scholarly journals ADDITION OF RICE HUSK NANOCELLULOSE TO THE IMPACT STRENGTH OF RESIN BASE HEAT CURED

2021 ◽  
Vol 4 (3) ◽  
pp. 119
Author(s):  
Muhammad Aditya Ramadhan Hasran ◽  
Dian Noviyanti Agus Imam ◽  
Bambang Sunendar

Background: One of the materials for denture bases is heat-cured acrylic resin (PMMA). This material still lacks impact strength as a mechanical strength property. The addition of reinforcing material is known to increase the mechanical strength of PMMA. One of the reinforcing materials added to PMMA is nano cellulose from rice husks, one of the wastes from agricultural products. Purpose: This study aims to determine rice husk nano cellulose's addition to the PMMA denture base's impact strength. Method:  The research sample consisted of six groups, each group consisting of 8 samples selected by simple random. The PI, P2, P3, P4, P5, and K groups were PMMA with 1%, 2%, 3%, 4%, 5% nano cellulose, and without nano cellulose. Result: Mean impact strength test results were 41.50 x 10-3 ± 3.891 J / mm2 for P1, 44.13 x 10-3 ± 3,980 J / mm2 for P2, 45.63 x 10-3 ± 4,438 J / mm2 for P3, 46.87 x 10-3 ± 4,824 J / mm2 for P4, 49.12 x 10-3 ± 4.016 J / mm2 for P5 and 36.25 x 10-3 ± 1.982 J / mm2 for K. One way Anova test results with p-value of 0.000 indicates differences in the six groups (p<0.05). Conclusion: This study concludes that the impact strength value of PMMA with the addition of rice husk nano cellulose has increased compared to the control group without the addition of rice husk nano cellulose.

DENTA ◽  
2018 ◽  
Vol 12 (1) ◽  
pp. 51
Author(s):  
Widaningsih Widaningsih ◽  
Annete Juwita ◽  
Puguh Bayu Prabowo

<p><strong><em>Background:</em></strong><em> Self-cured acrylic resin is a material used for repairing broken and fractured dentures. Zirconium dioxide (ZrO2) is a reinforcing material that is being developed as an additive to the acrylic resin. <strong>Objective:</strong> to determine the effect of zirconium dioxide (ZrO<sub>2</sub>) addition on self-cured acrylic resin on impact strength. <strong>Material and Methods:</strong> This study was a true experimental laboratory study with the design of a post-test only control group design, using 24 pieces of self-cured acrylic resin measuring 65 x 10 x 2.5 mm divided into 4 groups with and without zirconium addition dioxide (ZrO<sub>2</sub>) nanoparticles. Zirconium dioxide (ZrO<sub>2</sub>) nanoparticles were silanized first by mixing the silane coupling agent. Furthermore, the impact strength was tested on the plate. The data obtained were analyzed using the One Way ANOVA test. <strong>Results:</strong> there were significant differences in the impact strength between the groups with a significance value of 0,000 (p &lt;0.05). <strong>Conclusion:</strong> there was a difference in the increase of impact strength in acrylic resin self-cured with the addition of ZrO<sub>2</sub> nanoparticles concentrations of 3%, 5%, and 7%.</em></p><p><em><br /></em></p><p><strong><em>Key words:</em></strong><em> Self cured acrylic resin, zirconium dioxide, impact strength</em><em></em></p><p><strong><em> </em></strong></p><strong><em>Correspondence </em></strong><em>: Widaningsih, Department of Prosthodonti, Faculty of Dentistry, Hang Tuah University, Arif Rahman Hakim 150, Sukolilo, Surabaya, Phone 0818312757, Email: </em><a href="mailto:[email protected]"><em>[email protected]</em></a>


2021 ◽  
Vol 6 (2) ◽  
pp. 106
Author(s):  
Mara Gustina ◽  
Widjijono Widjijono ◽  
Endang Wahyuningtyas

