scholarly journals 3D investigation of steel fiber distribution in reinforced concrete by X-ray microtomography

2015 ◽  
Vol 8 (5) ◽  
pp. 707-720 ◽  
Author(s):  
A. C. MACHADO ◽  
M. A. SILVA ◽  
R. D. T. FILHO ◽  
M. S. PFEIL ◽  
I. LIMA ◽  
...  
Keyword(s):  
Spatial Distribution ◽  
Reinforced Concrete ◽  
Three Dimensional ◽  
Absorption Capacity ◽  
Steel Fibers ◽  
Three Dimensions ◽  
Morphological Properties ◽  
X Ray ◽  
Brittle Behavior ◽  
Computed Microtomography

ABSTRACTThe effects of the inclusion of steel fibers in concrete have been widely studied in order to investigate possible changes in mechanical properties, such as the increase in tensile strength, ductility, stiffness, toughness (energy absorption capacity), and durability. An immediate consequence of this addition is the mitigation of concrete's brittle behavior, so that the material meets new quality requirements. In this context, it is important to study the spatial distribution of the entire internal structure of these materials. Three-dimensional computed microtomography is a non-destructive inspection technique used to characterize the internal structures of various materials based on X-ray interaction with the inspected object. Topological and morphological properties can be obtained directly in three dimensions by means of mathematical reconstruction of the radiographs, which allows analyzing, for example, porosity and distribution of objects. In this context, the aim of this study is to investigate the spatial distribution of steel fibers, as well as of porosity in reinforced concrete samples. To this end, we used a microtomography system calibrated to operate at a voltage of 80 kV, electric current of 100 μA and a pixel size equal to 24 µm. The results showed low porosity and that the steel fibers were not uniformly distributed throughout the sample.

scholarly journals Gold Exploration in Two and Three Dimensions: Improved and Correlative Insights from Microscopy and X-Ray Computed Tomography

Minerals ◽  
2020 ◽  
Vol 10 (5) ◽  
pp. 476
Author(s):  
Joshua Chisambi ◽  
Bjorn von der Heyden ◽  
Muofhe Tshibalanganda ◽  
Stephan Le Roux
Keyword(s):  
Computed Tomography ◽  
Spatial Distribution ◽  
Gold Mineralization ◽  
Three Dimensional ◽  
Three Dimensions ◽  
Low Grade ◽  
X Ray ◽  
3D Space ◽  
X Ray Computed ◽  
2D And 3D

In this contribution, we highlight a correlative approach in which three-dimensional structural/positional data are combined with two dimensional chemical and mineralogical data to understand a complex orogenic gold mineralization system; we use the Kirk Range (southern Malawi) as a case study. Three dimensional structures and semi-quantitative mineral distributions were evaluated using X-ray Computed Tomography (XCT) and this was augmented with textural, mineralogical and chemical imaging using Scanning Electron Microscopy (SEM) and optical microscopy as well as fire assay. Our results detail the utility of the correlative approach both for quantifying gold concentrations in core samples (which is often nuggety and may thus be misrepresented by quarter- or half-core assays), and for understanding the spatial distribution of gold and associated structures and microstructures in 3D space. This approach overlays complementary datasets from 2D and 3D analytical protocols, thereby allowing a better and more comprehensive understanding on the distribution and structures controlling gold mineralization. Combining 3D XCT analyses with conventional 2D microscopies derive the full value out of a given exploration drilling program and it provides an excellent tool for understanding gold mineralization. Understanding the spatial distribution of gold and associated structures and microstructures in 3D space holds vast potential for exploration practitioners, especially if the correlative approach can be automated and if the resultant spatially-constrained microstructural information can be fed directly into commercially available geological modelling software. The extra layers of information provided by using correlative 2D and 3D microscopies offer an exciting new tool to enhance and optimize mineral exploration workflows, given that modern exploration efforts are targeting increasingly complex and low-grade ore deposits.

