Atmosphere Effect on Sintering Behaviour of Astaloy CrM and Astaloy CrL Höganäs Powders with Manganese and Carbon Additions / Wpływ Atmosfery Na Spiekalność Komercyjnych Proszków Höganäs Astaloy CrM I Astaloy CrL Z Dodatkami Manganu I Węgla

2012 ◽  
Vol 57 (4) ◽  
pp. 1001-1009 ◽  
Author(s):  
T. Pieczonka ◽  
M. Sułowski ◽  
A. Ciaś
Keyword(s):  
Chemical Composition ◽  
Sintering Temperature ◽  
Minor Effect ◽  
Sintering Atmosphere ◽  
Dimensional Changes ◽  
Atmosphere Effect ◽  
Final Density ◽  
Sintering Behaviour ◽  
Carbon Additions ◽  
Dilatometric Data

Dilatometric data for Astaloy CrM (3% Cr-0.5% Mo) and Astaloy CrL (1.5% Cr-0.2% Mo) powders with additions of 0.3% carbon and 3.0% manganese during sintering cycles up to 1120 and 1250°C in different atmospheres are reported. For comparison, also Astaloy CrM and Astaloy CrL powders were investigated. Starting with green densities of approx. 6.8 g/cm3, the final density of sintered compacts was influenced mainly by the sintering temperature, while the results showed the only minor effect of the sintering atmosphere on the final dimensional changes. However, the sintering atmosphere influences the sintering behaviour, microstructure and the final chemical composition of sintered compacts. In sintered and in the dilatometer cooled Mn-Cr-Mo-C steels predominantly bainitic structures were obtained.

scholarly journals Dilatometric investigations of Fe – Cr – Mo – C system

2018 ◽  
Vol 2 (2) ◽  
pp. 1-13
Author(s):  
Maciej Sulowski ◽  
Ewa Lichańska ◽  
Paweł Kulecki ◽  
Monika Tenerowicz-Żaba ◽  
Anna Staniek
Keyword(s):  
Carbon Content ◽  
Sintering Behavior ◽  
Density Level ◽  
Pressing Pressure ◽  
Pure Nitrogen ◽  
Sintering Atmosphere ◽  
Single Action ◽  
Dimensional Changes ◽  
Heating And Cooling ◽  
Final Density

Sintering behavior in high purity nitrogen and mixture of 5% H2-95% N2 of Fe-(Cr)-(Mo)-C system was investigated. The mixtures, differ from chromium, molybdenum and carbon content were prepared in Turbula mixer. Then, using single-action pressing in a rigid die at pressing pressure 400 MPa, green compacts with density level 5.9±0.17 g/cm3 were pressed. Sintering was carried out in a horizontal push rod dilatometer Netzsch 402E at 1120 and 1250°C for 60 min. Heating and cooling rates were 10 and 20°C/min., respectively. After heating, compacts were isothermal sintered at 1120 or 1250°C for 60 minutes an cooled up to 200°C, then isothermally hold for 60 minutes and definitely cooled to the room temperature. Pure nitrogen and mixture of 5% H2-95% N2 were employed as sintering atmospheres. During investigations the influence of isothermal sintering temperature, chemical composition of sintering atmosphere, chromium, molybdenum and carbon content was followed by dilatometry. The aim of investigations was to determine transformation temperatures. It was shown that the dimensional changes occurring during heating and isothermal sintering and the final density of sintered compacts are influenced by sintering parameters and the alloying elements concentration in powder mixture.

Effects of Sintering Conditions on Properties of a Warm Compacted Stainless Steel Powder

2012 ◽  
Vol 217-219 ◽  
pp. 483-486
Author(s):  
Mei Yuan Ke
Keyword(s):  
Tensile Strength ◽  
Stainless Steel ◽  
Sintered Density ◽  
Sintering Temperature ◽  
Steel Powder ◽  
Stainless Steel Powder ◽  
Sintering Atmosphere ◽  
Comprehensive Properties ◽  
Ammonia Atmosphere ◽  
Sintering Conditions

Effects of Sintering atmosphere and temperature on properties of warm compacted 410L stainless steel powder were studied. Sintered density, hardness, tensile strength and elongation were measured. Results showed that in order to achieve high comprehensive properties, the optimal sintering temperature was 1230°C for 410L stainless steel powder. At the same sintering temperature, density and hardness sintered in vacuum were much higher than that sintered in cracked ammonia while tensile strength sintered in cracked ammonia were much higher than that in vacuum. When sintered in vacuum at 1230°C, sintered density was 7.45 g•cm-3, hardness was 65 HRB, tensile strength was 410 MPa and elongation was 29.5%. When sintered in cracked ammonia atmosphere at 1230°C, sintered density was 7.26 g•cm-3, hardness was 97 HRB, tensile strength was 515 MPa and elongation was 3.8%.

