scholarly journals Pengaruh beban kompaksi dan suhu sintering terhadap densitas dan sifat mekanik aluminium water atomized

2019 ◽  
Vol 17 (2) ◽  
Author(s):  
Heru Sukanto

<p class="biasa">The powder size used in the research were maximum of 297mm and maximum of 105m resulted by water atomization. Both powder sizes were dry mixed by ratio of 65:35 %wt and was added by 1,25% wt of wax. Mixing was taking a place in steel cylinder with diameter of 2” roteted at 140 rpm for 2 hr. Green body was formed by pressing pressure of 280, 340, 400 and 435 Mpa. Sintering was conducted in argon and temperatures variation of 500, 550, 600 and 650<sup>o</sup>C for 2 hr.</p><p class="biasa">The results show thet sintering temperature change have no significant effects on density and mechanical properties while presing pressure have dominantly effects. Traverse rupture strength, density and hardness growth with  increasing pressing pressure but they will decrease with increasing sintering temperature. The best increasing of mechanical properties was occurred at temperature sintering of 500<sup>o</sup>C and compaction pressure of 400 Mpa.</p>

2013 ◽  
Vol 372 ◽  
pp. 398-401
Author(s):  
Hee Jin Jeong ◽  
Hwan Kyun Yeo ◽  
Dae Yeol Bae ◽  
Je Hyun Kim ◽  
Dong Woo Kim ◽  
...  

This study proposes the research method to examine through experiment the mechanical properties of final products based on the size and sintering temperature of powder particle during STS630 powder based metal injection molding and heat treatment processing condition after the sintering. The feedstock for the injection was manufactured based on STS630 powder with the diameter of 7.0±1.0μm and 8.0±1.0μm and the sintering was carried at 2 temperature conditions of 1300°C and 1355°C after the injection and debinding process. Heat treatment conditions of sample after the sintering were divided into 2 types thus final samples of total 8 cases were manufactured. Then, the 5 types of mechanical properties test were conducted. Optimal processing conditions for MIM molding and heat treatment of STS630 powder could be established based on it.


2019 ◽  
Vol 38 (2019) ◽  
pp. 792-805 ◽  
Author(s):  
S. Ramakrishna Kandala ◽  
Kantesh Balani ◽  
Anish Upadhyaya

AbstractThe present study compares the mechanical properties and electrochemical behaviour of austenitic (AISI 316 L) stainless steel compacted at different pressures (200, 400 and 600 MPa), which are conventionally sintered at supersolidus temperature of 1,400°C. As expected, increase in compaction pressure (from 200 MPa) to 600 MPa has shown decreased shrinkage (from 7.3% to 4.2% radial and 5.5% to 3.4% axial, respectively) and increased densification (up to ~92%). Their electrochemical behaviour was investigated in 0.1 N H2SO4 solution by potentiodynamic polarization and electrochemical impedance spectroscopy. The mechanical properties (such as yield-, tensile- and transverse rupture strength) and electrochemical behaviour with pressure have been correlated with densification response and microstructure (pore type, volume and morphology). Highest densification (~92% theoretical) achieved at 600 MPa (compaction pressure) and 1,400°C (sintering temperature) resulted in excellent combination of tensile strength and ductility (456 ± 40 MPa and 25 ± 1.1% respectively), while showing lowest corrosion rate (0.1 mmpy or 4.7 mpy) due to the presence of isolated porosity in the sintered samples.


2013 ◽  
Vol 275-277 ◽  
pp. 1917-1920
Author(s):  
Bing Liang Liang ◽  
Yun Long Ai ◽  
Chang Hong Liu ◽  
Nan Jiang

WC-Co cemented carbide specimens were prepared via vacuum sintering. The influences of composition and sintering temperature on phase composition, microstructure and mechanical properties of WC-Co cemented carbide were investigated. The results show that dense specimens were obtained in the sintering temperature range of 1280~1400°C and the relative density reached over 95%. Only WC and Co3W3C (-phase) were detected by XRD without any else phases, even though Co. With the ascended sintering temperature, hardness increased and the transverse rupture strength (TRS) ascended to peak value and then descended. WC-Co cemented carbide with excellent mechanical properties (HRA>90, TRS~700MPa and KIC>10MPa•m1/2) were obtained.


2016 ◽  
Vol 1133 ◽  
pp. 259-263 ◽  
Author(s):  
Mohd Hasnan Abdull Hamid ◽  
Fazira Suriani Mohamed Fadzil ◽  
Mohd Asri Selamat ◽  
M.A. Ahmad

Cobalt chromium molybdenum (CoCrMo) alloy is widely used in artificial hip and knee joints because of their excellence corrosion and wear resistance, as well as good mechanical properties and biocompatibility. This study investigates the effect of sintering temperature on the microstructure and mechanical properties of CoCrMo using powder metallurgy technique. CoCrMo powder was mixed with zinc stearate and then put into the shaker mixer at 65 rpm for 3 hours. The powder was then compacted at a pressure of 18T using an automated hydraulic press and sintered at a temperature in the range of 1200 – 1400 °C under 95 Vol% N2/ 5 Vol% H2atmosphere. The microstructure, physical and mechanical properties of the samples are analyzed using scanning electron microscopy (SEM), Vickers’s microhardness tester and transverse rupture strength (TRS). The study reveals that the density, hardness and strength of CoCrMo samples increase as sintering temperature increases.


