scholarly journals Research of the regularities of obtaining silver nanoparticles with applying of polyvinylpyrolidone and their effect on composite’s fungibactericidal properties

2021 ◽  
Vol 4 (1) ◽  
pp. 237-242
Author(s):  
Н. D. Dudok ◽  
◽  
N. B. Semenyuk ◽  
T. V. Skorokhoda ◽  
Yu. Ya. Melnyk ◽  
...  
Keyword(s):  
Silver Nanoparticles ◽  
Antimicrobial Properties ◽  
Silver Ions ◽  
Reduction Reaction ◽  
Reducing Agent ◽  
Practical Application ◽  
Technological Factors ◽  
Porous Blocks ◽  
The Impact ◽  
Kinetics Of

The influence of technological factors on the regularities of obtaining silver nanoparticles using polyvinylpyrrolidone as reducing agent has been researched and its influence in compositions content on antimicrobial properties of last ones have been defined. The impact of temperature and polyvinylpyrrolidone content as well as Ag+ concentration on the kinetics of the reduction reaction of silver ions was determined. Silver-containing composites in the form of porous blocks and films were synthesized and their bactericidal and fungicidal properties were studied. The possibility of practical application of composites in biomedical area in the processes of osteogenesis has been confirmed.

scholarly journals Preparation and characterization of sodium alginate/acrylic acid composite hydrogels conjugated to silver nanoparticles as an antibiotic delivery system

2021 ◽  
Vol 10 (1) ◽  
pp. 860-873
Author(s):  
Parvaneh Mohamadinia ◽  
Navideh Anarjan ◽  
Hoda Jafarizadeh-Malmiri
Keyword(s):  
Silver Nanoparticles ◽  
Acrylic Acid ◽  
Sodium Alginate ◽  
Release Kinetics ◽  
Silver Ions ◽  
Optimization Analysis ◽  
Composite Hydrogels ◽  
The Impact ◽  
Kinetics Of

Abstract Hydrogels are promising drug delivery systems attributable to their unique characteristics such as high hydrophilicity, controllability, biocompatibility, and facile production routines. The aim of this research was the preparation of sodium alginate/acrylic acid (AAc) composite hydrogels conjugated to silver nanoparticles to deliver the cephalexin as a model antibiotic compound. The reduction of silver ions into silver nanoparticles as well as the stabilization of created nanoparticles ensued simultaneously with hydrogel backbone formulation during microwave irradiation and monomer cross-linking processes. The impact of AAc and silver ion concentrations and the radiation time of microwave were then investigated on the main characteristics of hydrogels. The results indicated that the hydrogels’ characteristics could be significantly predicted by studying all independent parameters through various second-order polynomial models. The multiple optimization analysis suggested that the prepared hydrogels using 7.8 g AAc and 1.5 g silver nitrate and 1 min microwave radiation could give the best hydrogels with the highest swelling degree, gel fraction, cephalexin absorption, and antibacterial activity. The morphology and either absorption or release kinetics of cephalexin by the optimum prepared hydrogels were also investigated. No significant differences between the experimental and predicted data confirmed the suitability of the suggested models.

Testing of photocatalytic potential of silver nanoparticles produced through nonthermal plasma reduction reaction and stabilized with saccharides

2021 ◽  
pp. 1-14
Author(s):  
N.U.H. Altaf ◽  
M.Y. Naz ◽  
S. Shukrullah ◽  
H.N. Bhatti
Keyword(s):  
Silver Nanoparticles ◽  
Band Gap ◽  
Light Exposure ◽  
Argon Plasma ◽  
Silver Ions ◽  
Reduction Reaction ◽  
Diameter Distribution ◽  
Light Spectrum ◽  
Plasma Reduction ◽  
Narrow Diameter Distribution