scholarly journals Sintering behaviour and microwave dielectric properties of MgO-2B2O3-xwt%BaCu(B2O5)-ywt%H3BO3 ceramics

2021 ◽  
Author(s):  
Haiquan Wang ◽  
Shixuan Li ◽  
Kangguo Wang ◽  
Xiuli Chen ◽  
Huanfu Zhou
Keyword(s):  
Dielectric Properties ◽  
Bulk Density ◽  
Single Phase ◽  
Sintering Temperature ◽  
Microwave Dielectric Properties ◽  
X Ray Diffraction ◽  
Microwave Dielectrics ◽  
X Ray ◽  
Microwave Dielectric ◽  
Sintering Behaviour

AbstractThis study investigates the bulk density, sintering behaviour, and microwave dielectric properties of the MgO-2B2O3 series ceramics synthesised by solid-state reaction. According to the X-ray diffraction and microstructural analyses, the as-prepared MgO-2B2O3 ceramics possess a single-phase structure with a rod-like morphology. The effects of different quantities of H3BO3 and BaCu(B2O5) (BCB) on the bulk density, sintering behaviour, and microwave dielectric properties of the MgO-2B2O3 ceramics were investigated. Accordingly, the optimal sintering temperature was obtained by adding 30 wt% H3BO3 and 8 wt% BCB. We also reduced the sintering temperature to 825 °C. Furthermore, the addition of 40 wt% H3BO3 and 4 wt% BCB increased the quality factor, permittivity, and temperature coefficient of resonance frequency of MgO-2B2O3 to 44,306 GHz (at 15 GHz), 5.1, and −32 ppm/°C, respectively. These properties make MgO-2B2O3 a viable low-temperature co-fired ceramic with broad applications in microwave dielectrics.

Microstructure and Mechanical Properties Study of CoCrMo Parts Sintered under Control Atmosphere

2016 ◽  
Vol 1133 ◽  
pp. 85-89
Author(s):  
Mohamad Azmirruddin Ahmad ◽  
Fazira Suriani Mohamed Fadzil ◽  
Mazlan Mohamad ◽  
Mohamad Hasnan Abdul Hamid ◽  
Mohd Asri Selamat
Keyword(s):  
Mechanical Properties ◽  
Sintering Temperature ◽  
Inert Gases ◽  
Cobalt Chromium ◽  
Sintered Compact ◽  
Sintering Atmosphere ◽  
Knee Replacements ◽  
Powder Pressing ◽  
Cobalt Chromium Molybdenum ◽  
Bio Compatibility

Their excellent properties, such as corrosion resistance, fatigue strength and bio-compatibility, made Cobalt-chromium-molybdenum (CoCrMo) were used in total hip and knee replacements and dental devices. The green CoCrMo compacts specimens in rectangle shape were fabricated by powder pressing technique. The effects of sintering temperature and atmosphere on the mechanical properties and microstructure of the CoCrMo compacts which is sintered at 1300°C-1400°C under two different inert gases sintering atmosphere (Ar2/N2H2) were investigated. The experimental results show that the grain boundaries sizes of CoCrMo compact sintered specimen were increased with increasing sintering temperature. The CoCrMo compacts specimens sintered at 1350°C under inert gases N2H2 atmosphere possess highest density (8.096 g/cm3) and hardness (327.1Hv). However, when the compacts specimens are sintered at 1400°C, the density (7.596 g/cm3) and hardness (320 Hv) properties of sintered compact were decreased.

Aspects about Sintering Behaviour of a Titanium Hydride Powder Based Alloy Used for Automotive Components

2016 ◽  
Vol 823 ◽  
pp. 467-472
Author(s):  
Cristina Ileana Pascu ◽  
Stefan Gheorghe ◽  
Ilie Dumitru ◽  
Claudiu Nicolicescu
Keyword(s):  
Automotive Industry ◽  
Sintering Temperature ◽  
Low Cost ◽  
Test Results ◽  
Automotive Components ◽  
Titanium Hydride Powder ◽  
Powder Particles ◽  
Sintering Behaviour ◽  
High Originality ◽  
Hydride Powder

For this study with high originality, some aspects about the sintering behaviour of Titanium based alloy used for automotive components are presented. This paper presents the experimental results concerning the processing of Ti based alloy by Powder Metallurgy (PM) technology. The initial powder mixture consists in TiH2 micrometric powder particles that have been combined with some metallic powders for improving the final mechanic-chemicals and functional properties for using in the automotive industry. The classical PM route have been applied for obtaining a low-cost Ti- alloy.As a result it was compulsory to study the parameters that influence the densification process and the sintered properties, depending on the sintering temperature. The experimental test results were processed using the STATISTICA program. Therefore the influence of these sintering temperatures on the height and diameter shrinkages, density and hardness for the alloys based on Ti micrometric powders has been studied.