Investigation of Microcrack Growth in [0/90]s Composite Laminates

2003 ◽  
Author(s):  
Melody A. Verges ◽  
Paul J. Schilling ◽  
Paul D. Herrington ◽  
Arun K. Tatiparthi
Keyword(s):  
Optical Microscopy ◽  
Composite Laminates ◽  
Damage Evolution ◽  
Applied Load ◽  
Three Dimensional ◽  
Three Dimensions ◽  
X Ray ◽  
Computed Microtomography ◽  
X Ray Computed ◽  
Microcrack Growth

Techniques such as optical microscopy and X-radiography have provided useful information regarding damage in composite laminates, particular in therms of microcracking behavior in individual plies. This focuses on the investigation of microcracking and damage evolution in loaded composite laminates via X-ray computed microtomography. The main advantage in the use of such a technique is that damage within the composite can be assessed in three-dimensions without destruction of the composite. In this work, IM7/977–2, IM7/5555, and IM7/5276-1 coupons were uniaxially tested in a tensile substage, Graphs that convey microcracking density information as a function of applied load were created for [0/90/90/0] laminates. The three dimensional geometry and connectivity of microcracks and other damage in these samples were investigated through microtomographic reconstruction.

scholarly journals Three-dimensional propagation in near-field tomographic X-ray phase retrieval

2016 ◽  
Vol 72 (2) ◽  
pp. 215-221 ◽  
Author(s):  
Aike Ruhlandt ◽  
Tim Salditt
Keyword(s):  
Phase Retrieval ◽  
Near Field ◽  
Three Dimensional ◽  
Three Dimensions ◽  
Current Phase ◽  
Computationally Efficient ◽  
X Ray ◽  
Reconstruction Quality ◽  
Consistency Constraints

This paper presents an extension of phase retrieval algorithms for near-field X-ray (propagation) imaging to three dimensions, enhancing the quality of the reconstruction by exploiting previously unused three-dimensional consistency constraints. The approach is based on a novel three-dimensional propagator and is derived for the case of optically weak objects. It can be easily implemented in current phase retrieval architectures, is computationally efficient and reduces the need for restrictive prior assumptions, resulting in superior reconstruction quality.

Three-dimensional X-ray diffraction imaging of process-induced dislocation loops in silicon

2011 ◽  
Vol 44 (3) ◽  
pp. 526-531 ◽  
Author(s):  
David Allen ◽  
Jochen Wittge ◽  
Jennifer Stopford ◽  
Andreas Danilewsky ◽  
Patrick McNally
Keyword(s):  
Semiconductor Industry ◽  
Three Dimensional ◽  
Crystal Defects ◽  
Three Dimensions ◽  
Dimensional Structure ◽  
Dislocation Loops ◽  
X Ray Diffraction ◽  
X Ray ◽  
Diffraction Imaging ◽  
Relationship Of

In the semiconductor industry, wafer handling introduces micro-cracks at the wafer edge and the causal relationship of these cracks to wafer breakage is a difficult task. By way of understanding the wafer breakage process, a series of nano-indents were introduced both into 20 × 20 mm (100) wafer pieces and into whole wafers as a means of introducing controlled strain. Visualization of the three-dimensional structure of crystal defects has been demonstrated. The silicon samples were then treated by various thermal anneal processes to initiate the formation of dislocation loops around the indents. This article reports the three-dimensional X-ray diffraction imaging and visualization of the structure of these dislocations. A series of X-ray section topographs of both the indents and the dislocation loops were taken at the ANKA Synchrotron, Karlsruhe, Germany. The topographs were recorded on a CCD system combined with a high-resolution scintillator crystal and were measured by repeated cycles of exposure and sample translation along a direction perpendicular to the beam. The resulting images were then rendered into three dimensions utilizing open-source three-dimensional medical tomography algorithms that show the dislocation loops formed. Furthermore this technique allows for the production of a video (avi) file showing the rotation of the rendered topographs around any defined axis. The software also has the capability of splitting the image along a segmentation line and viewing the internal structure of the strain fields.

scholarly journals The Numerical Investigation of Aluminum Foam-protected Reinforced Concrete Slabs under Blast Loading Using AUTODYN-3D

2018 ◽  
Vol 206 ◽  
pp. 01014
Author(s):  
Ahmed K. Taha ◽  
Zhengguo Gao ◽  
Dahai Huang
Keyword(s):  
Reinforced Concrete ◽  
Aluminum Foam ◽  
Steel Plate ◽  
Three Dimensional ◽  
Experimental Tests ◽  
High Energy ◽  
Absorption Capacity ◽  
Concrete Panels ◽  
Reinforced Concrete Slabs ◽  
Concrete Target