In this study, silver nanoparticles (AgNPs) were produced through an atmospheric pressure plasma reduction reaction and tested for photodegradation of methyl blue (MB) under sunlight exposure. The argon plasma born reactive species were used to reduce silver ions to AgNPs in the solution. Glucose, fructose and sucrose were also added in the solution to stabilize the growth process. The glucose stabilized reaction produced the smallest nanoparticles of 12 nm, while sucrose stabilized reaction produced relatively larger nanoparticles (14 nm). The nanoparticles exhibited rough morphology and narrow diameter distribution regardless of stabilizer type. The narrow diameter distribution and small band gap helped activating majority of nanoparticles at a single wavelength of light spectrum. The band gap energy of AgNPs varied from 2.22 eV to 2.41 eV, depending on the saccharide type. The photoluminescence spectroscopy of AgNPs produced emission peaks at 413 nm, 415 nm, and 418 nm. The photocatalytic potential of AgNP samples was checked by degrading MB dye under sunlight. The degradation reaction reached a saturation level of 98% after 60 min of light exposure.

The impact of stabilization mechanism on the aggregation kinetics of silver nanoparticles

2012 ◽  
Vol 429 ◽  
pp. 325-331 ◽  
Author(s):  
Amro M. El Badawy ◽  
Kirk G. Scheckel ◽  
Makram Suidan ◽  
Thabet Tolaymat
Keyword(s):  
Silver Nanoparticles ◽  
Aggregation Kinetics ◽  
Stabilization Mechanism ◽  
The Impact ◽  
Kinetics Of

scholarly journals A REVIEW: A GREEN APPROACH FOR THE SYNTHESIS OF SILVER NANOPARTICLES AND ITS ANTIBACTERIAL APPLICATIONS

2018 ◽  
Vol 11 (8) ◽  
pp. 74 ◽  
Author(s):  
Shyla Marjorie Haqq ◽  
Amit Chattree
Keyword(s):  
Silver Nanoparticles ◽  
Antimicrobial Properties ◽  
Nanoparticle Synthesis ◽  
Silver Ions ◽  
Multidrug Resistant ◽  
X Ray Diffraction ◽  
Green Approach ◽  
Transmission Electron ◽  
Uv Visible ◽  
Silver Nanoparticle Synthesis

  This review is based on the synthesis of silver nanoparticles (AgNPs) using a green approach which is biofabricated from various medicinal plants. AgNPs were prepared from the various parts of the plants such as the flowers, stems, leaves, and fruits. Various physiochemical characterizations were performed using the ultraviolet (UV)-visible spectroscopy, Fourier transform infrared spectroscopy, X-ray diffraction spectroscopy, transmission electron microscopy, and energy dispersive spectroscopy. AgNPs were also used to inhibit the growth of bacterial pathogens and were found to be effective against both the Gram-positive and Gram-negative bacteria. For the silver to have antimicrobial properties, it must be present in the ionized form. All the forms of silver-containing compounds with the observed antimicrobial properties are in one way or another source of silver ions. Although the antimicrobial properties of silver have been known, it is thought that the silver atoms bind to the thiol groups in enzymes and subsequently leads to the deactivation of enzymes. For the silver to have antimicrobial properties, it must be present in the ionized form. The study suggested that the action of the AgNPs on the microbial cells resulted into cell lysis and DNA damage. AgNPs have proved their candidature as a potential antibacterial against the multidrug-resistant microbes. The biological agents for synthesizing AgNPs cover compounds produced naturally in microbes and plants. Reaction parameters under which the AgNPs were being synthesized hold prominent impact on their size, shape, and application. Silver nanoparticle synthesis and their application are summarized and critically discussed in this review.

scholarly journals Green Synthesis of Silver Nanoparticles using Salacca zalacca Extract as Reducing Agent and It’s Antibacterial Activity

