scholarly journals Effect of Ageing on the Tracking Characteristics of High-Temperature Vulcanized Silicone Rubber Hybrid Composites for High Voltage Insulation

Materials ◽  
2020 ◽  
Vol 13 (10) ◽  
pp. 2242 ◽  
Author(s):  
Mohamed Ghouse Shaik ◽  
Vijayarekha Karuppaiyan

Micro-sized aluminum trihydrate (ATH) filled silicone rubber is useful as insulation in the electric power system. The addition of nanofillers can improve further, its overall performance. However, the degradation of such silicone insulator due to ageing has not yet been thoroughly analysed. Motivated by this, an investigation was done to observe the effect of ageing on the tracking, and the material characteristics of SiO2 nanofillers added micro-sized ATH-filled Silicone rubber. For this, the samples were prepared using different weight percentage of SiO2 nanofillers and were thermally-aged and water-aged in the laboratory environment. A well-regulated tracking-test setup was assembled, and the leakage current characteristics of the fresh, thermal-aged and water-aged samples were observed, as per international electro technical commission standard (IEC) 60,587. After tracking, the surface morphology of these samples was studied using scanning electron microscopy (SEM). Further, energy dispersive X-ray analysis (EDAX) was carried out to observe the elements present at the surface and, Fourier transform infra-red (FTIR) spectroscopy was conducted to study the changes in the chemical structure. Investigations through the leakage current, SEM, EDAX and FTIR revealed that the addition of nanofillers improved the tracking characteristics of the aged hybrid composite insulation samples, thereby minimising any early failures.

Energies ◽  
2019 ◽  
Vol 12 (12) ◽  
pp. 2401 ◽  
Author(s):  
Youngtaek Jeon ◽  
Shin-Ki Hong ◽  
Myungchin Kim

It is necessary for polymeric materials to have superior tracking resistance against various stress conditions for outdoor applications. In this study, the effect of nano-sized alumina tri-hydrate (ATH) particles on the tracking resistance of silicone rubber (SiR) is studied. Specimens with filler loadings of 1, 3, 5, 10, and 20 wt % are used for performance characterization. From the inclined plane test (IPT) results, apparent improvement in tracking resistance was achieved by mixing 3 wt % of nano-sized fillers, compared to unfilled specimens. ATH/SiR nanocomposites with 5 wt % loading showed comparable tracking performance to SiO2/SiR microcomposites with 20 wt % loading. For detailed analysis, measurements of surface contact angle (SCA) and surface leakage current, and thermo-gravimetric analysis (TGA) were performed. As the nano-ATH filler concentration increased, both thermal stability and leakage current characteristics were improved. Such results agreed with the tracking resistance performance by showing that thermal decomposition and surface charge transport is inhibited in ATH/SiR nanocomposites. Furthermore, performance improvement in nanocomposites was achieved, even at low filler loadings, compared to microcomposites. Meanwhile, the change in SCA was found to be rather limited, regardless of filler loading and filler size.


2021 ◽  
pp. 096739112199290
Author(s):  
N Rasana ◽  
K Jayanarayanan ◽  
Krishna Prasad Rajan ◽  
Aravinthan Gopanna

Multiscale hybrid composites were prepared using varying weight percentages (0 to 5) of multiwalled carbon nanotubes (MWCNTs) as nanofiller and a fixed weight percentage (20) of short glass fibres as micro filler (in polypropylene (PP) matrix. The shear and extensional viscosity of the composites was measured using a capillary rheometer. It was observed that even at higher shear rates the synergism of micro and nanofillers in the matrix significantly enhanced the melt viscosity. The complex nanotube network entanglement with micro fillers and PP chains imparted restrictions to the polymer chain movements. The prepared samples were subjected to thermal ageing at 100°C for 4 days in hot air oven. After ageing, multiscale composite with 3 wt% MWCNTs exhibited 28.57% enhancement in strain at break, whereas the tensile strength and modulus reduced by 6.8% and 8% respectively. The fracture toughness properties like strain energy release rate and critical stress intensity factor were not affected for multiscale composite at the optimum content of 3 wt% MWCNT, even after thermal ageing.


Author(s):  
D. S. Sai Ravi Kiran ◽  
Alavilli Sai Apparao ◽  
Vempala GowriSankar ◽  
Shaik Faheem ◽  
Sheik Abdul Mateen ◽  
...  

This paper investigates the machinability characteristics of end milling operation to yield minimum tool wear with the maximum material removal rate using RSM. Twenty-seven experimental runs based on Box-Behnken Design of Response Surface Methodology (RSM) were performed by varying the parameters of spindle speed, feed and depth of cut in different weight percentage of reinforcements such as Silicon Carbide (SiC-5%, 10%,15%) and Alumina (Al2O3-5%) in alluminium 7075 metal matrix. Grey relational analysis was used to solve the multi-response optimization problem by changing the weightages for different responses as per the process requirements of quality or productivity. Optimal parameter settings obtained were verified through confirmatory experiments. Analysis of variance was performed to obtain the contribution of each parameter on the machinability characteristics. The result shows that spindle speed and weight percentage of SiC are the most significant factors which affect the machinability characteristics of hybrid composites. An appropriate selection of the input parameters such as spindle speed of 1000 rpm, feed of 0.02 mm/rev, depth of cut of 1 mm and 5% of SiC produce best tool wear outcome and a spindle speed of 1838 rpm, feed of 0.04 mm/rev, depth of cut of 1.81 mm and 6.81 % of SiC for material removal rate.


2001 ◽  
Vol 685 ◽  
Author(s):  
Won-Jae Lee ◽  
Chang-Ho Shin ◽  
In-Kyu You ◽  
Il-Suk Yang ◽  
Sang-Ouk Ryu ◽  
...  

AbstractThe SrTa2O6 (STO) thin films were prepared by plasma enhanced atomic layer deposition (PEALD) with alternating supply of reactant sources, Sr[Ta(C2H5O)5(C4H10NO)]2 {Strontium bis-[tantalum penta-ethoxide dimethyllaminoethoxide]; Sr(Ta(OEt)5▪dmae)2} and O2plasma. It was observed that the uniform and conformal STO thin films were successfully deposited using PEALD and the film thickness per cycle was saturated at about 0.8 nm at 300°C. Electrical properties of SrTa2O6 (STO) thin films prepared on Pt/SiO2/Si substrates with annealing temperatures have been investigated. While the grain size and dielectric constant of STO films increased with increasing annealing temperature, the leakage current characteristics of STO films slightly deteriorated. The leakage current density of a 40nm-STO film was about 5×10−8A/cm2 at 3V.


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