Non-dental glass fiber is one of the materials that can be used to increase the impact strength of a acrylic resin base plate, containing a similar composition to that of dental e-glass fiber. Orientation and positions of fiber affect the reinforcement effectiveness. This research aimed to examine the effect of the orientation of non-dental glass fiber in the compression position on the impact strength of an acrylic resin base plate. The research was conducted on 16 acrylic resin plates with fiber (65 mm x 10 mm x 2.5 mm) addition. The samples were divided into 4 groups (combination of different woven orientation unidirectional, bidirectional woven in the compression position, and control). The material used in this study was heat-cured acrylic resin QC-20 brand, non-dental glass fiber (without any brand). Impact strength was tested using an impact testing machine. The data obtained were analyzed using one-way ANOVA test and LSD (p<0.05). In this research the impact strength of the base plate with the addition of fiber increased 8.54 ± 2.21; 13.21 ± 2.34; 16.81 ± 2.80 kJ/m2 compared to that of the control group, i.e. 4.98 ± 1.05 kJ/m2. One-way ANOVA test showed a significant effect (p<0.05) of the fiber orientation variations on the compression position. This research concluded that the addition of nondental e-glass fiber (composed of SiO252.56-56.88%), diameter 17.12–20.03 µm) in the compression zone increases theimpact strength of acrylic resin base plate. Fibers with unidirectional orientationprovides the highest increase in the impact strength of acrylic resin base plate.


2021 ◽  
Vol 17 (1) ◽  
pp. 49-55
Author(s):  
Ni Kadek Sugianitri ◽  
◽  
Suhendra Suhendra ◽  

Introduction: Acrylic resin is the most common material for the denture base because the acrylic resin has good esthetics, ease of processing, reparability, and inexpensive. A disadvantage of acrylic resin is that it is easy to be cracked. One of the ways to resolve this problem is by adding agave sisalana fiber and E-glass fiber. The purpose of this study was to find out the effect of the addition of agave sisalana fiber and E-glass fiber on the impact strength of an acrylic resin denture plate reparation. Material and Method: The experiment involved twenty-seven plates of heat-cured acrylic with the dimensions of 55x 10 x 10 mm with the 26 x 5 x 4 mm for the cavity to measure, each measurement divided into three groups, with nine samples for each group. The first group was a control group (without fiber), the second group was a group with agave sisalana fiber addition, the third group was a group with e-glass fiber addition. All plates were soaked in distillation water for one day at 37o C. Plates were tested for impact strength using the Charpy method. All data obtained were analyzed with one-way ANOVA followed by LSD (Least Significant Difference) with p<0,05. Result and Discussion: The result showed that the influences of impact strength between without fiber with agave sisalana fiber and E-glass fiber addition on acrylic denture reparation. Acrylic denture reparation in both fibers with concentration 3,3%, agave sisalana fiber has the highest impact strength rather than e-glass fiber. Conclusion: The conclusion of this study is that there is an increase in impact strength with agave sisalana fiber and E-glass fiber addition on acrylic denture reparation and agave sisalana fiber has the highest impact strength.


2018 ◽  
Vol 12 (1) ◽  
pp. 202-212 ◽  
Author(s):  
Hawraa Khalid Aziz

Background: The criteria of conventional curing of polymethyl methacrylate do not match the standard properties of the denture base materials. Objectives: This research was conducted to investigate the addition of TiO2 nano practical on impact strength, thermal conductivity and color stability of acrylic resin cured by microwave in comparison to the conventional cured of heat-polymerized acrylic resin. Materials and Methods: 120 specimens made of high impact acrylic resin were divided into two main groups according to the type of curing (water bath, microwave), then each group was subdivided into two groups according to the addition of 3% TiO2 nano-fillers and control group (without the addition of TiO2 0%). Each group was subdivided according to the type of test into 3 groups with 10 specimens for each group. Data were statistically analyzed using Student t-test to detect the significant differences between tested and control groups at significance level (P<0.05). Results: According to curing type methods, the results showed that there was a significant decrease in impact strength of microwaved cured resin, but there was no significant difference in the thermal conductivity and color stability of resin. In addition, by using nanofiller, there was a significant increase in the impact strength and color stability with the addition of 3% TiO2 nanofillers, but no significant difference was found in the thermal conductivity of the acrylic resin. Conclusion: The microwave curing of acrylic resin had no change in the color stability and thermal conductivity in comparison to the water bath, but the impact strength was decreased. The addition of 3% TiO2 improved the impact and the color stability, but the thermal conductivity did not change.