2019 ◽  
Vol 31 (12) ◽  
pp. 2804-2810
Author(s):  
Anti Kolonial Prodjosantoso ◽  
Oktanio Sigit Prawoko ◽  
Maximus Pranjoto Utomo ◽  
Lis Permana Sari
Keyword(s):  
Escherichia Coli ◽  
Silver Nanoparticles ◽  
Antibacterial Activity ◽  
Staphylococcus Epidermidis ◽  
Silver Ions ◽  
Reduction Reaction ◽  
Face Centered Cubic ◽  
Gram Positive Bacteria ◽  
Transmission Electron ◽  
Face Centered

In this article, the synthesis of silver nanoparticles through a reduction reaction process using Salacca zalacca extract is reported. The AgNPs were characterized using X-ray diffraction, transmission electron microscopy, Fourier transform infrared and UV-visible spectrophotometry methods. The AgNPs antibacterial activity was determined against of Gram-positive bacteria (Staphylococcus epidermidis) and Gram-negative bacteria (Escherichia coli). The main functional groups contained in Salacca zalacca extract are carbonyl, hydroxyl and nitrile groups, which are believed to reduce the silver ions to metal. The surface plasmon resonance values of brownish red AgNPs are in the range of 410 nm to 460 nm. The structure of AgNPs is face centered cubic (FCC). The diameter of silver nanoparticles crystallite is 14.2 ± 2.6 nm. The AgNPs growth inhibition zones of Escherichia coli and Staphylococcus epidermidis are 9.6 mm and 9.2 mm, respectively.

Silver Nanoparticles: Transport and Fate in the Environment

2018 ◽  
Vol 2 (08) ◽  
Author(s):  
Kayla Dean ◽  
Felicia Jefferson
Keyword(s):  
Silver Nanoparticles ◽  
Consumer Products ◽  
Engineered Nanoparticles ◽  
Practical Application ◽  
Potential Toxicity ◽  
Current State ◽  
History Analysis ◽  
Potential Risks ◽  
Analytical Tools ◽  
The Impact

Within the previous few years major advances in the development of nanotechnologies and practical application of artificial nanoparticles (NPs) and nanomaterials (NMs) have resulted. As society becomes further aware that the use of nanomaterials is ever growing in consumer products and their presence in the environment, critical interest on the impact of this emerging technology has grown. A major concern is whether the unknown risks of engineered nanoparticles, in particular, their impact on health and environment, outweighs their established benefits to society. The goal is to evaluate their potential toxicity in the environment. Silver nanoparticles exhibit an important effect on microbial processes in environmental exposures. This study provides a brief review over the current state-of-knowledge about AgNPs from various studies in this area, including the history, analysis, source, transport, fate, and potential risks of AgNPs. In order to fully investigate the transport and fate of AgNPs in the environment, appropriate methods for the pre-concentration, separation, and speciation of AgNPs should be developed, and analytical tools for the characterization and detection of AgNPs in complicated environmental studies must be incorporated.

scholarly journals Preparation And Characterization of Sodium Alginate/Acrylic Acid Composite Hydrogels Conjugated To Silver Nanoparticles As An Antibiotic Delivery System

2021 ◽  
Author(s):  
Parvaneh Mohamadinia ◽  
Navideh Anarjan
Keyword(s):  
Silver Nanoparticles ◽  
Antibacterial Activity ◽  
Acrylic Acid ◽  
Sodium Alginate ◽  
Release Kinetics ◽  
Silver Ions ◽  
Composite Hydrogels ◽  
Gel Fraction ◽  
Good Biocompatibility ◽  
The Impact

