2-pyrrolidone - capped Mn3O4 nanocrystals
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AbstractWater-soluble Mn3O4 nanocrystals have been prepared through thermal decomposition in a high temperature boiling solvent, 2-pyrrolidone. The final product was characterized with XRD, SEM, TEM, FTIR and Zeta Potential measurements. Average crystallite size was calculated as ∼15 nm using XRD peak broadening. TEM analysis revealed spherical nanoparticles with an average diameter of 14±0.4 nm. FTIR analysis indicated that 2-pyrrolidone coordinates with the Mn3O4 nanocrystals only via O from the carbonyl group, thus confining their growth and protecting their surfaces from interaction with neighboring particles.
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pp. 59-66
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pp. 108
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1976 ◽
Vol 24
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pp. 484-487
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pp. 345-352
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2015 ◽
Vol 645-646
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pp. 394-399
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