  
Vol 47 (1) ◽  
Author(s):  
Juliana Dantas de Oliveira ◽  
Daniely Karen Matias Alves ◽  
Mayker Lazaro Dantas Miranda ◽  
José Milton Alves ◽  
Marcelo Nogueira Xavier ◽  
...  

ABSTRACT: Campomanesia adamantium is a native fruit species of the Cerrado and is used in food and medicines and as bee pasture. The chemical composition of essential oils obtained from plants of the same species have varying constituent proportions due to the influence of extractive factors, environmental, genetic and ontogenetic. This study aimed to identify the influence of hydrodistillation time on the content and chemical composition of essential oil extracted from the leaves of C. adamantium . Treatments consisted of five extraction times (1, 2, 3, 4, and 5h) using Clevenger with five replications in a completely randomized design. It was observed that after two hours of hydrodistillation, the essential oil content remains constant. Regarding the chemical constituents of essential oil, variation of the proportions of the compounds tested occurred at all hydrodistillation times. The compounds spathulenol oxygenated sesquiterpenes and caryophyllene oxide were the majority in the five hydrodistillation times.

2021 ◽  
Vol 13 (11) ◽  
pp. 23
Author(s):  
Teomar Duarte da Silva ◽  
Michele Trombin de Souza ◽  
Mireli Trombin de Souza ◽  
Roger Raupp Cipriano ◽  
Humberto Ribeiro Bizzo ◽  
...  

The restinga is an Atlantic Forest ecosystem characterized by tree, shrub, and herb species that are rich sources of essential oils. In this study, we aim to quantify the essential oil content and determine the chemical constituents of fresh leaves of 14 plant species in a restinga stretch in southern Brazil. Essential oils were obtained by hydrodistillation in a Clevenger-type apparatus and analyzed by gas chromatography coupled to mass spectrometry. Campomanesia reitziana, Cortaderia selloana, and Sophora tomentosa had no essential oils. Total essential oil content ranged from 0.01% (Mikania involucrata) to 1.56% (Varronia curassavica). In total, 60 chemical constituents were identified, representing between 46.2% and 96.5% of the chemical composition of the essential oils. Limonene was the common constituent in all species in which the essential oils were present. The major constituents were ar-curcumene (15.1%) and cis-chrysanthenol (14.2%) in Ambrosia elatior; benzyl benzoate (43.5%) and benzyl salicylate (23.7%) in Aniba firmula; caryophyllene oxide (35.7%) and spathulenol (10.6%) in Austroeupatorium inulaefolium; spathulenol (19.8%) and caryophyllene oxide (14.0%) in Baccharis spicata; caryophyllene oxide (16.3%) in Eugenia astringens; curzerene (30.0%), limonene (13.0%), and germacrone (11.9%) in Eugenia uniflora; caryophyllene oxide (17.1%) and ledol (11.3%) in Lantana camara; caryophyllene oxide (27.7%) and limonene (12.7%) in M. involucrata; 1,8-cineole (19.8%) in Psidium cattleianum; limonene (10.2%) in Schinus terebinthifolius, and allo-aromadendrene (15.2%) in V. curassavica. We expect that our results can assist in selecting species of potential interest for herbal, phytotherapeutic, and cosmetic products.


2019 ◽  
Vol 35 (6) ◽  
Author(s):  
Juliana Oliveira de Melo ◽  
Arie Fitzgerald Blank ◽  
Alisson Marcel Souza de Oliveira ◽  
Thiago Matos Andrade ◽  
Maria de Fátima Arrigoni-Blank ◽  
...  

Lippia gracilis, popularly known in Brazil as ‘alecrim-de-tabuleiro’, is used for many purposes, especially as antimicrobial and antiseptic. The drying process of aromatic and medicinal plants aims to minimize the loss of active principles and slow their deterioration, which may greatly influence the yield and chemical composition of some species. The objective of this study was to evaluate the effect of drying times (0, 2, 4, and 8 days) on the content and chemical composition of the essential oil of L. gracilis accessions LGRA-106, LGRA-109, and LGRA-201. The leaves were dried at 40 oC, and essential oil was extracted by hydrodistillation. Chemical analysis was performed by GC/MS. The experiment was carried out in a completely randomized design with three replications. The accessions of L. gracilis LGRA-106, LGRA-109, and LGRA-201 presented higher essential oil at four days of drying time. The accession LGRA-201 showed the highest essential oil yields at four and eight days of drying, with mean values of 0.038 and 0.029 mL g-1, respectively. The drying time did not influence the contents of thymol, methyl-thymol, γ-terpinene, and carvacrol in the essential oils of L. gracilis, but affected the contents of β-caryophyllene, p-cymene, and carvacrol acetate. The essential oils of the three accessions analyzed in this study revealed different chemical profiles.


2012 ◽  
Vol 30 (3) ◽  
pp. 385-390 ◽  
Author(s):  
Martiely S Santos ◽  
Caroline N Jezler ◽  
Ariana RMF de Oliveira ◽  
Rosilene A Oliveira ◽  
Marcelo S Mielke ◽  
...  