2018 ◽  
Vol 1 (2) ◽  
pp. 81
Author(s):  
Chanita Elonianty ◽  
Titien Hary Agustantina ◽  
Intan Nirwana

Background: The prevalence of acrylic resin dentures fracture due to accidental drop is relatively high especially when it is being cleaned by patient. The effort to strengthen acrylic resin denture was done by adding Bambusa arundinacea (Retz.) Willd fibers, which was based on previous research. It has been proven that the addition of bamboo fiber to self-cured acrylic resin can increase the tensile strength. It has acceptable tensile properties, relatively low cost, high toughness, and good thermal properties. Purpose: To determine the impact strength of heat-cured acrylic resin after the addition of Bambusa arundinacea (Retz.) Willd. fibers at various lengths and weights. Methods: Bambusa arundinacea (Retz.) Willd. fibers with lengths of 2 mm, 6 mm, 12 mm and weights of 3wt%, 6wt%, 9wt% were added to heat-cured acrylic resin. The impact strength of heat-cured acrylic resin was tested using the Charpy method with mini impact tester KRY type. The test results were calculated using the impact strength formula. The research data were analyzed using one-way anova test and Tukey HSD test. Results: The data analysis showed that there was a significant difference in impact strength of heat-cured acrylic resin after the addition of Bambusa arundinacea (Retz.) Willd fibers. Conclusion: Addition of Bambusa arudinacea (Retz.) Willd. fibers increased the impact strength of heat-cured acrylic resin respective to the increment of length and weight of Bambusa arudinacea (Retz.) Willd. fibers.


2021 ◽  
Vol 58 (3) ◽  
pp. 239-246
Author(s):  
Aisha Kiran ◽  
Faiza Amin ◽  
Muneeb A Lone ◽  
Imran Alam Moheet ◽  
Maham M Lone ◽  
...  

This study determined and compared the influences of various processing techniques including air circulating oven (ACO), dry heat oven (DHO) and water bath (WB) on the impact strength (IS) and microhardness (HV) of the conventional heat cure acrylic resin (CHCAR) and rubber reinforced heat cure acrylic resin (RRHCAR). Samples were fabricated using CHCAR (control Group A; n=114) and RRHCAR (experimental Group B; n=114). Group A and B were further divided into subgroups according to processing techniques: ACO, DHO and WB (n=38 each) for both testing variables microhardness and impact strength (n=19 each). Charpy testing machine and Vickers microhardness tester were utilized. Analysis of variance was applied to determine the presence of significant differences among processing techniques while P-value ≤ 0.05 was considered as significant. Water bath (P-value [0.001) and DHO technique (p-value [0.001) showed significant differences between both groups� impact strength and microhardness. Microhardness of group A and B showed a significant difference (p-value 0.002) when processed by ACO. Impact strength and micro hardness were improved in RRHCAR compared to CHCAR processed by ACO and DHO in comparison to WB technique. Rubber reinforced heat cure acrylic resin revealed improvement in the impact strength and microhardness. The air circulating oven exhibited highest microhardness in both testing materials. Dry heat oven showed improved values of impact strength in conventional heat cure acrylic resin.


2018 ◽  
Vol 12 (1) ◽  
pp. 946-951
Author(s):  
Firas Abd Kati

Background: For many dental and facial restorations, acrylic resins are the materials of choice because of their appropriate physical and mechanical properties. When making the ocular prosthesis from such materials, it is essential to add the perfect shade in order to match the colour of normal eye. This, however, might have a significant effect on the mechanical properties of acrylic resins. Objective: The purpose of this study was to assess the effect of adding the white oil paint (titanium dioxide) to clear acrylic resins on their impact strength. Methods: 20 samples were constructed from heat cured acrylic resins, and divided into two groups (control and experimental) and each group had 10 samples. The first group was made from clear acrylic resin without the addition of white oil paints, and the second group (experimental) comprised the addition of 1 ml of the white oil paints to acrylic samples. Such samples were prepared with dimensions of (80 mm X10 mm X4 mm) length, width, and thickness, respectively. All the samples were tested by the Charpy's impact strength test. They were exposed to the load till the fracture occurred. All the values were analyzed using SPSS version 20, and the independent T-test was used for comparison between the 2 groups. Results: A statistically significant decrease (P-value < 0.001) was found in the impact strength of acrylic resins after the addition of titanium dioxide oil paints (experimental group: 5.97 + 1.11, control group: 9.42+1.32 KJ/M2). Conclusion: This study concluded that the addition of titanium dioxide oil paint significantly reduces the impact of strength of the acrylic resin. It is suggested to use different stains which will have no negative effect on impact strength of the acrylic resin.


