Fabrication of Ni-ZrO2 Nanocomposite Coating by Electroless Deposition Technique

2020 ◽  
Vol 38 (5A) ◽  
pp. 649-655
Author(s):  
Hiba M. Algailani ◽  
Adel K. Mahmoud ◽  
Hanaa A. Al-Kaisy
Keyword(s):  
Stainless Steel ◽  
Corrosion Resistance ◽  
Electroless Deposition ◽  
Nanocomposite Coating ◽  
Nanocomposite Coatings ◽  
Zro2 Nanoparticles ◽  
Deposition Method ◽  
Deposition Technique ◽  
Stainless Steel 316L ◽  
X Ray

This work aims preparation of Ni-based nanocomposite coating by electroless deposition method onto stainless steel (316L) substrate, the present work will compare the effects of incorporation of ZrO2 nanoparticles at different percentages (1.25 wt %, 2.25 wt %, and 4.25 wt %) Ni-based electroless deposition coating of the bath nanocomposite on the phase structure, microhardness, and corrosion resistance is studied. Where the structure and chemical composition of nanocomposite coatings were studied by using (X-ray), (SEM) and (EDS). of Ni - ZrO2 nanocomposite coating exhibits much-increased microhardness and remarkably improved corrosion resistance. 

Stainless Steel 316 L Metal Coating with Capiz Shell Hydroxyapatite Using Electrophoretic Deposition Method as Bone Implant Candidate

2020 ◽  
Vol 840 ◽  
pp. 336-344
Author(s):  
Martinus Kriswanto ◽  
Muhammad Khairurrijal ◽  
Dave Leonard Junior Wajong ◽  
Tofan Maliki Kadarismanto ◽  
Yusril Yusuf
Keyword(s):  
Stainless Steel ◽  
Electrophoretic Deposition ◽  
Sintering Temperature ◽  
Deposition Method ◽  
Stainless Steel 316L ◽  
Bone Implant ◽  
X Ray ◽  
Withdrawal Speed ◽  
Stainless Steel 316 ◽  
Scanning Electron

Hydroxyapatite (HAp) made of capiz shell has been successfully coated onto stainless steel 316L substrate using electrophoretic deposition (EPD) method. In this study, three variations were applied, they were the voltages of 25 V and 50 V, the withdrawal speeds of 0.1 mm/s, 0.5 mm/s, and 1 mm/s, and the sintering temperatures of 750, 850, and 950 °C. These variations were applied to determine the differences in morphology and crystal structure of the layers so that the most suitable result was obtained as a candidate for the bone implant. Characterization was done by Scanning Electron Microscope and X-Ray Diffractometer. The EPD process and the application of sintering temperature eliminated the phase of B type apatite carbonate which made the purity of the HAp layer higher. The SEM results show that the layer was more homogeneous and free of cracking at a voltage of 50 V and the withdrawal speed of 0.1 mm/s. The layer density was higher as the voltage and sintering temperature increased. Higher sintering temperature also made the layer more homogeneous, but at 950 °C, stainless steel 316L substrate underwent a phase transformation which caused the decreasing of the purity of the HAp layer. The best results were obtained by applying a50 V voltage, a withdrawal speed of 0.1 mm/s, and a sintering temperature of 850 °C.

A study of the electrophoretic deposition of polycaprolactone-chitosan-bioglass nanocomposite coating on stainless steel (316L) substrates

2021 ◽  
pp. 088391152110635
Author(s):  
Zahra Sadeghinia ◽  
Rahmatollah Emadi ◽  
Fatemeh Shamoradi
Keyword(s):  
Stainless Steel ◽  
Surface Treatment ◽  
Electrophoretic Deposition ◽  
Deposition Time ◽  
Sol Gel ◽  
Nanocomposite Coating ◽  
Deposition Method ◽  
Stainless Steel 316L ◽  
Gel Method

In this research, bioglass nanoparticles were synthesized via sol-gel method and a polycaprolactone-chitosan-bioglass nanocomposite coating was formed on SS316L substrate using electrophoretic deposition method. Then, the effects of voltage and deposition time on morphology, thickness, roughness, and wettability of final coating were investigated. Finally, biocompatibility and toxicity of the coating were evaluated. The results showed that increase of both time and voltage enhanced the thickness, roughness, and wettability of coating. Also, increase of deposition time increased the agglomeration. Therefore, it can be concluded that voltage of 20 V and time of 10 min are suitable for the formation of a uniform agglomerate-free coating. The presence of bioglass nanoparticles also led to the increase of roughness and improvement of polycaprolactone hydrophobicity. The results also showed higher bioactivity in polycaprolactone-chitosan-1% bioglass nanocomposite coating sample. This sample had a roughness ( Ra) of 1.048 ± 0.037 μm and thickness of 2.54 ± 0.14 μm. In summary, the results indicated that coating of polycaprolactone-chitosan-bioglass nanocomposite on SS316L substrate could be a suitable surface treatment to increase its in vivo bioactivity and biocompatibility.