Alpinia zerumbet is an aromatic and medicinal plant rich in essential oil, known as colônia. Essential oils are derived from secondary metabolism and may be a source of raw materials for cosmetic, pharmaceutical, food and perfumery industry. The plant secondary metabolism and biosynthetic activity can vary according to endogenous and exogenous factors to which it is exposed. In this context, in this study we evaluated the influence of harvest time and plant age of Alpinia zerumbet on biomass and essential oil production. For the harvest time experiment the plants of A. zerumbet were harvested at different times (8, 10, 12, 14, 16 and 18 h), using a completely randomized design with four replications. In the plant age experiment the seedlings were propagated by division of rhizomes and grown in a completely randomized design with treatments consisting of four ages (3, 6, 9 and 12 months after transplanting), with seven replications. The extractions of the essential oil were performed by oil hydrodistillation in Clevenger apparatus and chemical analysis by gas chromatography coupled with mass spectrometry (CG-MS). There was an effect of harvest time on the essential oil content with the highest value (0.48%) found at 14:33 h with no change in the chemical composition. In relation to plant age, there was a significant increase in aboveground biomass of plants, accompanied by increases in height, number of shoots, and essential oil content and yield. The major compound terpinen-4-ol was present in higher concentrations in plants harvested between six and nine months old.


Author(s):  
Dalva Paulus ◽  
Dislaine Becker ◽  
Gilmar Antônio Nava ◽  
Daiane Luckmann ◽  
Claúdia de Andrade Moura

Aims: The cultivation of medicinal plants in intercropping with other species of agricultural use has been an alternative to make production sustainable in family farming. The objective of this work was to evaluate the growth, biomass production, and chemical composition of the essential oil of mint (Mentha x gracilis Sole) in intercropping with fruit species in an agroforestry system. Study Design:  The experimental design was randomized blocks with four treatments, mint interplanted with citrus (Citrus sinensis L. Osbeck), bananas (Musa spp.), blackberries (Morus nigra), or Barbados cherries (Malpighia glabra). Place and Duration of Study: The experiment was conducted in the agroforestry located in the sector of Olericultura of the Federal University of Technology – Paraná (UTFPR), Brazil, in the period between November 2015 to February 2017. Methodology: We analyzed light intensity, relative chlorophyll index, height, leaf area, biomass accumulation, essential oil content, oil production and chemical composition of mint grown in agroforestry. Results: The highest production of biomass and essential oil were obtained in the intercropping of mint with citrus and Barbados cherries, possibly due to the edaphic climatic conditions, such as greater light intensity, that favored the growth, production, and chemical composition of the mint essential oil. Bananas and blackberries intercropped with mint were not beneficial for the growth and production of essential oils. Conclusion: The intercropping of mint with citrus and Barbados cherries resulted in higher growth, biomass accumulation, and essential oil content and production. The major components of the essential oils were linalool and carvone, with higher percentages in the intercropping of mint with citrus and Barbados cherries. The cultivation of mint by intercropping with fruit species such as citrus and Barbados cherries is an option to diversify the production of medicinal plants, making it sustainable.


1970 ◽  
Vol 37 (2) ◽  
pp. 211-212 ◽  
Author(s):  
Jasim Uddin Chowdhury ◽  
Md Nazrul Islam Bhuiyan ◽  
Nemai Chandra Nandi

Essential oils obtained by hydrodistillation from needles, dry needles, inflorescences and resin of Pinus caribaea Morelet were analyzed by GC-MS. Seven chemical constituents in oil of needles, 13 in dry needles, 4 in inflorescences and 6 in resin were identified. The major constituents found in the needle oil are limonene, caryophyllene and germacrene D in the dry needle oil limonene, caryophyllene oxide and caryophyllene in the inflorescences oil caryophyllene oxide, limonene and crypton and in the resin oil bicyclo[3.1.1]hept -2-ene, 2,6,6- trimethyl- (52.82%), longifolen, crypton and β-pinene. Key words: Pinus caribaea, Chemical composition, Essential oil, GC-MS doi:10.3329/bjb.v37i2.1735 Bangladesh J. Bot. 37(2): 211-212, 2008 (December)


2018 ◽  
Vol 17 (04) ◽  
pp. 19-27
Author(s):  
Tam T. M. Pham

The study was carried out from June to December, 2014. The objective of this study was to determine a suitable topping time for sweet basil variety grown in the net house at Research and Development Center for Hi-Tech Agriculture Ho Chi Minh City. A two-factorial experiment was designed by the CRD (Completely Randomized Design) with three replications. Factor A consisted of three sweet basil varieties (TN12 as Control, TN33, and TN39) and the factor B was the topping times including untopping (the control), the topping when sweet basil at the four-leaves, at the six-leaves and at the eight-leaves period. The results showed that variety TN39 was suitable for extracting basil-oil because of the highest yield (3,365.4 kg/1,000 m2) and high total essential oil content (0.25%). Variety TN12 could be grown for fresh-eating spicy. The variety TN12 resulted in the fairly high yield (1,955.4 kg/1,000 m2) and total essential oil content (0.20%) with good taste. Topping the basil plant at the six-leaves period reached the highest yield of 2,172.3 kg/1,000 m2.