Aluminum foam is a lightweight material with high energy absorption capacity. In this study A Nonlinear three-dimensional hydrocode numerical simulation was carried out using autodyn-3d, which is an extensive code dealing with explosion problems. In this simulation, a high explosive material (comp B) is blasted against several concrete panels. The model was first validated using experimental tests carried out by Chengqing and has shown good results. Several numerical tests were carried out to study two parameters that affect the deflection of reinforced concrete panels. The parameters included are the thickness of concrete target and the thickness of steel plate. The results showed that increasing the thickness of the steel plate has an insignificant effect on the deflection of the reinforced concrete target while increasing the thickness of the concrete panel has a significant effect on the deflection of the concrete target.

Diffraction by crystals

2002 ◽  
Author(s):  
David Blow
Keyword(s):  
Fourier Transform ◽  
Three Dimensional ◽  
Incident Beam ◽  
Two Dimensions ◽  
Three Dimensions ◽  
Dimensional Structure ◽  
Angle Of Incidence ◽  
X Ray ◽  
Max Von Laue ◽  
The Fourier Transform

In Chapter 4 many two-dimensional examples were shown, in which a diffraction pattern represents the Fourier transform of the scattering object. When a diffracting object is three-dimensional, a new effect arises. In diffraction by a repetitive object, rays are scattered in many directions. Each unit of the lattice scatters, but a diffracted beam arises only if the scattered rays from each unit are all in phase. Otherwise the scattering from one unit is cancelled out by another. In two dimensions, there is always a direction where the scattered rays are in phase for any order of diffraction (just as shown for a one-dimensional scatterer in Fig. 4.1). In three dimensions, it is only possible for all the points of a lattice to scatter in phase if the crystal is correctly oriented in the incident beam. The amplitudes and phases of all the scattered beams from a three-dimensional crystal still provide the Fourier transform of the three-dimensional structure. But when a crystal is at a particular angular orientation to the X-ray beam, the scattering of a monochromatic beam provides only a tiny sample of the total Fourier transform of its structure. In the next section, we are going to find what is needed to allow a diffracted beam to be generated. We shall follow a treatment invented by Lawrence Bragg in 1913. Max von Laue, who discovered X-ray diffraction in 1912, used a different scheme of analysis; and Paul Ewald introduced a new way of looking at it in 1921. These three methods are referred to as the Laue equations, Bragg’s law and the Ewald construction, and they give identical results. All three are described in many crystallographic text books. Bragg’s method is straightforward, understandable, and suffices for present needs. I had heard J.J. Thomson lecture about…X-rays as very short pulses of radiation. I worked out that such pulses…should be reflected at any angle of incidence by the sheets of atoms in the crystal as if these sheets were mirrors.…It remained to explain why certain of the atomic mirrors in the zinc blende [ZnS] crystal reflected more powerfully than others.

Diffraction

2002 ◽  
Author(s):  
David Blow
Keyword(s):  
Red Light ◽  
Three Dimensional ◽  
Three Dimensions ◽  
X Rays ◽  
X Ray ◽  
Original Direction ◽  
Computational Procedures ◽  
Scattering Material ◽  
Opaque Object ◽  
Diffraction Effects