scholarly journals Semisolid State Sintering Behavior of Aluminum–Stainless Steel 316L Composite Materials by Powder Metallurgy

Materials ◽  
2019 ◽  
Vol 12 (9) ◽  
pp. 1473 ◽  
Author(s):  
Kwangjae Park ◽  
Dasom Kim ◽  
Kyungju Kim ◽  
Seungchan Cho ◽  
Kenta Takagi ◽  
...  
Keyword(s):  
Stainless Steel ◽  
Intermetallic Compounds ◽  
Vickers Hardness ◽  
Raw Materials ◽  
High Hardness ◽  
Engineering Industry ◽  
Sintering Behavior ◽  
Semisolid State ◽  
Stainless Steel 316L ◽  
X Ray

Aluminum (Al)-stainless steel 316L (SUS316L) composites were successfully fabricated by the spark plasma sintering process (SPS) using pure Al and SUS316L powders as raw materials. The Al-SUS316L composite powder comprising Al with 50 vol.% of SUS316L was prepared by a ball milling process. Subsequently, it was sintered at 630 °C at a pressure of 200 MPa and held for 5 min in a semisolid state. The X-ray diffraction (XRD) patterns show that intermetallic compounds such as Al13Fe4 and AlFe3 were created in the Al-SUS316L composite because the Al and SUS316L particles reacted together during the SPS process. The presence of these intermetallic compounds was also confirmed by using XRD, scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS), and EDS mapping. The mechanical hardness of the Al-SUS316L composites was analyzed by a Vickers hardness tester. Surprisingly, the Al-SU316L composite exhibited a Vickers hardness of about 620 HV. It can be concluded that the Al-SUS316L composites fabricated by the SPS process are lightweight and high-hardness materials that could be applied in the engineering industry such as in automobiles, aerospace, and shipbuilding.

Effects of Sintering Temperature on the Properties of Stainless Steel Foam

2015 ◽  
Vol 1087 ◽  
pp. 232-235
Author(s):  
Fazimah Mat Noor ◽  
N.I. Mad Rosip ◽  
Khairur Rijal Jamaludin ◽  
Sufizar Ahmad
Keyword(s):  
Stainless Steel ◽  
Average Pore Size ◽  
Vacuum Furnace ◽  
Stainless Steel 316L ◽  
Average Pore ◽  
X Ray ◽  
Replication Method ◽  
Pore Dimension ◽  
Steel Foam ◽  
Highly Porous

Foam replication method is capable of producing foams with a highly porous structure with adjustable pore dimension, shape and size. In this work, this method has been used to prepare stainless steel 316L foam and sintered at 1200°C, 1250°C and 1300°C in a vacuum furnace. The microstructure and elemental analysis of the sample were examined using scanning electron microscope (SEM) and Energy Dispersive X–Ray (EDX), while the mechanical properties of the samples was determined by using compression test. It was found that the average pore size was in the range of 330µm-350µm. The yield strength and elastic modulus are in the range of 58-66 GPa and 0.46-0.50GPa respectively.

Preparation and properties of duplex NI-P-TIO2/NI nanocomposite coatings

2019 ◽  
Vol 33 (01n03) ◽  
pp. 1940019 ◽  
Author(s):  
Weihui Zhang ◽  
Di Cao ◽  
Yanxin Qiao ◽  
Yuxin Wang ◽  
Xiang Li ◽  
...  
Keyword(s):  
Mechanical Property ◽  
Wear Resistance ◽  
Corrosion Resistance ◽  
Porous Structure ◽  
Outer Layer ◽  
Nanocomposite Coating ◽  
Nanocomposite Coatings ◽  
Coating Properties ◽  
Duplex Coating ◽  
Plating Solution