Author(s):  
Tran Huy Thai ◽  
Nguyen Thi Hien ◽  
Nguyen Duy Manh ◽  
Dinh Thi Thu Thuy ◽  
Nguyen Trung Thanh

The essential oils from the needles and branch of the Abies delaveyi subsp. fansipanensis was collected in Hoang Lien Natural Park, Lao Cai province and was obtained by steam distilation and the yields of essential oils were 0.27% and 0.08% from air-dry material. By the using GC/MS analysis, there are 44 and 52 constituents from needles and branch were identified and accounting 97.75% and 96.86% essential oil. The main constituents of needles essential oil were α-pinene (22.28%), β-phellandrene (17.80%), β-pinene (7.87%), α-cadinol (6.53%), myrcene (4.35%), δ-cadinene (4.39%). The main constituents of branchs essential oil were β-phellandrene (18.0%), α-pinene (10.95%), myrcene (10.76%), β-pinene (6.71%), abienol (6.71%). α-cadinol (3.31%). This is the first study on the chemical constituents of the essential oils from the needles and branchs of Abies delaveyi subsp. fansipanensis in Vietnam.


2006 ◽  
Vol 1 (5) ◽  
pp. 1934578X0600100
Author(s):  
Andreza Maria L. Pires ◽  
Maria Rose Jane R. Albuquerque ◽  
Edson P. Nunes ◽  
Vânia M. M. Melo ◽  
Edilberto R. Silveira ◽  
...  

The essential oils of Blainvellea rhomboidea (Asteraceae) were obtained by hydrodistillation and analyzed by GC/MS and GC/FID. Initially, the essential oil from the aerial parts was investigated. From the 18 identified components, 5-indanol (14.5%) followed by p-cymen-8-ol (10.1%), β-caryophyllene (9.6%), caryophyllene oxide (9.6%), limonene (8.6%), terpinolene (7.8%), and spathulenol (7.7%) were the major constituents. The oil was tested against seven bacterial strains and the results showed significant antimicrobial activity. As a consequence, the essential oils from leaves and from flowers were analyzed separately. The major constituents of the leaf oil were terpinolene (21.2%), β-caryophyllene (19.2%), spathulenol (9.1%), caryophyllene oxide (7.4%), and bicyclogermacrene (7.1%), while the oil of the flowers contained terpinolene (28.1%), 5-indanol (16.3%), p-cymen-8-ol (15.3%) and limonene (14.7%) as prevalent compounds. The oils were tested against the same bacterial strains and the flower oil was the more active. These results indicated that the components of the essential oil from flowers seem to be responsible for the activity.


2016 ◽  
Vol 16 (1) ◽  
pp. 87-94 ◽  
Author(s):  
Laxmi Devkota ◽  
Meena Rajbhandari

Turmeric has been recognized as a pharmaceutical crop. It is valuable primarily for essential oil and curcumin content. Chemical composition of the essential oils obtained from the rhizome of turmeric was determined by GC/MS technique. More than 75 compounds were detected and 67 of them were identified. They accounted for 98.59% of essential oil. The essential oil contained 15 monoterpenes (5.58%), 43 sesquiterpenes (84.37%) and 10 nonterpenic components (8.64%). The major constituents were ß-turmeron, a-turmeron, Epi-a-patschutene, ß-sesquiphellandrene, 1,4-dimethyl-2-isobutylbenzene, (±)-dihydro-ar-turmerone, zingiberene, E-a-atlantone and (-)-caryophyllene oxide. Thin layer chromatographic finger printing and quantitative determination of phenolics in acetone extract of commercially available turmeric samples were carried out using Folin-Ciocalteu colorimetric method. Gallic acid was used as the standard for the estimation of phenolics. All the investigated turmeric extracts contained relatively high amount of phenolics.Nepal Journal of Science and Technology Vol. 16, No.1 (2015) pp. 87-94


2020 ◽  
pp. 24-28
Author(s):  
Ravi Subban ◽  
Sundaram Kaveri

Artabotrys species which belongs to Annonaceae family are pleasant smelling and it is attributed to the presence of mono and sesquiterpenoids present in the essential oil of the plant. The objective of the present work is to review the chemical composition of the essential oils reported from twenty different Artabotrys species from various parts of the world. In the various Artabotrys species, the major compounds are monoterpene and sesquiterpene hydrocarbons and oxygenated sesquiterpenes.  The frequently and most commonly identified constituents are β-caryophyllene, caryophyllene oxide, 3-Carene, cyperene, cyperenone and 1,5-epoxy-salvial4(14)-ene.  Other constituents seems to be more specific to the respective Artabotrys species.


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