Diffraction refers to the effects observed when light is scattered into directions other than the original direction of the light, without change of wavelength. An X-ray photon may interact with an electron and set the electron oscillating with the X-ray frequency. The oscillating electron may radiate an X-ray photon of the same wavelength, in a random direction, when it returns to its unexcited state. Other processes may also occur, akin to fluorescence, which emit X-rays of longer wavelengths, but these processes do not give diffraction effects. Just as we see a red card because red light is scattered off the card into our eyes, objects are observed with X-rays because an illuminating X-ray beam is scattered into the X-ray detector. Our eye can analyse details of the card because its lens forms an image on the retina. Since no X-ray lens is available, the scattered X-ray beam cannot be converted directly into an image. Indirect computational procedures have to be used instead. X-rays are penetrating radiation, and can be scattered from electrons throughout the whole scattering object, while light only shows the external shape of an opaque object like a red card. This allows X-rays to provide a truly three-dimensional image. When X-rays pass near an atom, only a tiny fraction of them is scattered: most of the X-rays pass further into the object, and usually most of them come straight out the other side of the whole object. In forming an image, these ‘straight through’ X-rays tell us nothing about the structure, and they are usually captured by a beam stop and ignored. This chapter begins by explaining that the diffraction of light or X-rays can provide a precise physical realization of Fourier’s method of analysing a regularly repeating function. This method may be used to study regularly repeating distributions of scattering material. Beginning in one dimension, examples will be used to bring out some fundamental features of diffraction analysis. Graphic examples of two-dimensional diffraction provide further demonstrations. Although the analysis in three dimensions depends on exactly the same principles, diffraction by a three-dimensional crystal raises additional complications.

Three-Dimensional Characterization of the Microstructure of Bioglass/Polyethylene Composite by X-Ray Microtomography

2007 ◽  
Vol 330-332 ◽  
pp. 503-506
Author(s):  
Xiao Wei Fu ◽  
Jie Huang ◽  
E.S. Thian ◽  
Serena Best ◽  
William Bonfield
Keyword(s):  
Spatial Distribution ◽  
Volume Fraction ◽  
Three Dimensional ◽  
X Ray ◽  
Polyethylene Composite ◽  
Bioactive Properties ◽  
Recent Developments ◽  
3D Information

A Bioglass® reinforced polyethylene (Bioglass®/polyethylene) composite has been prepared, which combines the high bioactivity of Bioglass® and the toughness of polyethylene. The spatial distribution of Bioglass® particles within the composite is important for the performance of composites in-vivo. Recent developments in X-ray microtomography (XμT) have made it possible to visualize internal and microstructural details with different X-ray absorbencies, nondestructively, and to acquire 3D information at high spatial resolution. In this study, the volume fraction and 3D spatial distribution of Bioglass® particles has been acquired quantitatively by XμT. The information obtained provides a foundation for understanding the mechanical and bioactive properties of the Bioglass®/polyethylene composites.

scholarly journals Direct characterization of solute transport in unsaturated porous media using fast X-ray synchrotron microtomography

2020 ◽  
Vol 117 (38) ◽  
pp. 23443-23449 ◽  
Author(s):  
Sharul Hasan ◽  
Vahid Niasar ◽  
Nikolaos K. Karadimitriou ◽  
Jose R. A. Godinho ◽  
Nghia T. Vo ◽  
...  
Keyword(s):  
Solute Transport ◽  
High Speed ◽  
Three Dimensional ◽  
Concentration Field ◽  
Solute Concentration ◽  
Breakthrough Curves ◽  
Pore Scale ◽  
X Ray ◽  
Long Tails ◽  
Computed Microtomography

Solute transport in unsaturated porous materials is a complex process, which exhibits some distinct features differentiating it from transport under saturated conditions. These features emerge mostly due to the different transport time scales at different regions of the flow network, which can be classified into flowing and stagnant regions, predominantly controlled by advection and diffusion, respectively. Under unsaturated conditions, the solute breakthrough curves show early arrivals and very long tails, and this type of transport is usually referred to as non-Fickian. This study directly characterizes transport through an unsaturated porous medium in three spatial dimensions at the resolution of 3.25 μm and the time resolution of 6 s. Using advanced high-speed, high-spatial resolution, synchrotron-based X-ray computed microtomography (sCT) we obtained detailed information on solute transport through a glass bead packing at different saturations. A large experimental dataset (>50 TB) was produced, while imaging the evolution of the solute concentration with time at any given point within the field of view. We show that the fluids’ topology has a critical signature on the non-Fickian transport, which yet needs to be included in the Darcy-scale solute transport models. The three-dimensional (3D) results show that the fully mixing assumption at the pore scale is not valid, and even after injection of several pore volumes the concentration field at the pore scale is not uniform. Additionally, results demonstrate that dispersivity is changing with saturation, being twofold larger at the saturation of 0.52 compared to that at the fully saturated domain.

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