Influence of Thermal Treatment on YBa2Cu3O7-x Thick Films Prepared by Electrophoretic Deposition on Ni and Ag Substrates

2007 ◽  
Vol 1001 ◽  
Author(s):  
Laurent Dusoulier ◽  
Samuel Denis ◽  
Michel Dirickx ◽  
Philippe Vanderbemden ◽  
Marcel Ausloos ◽  
...  
Keyword(s):  
Thermal Treatment ◽  
Electrophoretic Deposition ◽  
Magnetic Induction ◽  
Sintering Temperature ◽  
Low Frequency ◽  
Shielding Effect ◽  
Magnetic Shielding ◽  
Chemical Contamination ◽  
Sintering Atmosphere ◽  
Ag Substrate

AbstractWe have studied the sintering parameters of YBa2Cu3O7-x (YBCO) coatings produced by electrophoretic deposition (EPD) on Ag and Ni substrates. The maximal sintering temperature is ∼ 930°C due to partial melting and chemical contamination for Ag and Ni substrates respectively. Increasing the sintering duration does not improve significantly the densification. When Ar sintering atmosphere is used, the coating density is strongly increased on Ag substrates while adhesion is poor on Ni substrates. The Ar-sintered YBCO coating deposited on planar Ag substrate displays a significant magnetic shielding effect for low frequency applied magnetic induction.

THE SUPERCONDUCTING STUDY OF TlBaCaCu2Oy

1988 ◽  
Vol 02 (09) ◽  
pp. 1095-1101
Author(s):  
JIE YAN ◽  
XIAOMING YANG ◽  
GUANGWEN PEI ◽  
ZHENYU MEN ◽  
DEYING SONG
Keyword(s):  
Sintering Temperature ◽  
X Ray Diffraction ◽  
Unit Cell Parameters ◽  
Sintering Atmosphere ◽  
X Ray ◽  
Cell Parameters ◽  
Sintering Time ◽  
Zero Resistance ◽  
Annealing Rate ◽  
The Stability

The relation of the superconductivity of TlBaCaCu 2 O y to the sintering temperature, sintering time, annealing rate and sintering atmosphere was studied. It was shown that the zero-resistance temperature of the superconductors of the type was up to 118K and the stability was to some extent quite good. Through X-ray diffraction analysis, the TlBaCaCu 2 O y was found to possess two kinds of tetragonal structures. The T co =118 K sample has the unit cell parameters of a=5.446(2)Å, c=35.698(2)Å; while for T co =93.5 K , one has the parameters of a=5.469(2)Å, c=30.051(2)Å, the substitution of Tl, Ba, Ca , by many other elements show that only TlBaMgCu 2 O y and TlMg 2 Cu 2 O y are superconductors and others are insulators.

Using NIR and ATR-FTIR spectroscopy to rapidly detect compression wood inPinus radiata

2014 ◽  
Vol 44 (7) ◽  
pp. 820-830 ◽  
Author(s):  
J. Paul McLean ◽  
Guangwu Jin ◽  
Maree Brennan ◽  
Michél K. Nieuwoudt ◽  
Philip J. Harris
Keyword(s):  
Chemical Composition ◽  
Compression Wood ◽  
Near Infrared ◽  
Water Saturation ◽  
Nir Spectroscopy ◽  
Analytical Techniques ◽  
Gradual Change ◽  
Least Squares Regression ◽  
Dimensional Changes ◽  
Discriminatory Analysis

Compression wood has undesirable properties for structural timber and for paper production. Traditional methods of detecting it are often time consuming and subjective. This study aimed to rapidly and impartially detect compression wood through the use of attenuated total reflectance Fourier transform infrared spectroscopy (ATR-FTIR) and diffuse reflectance near infrared (NIR) spectroscopy. Compression wood and non-compression wood samples were obtained from young Pinus radiata D. Don trees grown in New Zealand. Longitudinal dimensional changes were measured during drying or water saturation of the samples; lignin and galactose contents were determined using conventional analytical techniques. Chemical composition was here a more reliable discriminator between wood types than longitudinal dimensional changes. It was shown that partial least-squares regression (PLS-R) or discriminatory analysis (PLS-DA) could be used to build models on the training samples that could discriminate between wood types of the independently grown validation samples. Ultimately, both types of spectroscopies could be used to discriminate between compression wood and non-compression wood either through prediction or discriminatory analysis with equal success. Investigation into spectral differences between wood types, including sequential mixtures of wood types, showed that for the mid-IR region absorbance at a well-resolved lignin band could be used to discriminate compression wood from non-compression wood. For NIR, a similar investigation showed that absorbance values at four separate wavenumbers or the 6000–5600 cm−1region of the first derivative spectra were required for that discrimination. It is proposed that if there is a gradual change in the chemical composition of compression wood with its severity, then IR spectroscopy could feasibly be used to rapidly determine compression wood severity.

Sign in / Sign up

Export Citation Format

Share Document