Abstract Hydrogels are specific groups of polymers that are highly swellable in aqueous solutions, despite their water-in-soluble structures. Thus, they are promising drug delivery systems attributable to their unique characteristics such as high hydrophilicity, high controllability, facile production routines and, good biocompatibility. The aim of this research was the preparation of sodium alginate/acrylic acid composite hydrogels conjugated to silver nanoparticles to deliver the cephalexin as a model antibiotic compound. The reduction of silver ions into silver nanoparticles as well as the stabilization of created nanoparticles ensued simultaneously with hydrogel backbone formulation during microwave irradiation and monomer cross-linking processes. The impact of acrylic acid and silver ions concentrations and also the radiation time of microwave were then investigated on the main characteristics of hydrogels, namely, swelling ratio, gel fraction, cephalexin load and, antibacterial activity. The results indicated that the hydrogels’ characteristics could be significantly predicted by studied all independent parameters, through various second-order polynomial models. The multiple optimization analysis suggested that the prepared hydrogels using 7.8 g acrylic acid and 1.5 g silver nitrate and 1 min microwave radiation could give the best hydrogels with the highest swelling degree, gel fraction, cephalexin absorption and, antibacterial activity. The morphology and either absorption or release kinetics of cephalexin by/from the optimum prepared hydrogels were also investigated. No significant differences between the experimental and predicted data was confirmed the suitability of the suggested models.

scholarly journals Influence of Experimental Conditions on Deposition of Silver Nanoparticles Onto Surface of Graphene Oxide / Wpływ Warunków Eksperymentalnych Na Proces Osadzania Nanocząstek Srebra Na Powierzchni Tlenku Grafenu

2015 ◽  
Vol 60 (4) ◽  
pp. 2631-2636
Author(s):  
M. Wojnicki ◽  
I. Mania ◽  
M. Marzec ◽  
M. Gajewska ◽  
K. Mech
Keyword(s):  
Silver Nanoparticles ◽  
Graphene Oxide ◽  
Alkaline Solution ◽  
Acidic Solution ◽  
Deposition Process ◽  
Reducing Agent ◽  
Experimental Conditions ◽  
Initial Concentration ◽  
The Impact

Present work describes the influence of silver nanoparticles precursor form as well as the impact of graphene oxide initial concentration on deposition of the silver nanoparticles onto graphene oxide. Borane dimethylamine complex (DMAB) was used as the reducing agent. It was observed that application of silver ammonia complexes as the silver nanoparticles precursor as well as alkaline solution effect in higher quantity of deposited AgNPs in comparison to deposition process with the use of silver(I) nitrate in acidic solution.

scholarly journals Green Synthesis of Silver Nanoparticles Using Hypericum perforatum L. Extract and Evaluation of Their Antibacterial Activity

2020 ◽  
Vol 71 (2) ◽  
pp. 273-279
Author(s):  
Daniela Gitea ◽  
Andrei Teodorescu ◽  
Carmen Pantis ◽  
Delia Mirela Tit ◽  
Alexa Florina Bungau ◽  
...  
Keyword(s):  
Silver Nanoparticles ◽  
Antibacterial Activity ◽  
Antimicrobial Properties ◽  
Silver Ions ◽  
Antimicrobial Effect ◽  
Colloidal Dispersion ◽  
Colloidal Dispersions ◽  
Application Potential ◽  
Hypericum Perforatum L ◽  
Pathogenic Agents

Silver nanoparticles (AgNPs) ranging in size from 1-100 nm show good application potential in many medical fields (therapies, medical devices, molecular diagnostics) due to their antimicrobial properties. The purpose of this study is to characterize from physicochemical perspective the colloidal dispersion obtained through phyto-synthesis. The existence of colloidal silver particles was visually highlighted through Thyndall effect. The bio-reduction of silver ions was analyzed through modern techniques, UV-VIS spectrophotometry and Hyperspectral Microscopy. After getting the colloidal dispersion, its antibacterial activity was proved by sowing on different plates the following types of pathogenic agents: Staphylococcus aureus, Escherichia coli, Pseudomonas aeruginosa. The UV-VIS spectrum for the methanolic extract with 10% H. perforatum L. and for the silver colloidal dispersions was achieved, observing a max at 455 nm. The hyperspectral images were achieved observing the shape, conformation, and the size of the obtained particles. During the antibacterial efficacy testing on those three strains of pathological agents, in all situations, the colloidal dispersion had a promising antimicrobial effect.

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