Duplex Ni-P-TiO2/Ni coatings were deposited on the brass substrate by using two baths. Ni-P-TiO2 nanocomposite coatings were electroplated as the outer layer on the Ni-plated brass substrate by adding transparent TiO2 sol (0–50 mL/L) into the Ni-P plating solution. The microstructure, mechanical property and corrosion resistance of the duplex Ni-P-TiO2/Ni nanocomposite coatings were systemically investigated. The results show that the interface of duplex coating was uniform and the adhesion between two layers was extremely good. The microhardness of duplex Ni-P-12.5 mL/L TiO2 /Ni coating was [Formula: see text]616 HV[Formula: see text] compared to [Formula: see text]539 HV[Formula: see text] of Ni-P /Ni coating and [Formula: see text]307 HV[Formula: see text] of single Ni coating. Meanwhile, the wear resistance and the corrosion resistance of the duplex nanocomposite coating have also been improved remarkably compared with single Ni coating. However, adding excessive TiO2 sol (more than 12.5 mL/L) caused the agglomeration of TiO2 nanoparticles and led to a porous structure in the outer layer, resulting in the deterioration of coating properties.

Nanocomposite Coatings on Biomedical Grade Stainless Steel for Improved Corrosion Resistance and Biocompatibility

2012 ◽  
Vol 4 (10) ◽  
pp. 5134-5141 ◽  
Author(s):  
Srinivasan Nagarajan ◽  
Marimuthu Mohana ◽  
Pitchaimuthu Sudhagar ◽  
Vedarajan Raman ◽  
Toshiyasu Nishimura ◽  
...  
Keyword(s):  
Stainless Steel ◽  
Corrosion Resistance ◽  
Nanocomposite Coatings

Zn-TiO2 and ZnNi-TiO2 Nanocomposite Coatings: Corrosion Behaviour

2010 ◽  
Vol 636-637 ◽  
pp. 1079-1083 ◽  
Author(s):  
Augusto Gomes ◽  
I. Almeida ◽  
Tania Frade ◽  
Ana C. Tavares
Keyword(s):  
Room Temperature ◽  
Corrosion Potential ◽  
Corrosion Behaviour ◽  
Pulse Method ◽  
Nanocomposite Coating ◽  
Nanocomposite Coatings ◽  
Tio2 Films ◽  
X Ray Diffraction ◽  
X Ray ◽  
Steel Electrodes

This work presents the corrosion behaviour of the as-prepared of Zn-TiO2 and ZnNi-TiO2 films in neutral Na2SO4 solution and a first attempt to correlate with their composition, morphology and structure. The films were prepared by galvanostatic pulse method onto steel electrodes, at room temperature. The X-ray diffraction study revealed that the ZnNi alloy consists of a homogenous Ni5Zn21 phase and that the preferred crystallographic orientation of Zn deposits changes in the presence of TiO2. The SEM results show that the morphology of the metallic coating is function of the metal phase composition and become more porous in the presence of 1.5 wt% TiO2.The corrosion parameters for the nanocomposite coatings were compared with those of pure Zn and ZnNi electrodeposits, and the ZnNi-TiO2 nanocomposite coating shows the less cathodic corrosion potential.

Electropolishing of 316L Stainless Steel Using Sulfuric Acid-Free Electrolyte

2019 ◽  
Vol 141 (10) ◽  
Author(s):  
Wei Han ◽  
Fengzhou Fang
Keyword(s):  
Stainless Steel ◽  
Corrosion Resistance ◽  
Sulfuric Acid ◽  
Phosphoric Acid ◽  
Photoelectron Spectroscopy ◽  
316L Stainless Steel ◽  
Electrochemical Analysis ◽  
Limiting Current ◽  
Plateau Region ◽  
X Ray

Abstract The study is to investigate the electropolishing characteristics of 316L stainless steel in a sulfuric acid-free electrolyte of phosphoric acid and glycerol and to explore the possibility of using this eco-friendly electrolyte instead of the widely used sulfuric acid-based electrolyte. The influences of process parameters on polishing effects and the corrosion resistance of electropolished samples are investigated. The experimental results show that the electropolishing temperature and acid concentration are directly related to the mass transport mechanism in the limiting current plateau region. The grain boundaries of workpiece were electrochemically dissolved faster than the grain themselves at the beginning of the electropolishing process because they are more reactive than grains. Moreover, the conventional sulfuric—phosphoric acid electrolyte was also used to electropolish the 316L stainless steel, and the electropolished surfaces were compared with the sulfuric acid-free electrolyte proposed in this study. When the sulfuric acid-free electrolyte was used to electropolish the 316L stainless steel, the X-ray photoelectron spectroscopy (XPS) analysis shows that atomic Cr/Fe ratio of 316L stainless steel was increased from 0.802 to 1.909 after electropolishing process in the sulfuric acid-free electrolyte of phosphoric acid and glycerol. The corrosion resistance of the electropolished 316L stainless steel is studied using electrochemical analysis, and the results are verified experimentally.

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