2021 ◽  
Vol 12 (1) ◽  
pp. 227
Author(s):  
Azamataufiq Budiprasojo ◽  
Feby Erawantini

<p class="Abstract">The aim of this research is to analyze the effect of Titanium Dioxide (TiO2) nanoparticles as resin concentrate on mechanical strength. The tested mechanical strength is Bending strength, Impact Strength, and Microhardenest Strength. The types of resin used in this study were acrylic resin without conventional modification and acrylic resin with an additional 0.01 gr and 0.06 gr of TiO2. Specimen dimensions are made revered to ISO 20795-1 (2008) standard specifications. Mechanical strength was determined by using the universal testing machine, Izod pendulum impact testing machine, and also Vickers microhardness tester. From the analysis, the researcher found that the bending strength of resin acrylic was greatly decreased by increasing the TiO2 concentration. It happens in both TiO2 0.01gr and 0.06gr of acrylic resin compared to the non TiO2 resin. The impact strength of 0.01gr TiO2 acrylic resin was significantly increased compared to non TiO2 acrylic resin. But on the other hand for 0.06gr acrylic resin, impact strength was decreased and recorded the lowest impact strength. The highest Micro hardness strength was found in 0.06gr TiO2, It is significantly increased compared to 0.01gr TiO2 and 0gr TiO2. The general conclusion is, adding 0.01gr TiO2 nanoparticles as concentrated into acrylic resin can significantly increase the bending strength, bending strength, and microhardness strength. Meanwhile, adding 0.06gr Tio2 nanoparticles as concentrated into acrylic resin can only increase the bending strength and the microhardness strength, but not for its impact strength.</p>


2021 ◽  
Vol 74 (9) ◽  
pp. 2293-2296
Author(s):  
Rafah Habib Abdul Amir

The aim: This study evaluates the effect of adding silanized halloysite nanotubes to the polymethylmethacrylate (PMMA) resin on its hardness, impact strength, transverse strength. Materials and methods: Three groups of acrylic resin were prepared, one group without HNTs, was used as a control group (A). The other two groups contained 0.3% (B), 0.6% wt of silanized halloysite nanotubes (C). For each one, hardness, impact strength and transverse strength were measured. One-way ANOVA and Tukey’s test were used for comparison. Results: Regarding to the impact test, there was no significant difference between 0.3% concentration and the pure (control) group while 0.6% concentration had significant decrease compared to the pure group and so between the 0.3% group 0.6% group. For the hardness test, the 0.3% group had no significant difference with the pure group and a significant difference between group 0.6% group and the pure group while there was a no significant decrease between the 0.3% and 0.6% group with the higher hardness mean in the 0.3% compared to 0.6% group. For the transverse strength, both 0.3% wt concentration and 0.6% concentration showed significant difference compared to the pure group and also between each other with the lowest impact strength in 0.6% group followed by 0.3% group with the highest transverse strength in the pure group. Conclusions: The silanation of halloysite nanotubes reduces the mechanical properties of the heat-cured acrylic denture base material. The more concentration of silanazed halloysite nanotubes is added, the more weakening occurs in the acrylic material relating to the hardness, transverse strength and impact strength.


Author(s):  
Mohammed Moustafa Ahmed Gad ◽  
Mohamed Saber Ali ◽  
Ahmad M. Al-Thobity ◽  
Yousif A. Al-Dulaijan ◽  
Mai El Zayat ◽  
...  

Abstract Objective This study aimed to evaluate the effect of nanodiamond (ND) addition to repair resin with repair gap modifications on the flexural and impact strength of repaired polymethylmethacrylate denture base. Materials and Methods Heat-polymerized acrylic resin specimens (N = 100/test) were prepared and sectioned to half creating two repair gaps: 2.5- and 0 mm with 45 degrees beveling. They were further divided into subgroups (n = 20) according to ND concentration (control, 0.25%ND, and 0.50%ND), thermocycling (500 cycles) was done to half the specimens in each subgroup. Flexural strength was tested using 3-point bending test and impact strength was tested by Charpy's impact test. Analysis of variance and post-hoc Tukey's tests were performed for data analysis (α = 0.05). Scanning electron microscope was employed for fracture surface analysis and ND distribution. Results Before and after thermocycling, the addition of ND significantly increased the flexural strength and elastic modulus in comparison to control group (p ˂ 0.001), while 0 mm repair gap showed insignificant difference between ND-reinforced groups (p ˃ 0.05). Regarding impact strength, ND addition increased the impact strength with 0 mm gap in comparison to control and 2.5 mm with ND (p˂0.001), while later groups showed no significant in between (p ˃ 0.05). Comparing thermocycling effect per respective concentration and repair gap, thermocycling adversely affected all tested properties except elastic modulus with 0 mm–0.25 and 0 mm–0.5% and impact strength with 2.5 mm, 2.5 mm–0.25%, 2.5 mm– 0.5% (p ˃ 0.05). Conclusion ND addition combined with decreased repair gap improved the flexural strength, elastic modulus, and impact strength of repaired denture resin, while thermocycling has a negative effect on denture repair strength.


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