2014 ◽  
Vol 59 (4) ◽  
pp. 1499-1505 ◽  
Author(s):  
M. Sulowski

Abstract The effects of processing parameters on the microstructure and mechanical properties of Fe-Mn-Cr- Mo-C PM steels are described. Pre-alloyed Astaloy CrM and Astaloy CrL, low-carbon ferromanganese and graphite powders were used as the starting materials. After pressing in rigid die, the compacts were conventionally and high temperature sintered at 1120 and 1250°C, respectively. Sintering was carried out for 60 minutes in atmospheres with different H2/N2 ratios. Cooling rate from sintering temperature was 65°C min-1 (convective cooling). The specimens were subsequently tempered at 200°C for 60 minutes in air. All specimens were tested for tensile strength (UTS), elongation (A), offset yield strength (R0:2), transverse rupture strength (TRS), impact toughness and apparent surface hardness (HV 30). After mechanical tests the microstructure of Fe-Mn-Cr-Mo-C PM steels was studied by optical microscopy. These investigations have shown that, by sintering in inexpensive and safe nitrogen-rich atmospheres, it is possible to achieve mechanical properties similar to those of specimens sintered in pure hydrogen and hydrogen-rich atmospheres.


2012 ◽  
Vol 268-270 ◽  
pp. 340-343
Author(s):  
Chong Cai Zhang ◽  
Quan Wang

In this paper, the WC-16TiC-xTaC-9Co and Co are mixed together preparing for WC, (W, Ti, Ta) C. By high-energy ball milling, the powder is cold isostatic pressed and vacuum sintered by 1410°C, 1430°Cand 1450°C.The physical properties and the micrographs of samples are detected. The main conclusions are as following: sintered samples have the best comprehensive performance at 1450°C, the density of the sample is 99.7% and the actual density is 10.91g/cm3. The hardness is 92.8 HRA and the transverse rupture strength (TRS) is 1100MPa. The grain size grows up obviously with the high temperature. The average grain size of WC is 0.7μm and the average size of (W, Ti, Ta)C is 3μm.


2013 ◽  
Vol 589-590 ◽  
pp. 578-583 ◽  
Author(s):  
Ya Cong Chai ◽  
Han Lian Liu ◽  
Chuan Zhen Huang ◽  
Bin Zou ◽  
Hua He Liu

Ti(C,N)-based cermets were fabricated by the vacuum hot-processing technique. The effect of sintering process, initial powder size and binder content on mechanical properties of Ti(C,N)-based cermets were investigated. The composite was analyzed by the observation of scanning electron microscope (SEM) and energy dispersive spectrometry (EDS). The results showed that a lower sintering temperature led to insufficient liquid-phase sintering process, which reduced the density of the composite. However, higher temperature and longer holding time resulted in abnormal grain growth, which was not good for improving the mechanical properties of the composite. With the refinement of the initial powder size of the Ti(C,N), the fracture toughness reduced slightly, the flexural strength and Vickers hardness increased. The better mechanical properties were obtained when the binder content of the cermets was designed based on the eutectic composition of Mo-Ni binary alloy phase diagram.


2021 ◽  
Author(s):  
Johnson Kehinde Abifarin

Abstract Our previous study have reported synthesis and mechanical properties of natural hydroxyapatite (HA), but optimization of the measured hardness and compressive strength has not been examined. This paper presents optimization of mechanical characteristics (hardness and compressive strength), using Taguchi-grey relational analysis design. In the design, three factors with mixed levels (2 and 3) is employed with the consideration of sintering parameters (0 and 500 Pa compaction pressure, and 900, 1000 and 1100 oC sintering temperature), reported in the previous study. The orthogonal array L18 having 18 rows corresponding to the number of tests and the required columns was selected. Results obtained shows that HA with good hardness and compressive strength is feasible with less or no compaction pressure sintering parameter. An optimum grey relational grade (GRG) of the synthesized HA is 0.7171 and has experimental value within 95% confidence interval.The optimal sintering parameters are gotten to be 500Pa compaction pressure and 1100 oC sintering temperature. Result shows that sintering temperature having 99.90 percentage of contribution is the most significant factor, while compaction pressure and error are insignificant on the overall hardness and compressive strength of the synthesized HA.


2011 ◽  
Vol 335-336 ◽  
pp. 265-272 ◽  
Author(s):  
Bin Zhan ◽  
Ning Liu ◽  
Wei Xu ◽  
Jin Gang Shi

Four Ti(C, N)-based cermets was fabricated from different size of ceramic powder by the conventional powder metallurgy technique. Microstructure, fracture surfaces and crack propagation path of samples were observed by SEM, and mechanical properties such as transverse rupture strength, hardness and fracture toughness were measured. Results show that with the refinement of the raw TiC/TiN powders, the black cores and ceramic grains tend to be finer, the gains with white core-grey rim structure obviously increase, and the microstructure of cermet becomes inhomogeneous. The cermets fabricated from fine powders possess higher porosities. Compared with the cermets made from micron ceramic powders, the cermets fabricated from ceramic powders containing nano powder possess higher transverse rupture strength and lower fracture toughness. When the cermet is fabricated from micron TiC/nano TiN powders, its combination property is the best.


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