scholarly journals Strength and Fracture Mechanism of an Ultrafine-Grained Austenitic Steel for Medical Applications

Materials ◽  
2021 ◽  
Vol 14 (24) ◽  
pp. 7739
Author(s):  
Gennadiy V. Klevtsov ◽  
Ruslan Z. Valiev ◽  
Natal’ya A. Klevtsova ◽  
Maxim N. Tyurkov ◽  
Mikhail L. Linderov ◽  
...  

In this paper, we study the corrosion-resistant austenitic steel Fe-0.02C-18Cr-8Ni for medical applications. The microstructure and mechanical properties (tensile mechanical properties, torsional strength, impact toughness, and static and cyclic crack resistance) under different types of loading of the steel are investigated. The results are compared for the two states of the steel: the initial (coarse-grained) state and the ultrafine-grained state produced by severe plastic deformation processing via equal-channel angular pressing. It is demonstrated that the ultrafine-grained steel 0.08C-18Cr-9Ni has essentially better properties and is very promising for the manufacture of medical products for various applications that experience various static and cyclic loads during operation.

2005 ◽  
Vol 20 (2) ◽  
pp. 288-291 ◽  
Author(s):  
Y.H. Zhao ◽  
X.Z. Liao ◽  
Y.T. Zhu ◽  
R.Z. Valiev

Highest strength for 7075 Al alloy was obtained by combining the equal-channel-angular pressing (ECAP) and natural aging processes. The tensile yield strength and ultimate strength of the ECAP processed and naturally aged sample were 103% and 35% higher, respectively, than those of the coarse-grained 7075 Al alloy counterpart. The enhanced strength resulted from high densities of Guinier–Preston (G-P) zones and dislocations. This study shows that severe plastic deformation has the potential to significantly enhance the mechanical properties of precipitate hardening 7000 series Al alloys.


2016 ◽  
Vol 879 ◽  
pp. 1317-1322 ◽  
Author(s):  
Anna Mogucheva ◽  
Diana Yuzbekova ◽  
Tatiana Lebedkina ◽  
Mikhail Lebyodkin ◽  
Rustam Kaibyshev

The paper reports on the effect of severe plastic deformation on mechanical properties of an Al-4.57Mg-0.35Mn-0.2Sc-0.09Zr (in wt. pct.) alloy processed by equal channel angular pressing followed by cold rolling (CR). The sheets of the 5024 alloy with coarse grained (CG) structure exhibited a yield stress (YS) near 410 MPa and an ultimate tensile strength (UTS) of 480 MPa, while the YS and UTS of this material with ultrafine-grained (UFG) structure increased to 530 and 560 MPa, respectively. On the other hand, the elongation to failure decreased by a factor of 2 and 4 after CR and CR following ECAP, respectively. It was shown that dislocation strengthening attributed to extensive CR plays a major role in achieving high strength of this alloy. Besides these macroscopic characteristics, jerky flow caused by the Portevin-Le Chatelier (PLC) instability of plastic deformation was examined. The formation of UFG structure results in a transition from mixed type A+B to pure type B PLC serrations. No such effect on the serrations type was observed after CR.


2006 ◽  
Vol 503-504 ◽  
pp. 663-668 ◽  
Author(s):  
Jing Tao Wang ◽  
Zhong Ze Du ◽  
Feng Kang ◽  
Guang Chen

Pure copper (99.98%wt) square bars (32x32 mm) were processed by equal channel angular pressing (ECAP) Microstructure evolution was characterized by microscopy. Room temperature mechanical properties were obtained by tensile and micro-hardness tests. With increasing number of ECAP passes and cold rolling reductions, the initial coarse grained structure in the as-received material was transformed gradually into an ultrafine grained microstructure with an average grain size of 0.2~0.3 μm. Subsequent rolling resulted deformation twining in this ultrafine grained microstructure, which gives further strengthening in addition to the strengthening obtained by ECAP. Property anisotropy in three orthogonal directions of samples processed by ECAP was characterized by tensile testing.


2004 ◽  
Vol 821 ◽  
Author(s):  
Yonghao Zhao ◽  
Xiaozhou Liao ◽  
Ruslan Z. Valiev ◽  
Yuntian T. Zhu

AbstractEqual-channel angular pressing (ECAP) processed ultrafine grained (UFG) and coarse grained (CG) 7075 Al alloys were treated by natural aging and T651 temper (annealed at 120 °C for 48 h in Ar atmosphere), respectively. Mechanical tests showed that for the UFG sample, the natural aging resulted in the highest strength (the ultimate tensile strength is 720 MPa). In contrast, for the CG sample, the T651 treatment resulted in a higher strength (the ultimate strength is 590 MPa) than the natural aging (530 MPa). Microstructural analyses indicated that the enhanced strength of the T651 treated CG sample was mainly caused by high densities of G- P zones and metastable η' precipitates. The enhanced strength of the naturally aged UFG sample was mainly caused by the high densities of G-P zones and dislocations. Upon T651 treatment, the dislocation density of the UFG sample deceased significantly, overcompensating the precipitation strengthening.


2015 ◽  
Vol 60 (2) ◽  
pp. 605-614 ◽  
Author(s):  
T. Kvačkaj ◽  
A. Kováčová ◽  
J. Bidulská ◽  
R. Bidulský ◽  
R. Kočičko

AbstractIn this study, static, dynamic and tribological properties of ultrafine-grained (UFG) oxygen-free high thermal conductivity (OFHC) copper were investigated in detail. In order to evaluate the mechanical behaviour at different strain rates, OFHC copper was tested using two devices resulting in static and dynamic regimes. Moreover, the copper was subjected to two different processing methods, which made possible to study the influence of structure. The study of strain rate and microstructure was focused on progress in the mechanical properties after tensile tests. It was found that the strain rate is an important parameter affecting mechanical properties of copper. The ultimate tensile strength increased with the strain rate increasing and this effect was more visible at high strain rates$({\dot \varepsilon} \sim 10^2 \;{\rm{s}}^{ - 1} )$. However, the reduction of area had a different progress depending on microstructural features of materials (coarse-grained vs. ultrafine-grained structure) and introduced strain rate conditions during plastic deformation (static vs. dynamic regime). The wear behaviour of copper was investigated through pin-on-disk tests. The wear tracks examination showed that the delamination and the mild oxidational wears are the main wear mechanisms.


2008 ◽  
Vol 584-586 ◽  
pp. 182-187
Author(s):  
Lilia Kurmanaeva ◽  
Yulia Ivanisenko ◽  
J. Markmann ◽  
Ruslan Valiev ◽  
Hans Jorg Fecht

Investigations of mechanical properties of nanocrystalline (nc) materials are still in interest of materials science, because they offer wide application as structural materials thanks to their outstanding mechanical properties. NC materials demonstrate superior hardness and strength as compared with their coarse grained counterparts, but very often they possess a limited ductility or show low uniform elongation due to poor strain hardening ability. Here, we present the results of investigation of the microstructure and mechanical properties of nc Pd and Pd-x%Ag (x=20, 60) alloys. The initially coarse grained Pd-x% Ag samples were processed by high pressure torsion, which resulted in formation of homogenous ultrafine grain structure. The increase of Ag contents led to the decrease of the resulted grain size and change in deformation behavior, because of decreasing of stacking fault energy (SFE). The samples with larger Ag contents demonstrated the higher values of hardness, yield stress and ultimate stress. Remarkably the uniform elongation had also increased with increase of strength.


2006 ◽  
Vol 503-504 ◽  
pp. 31-36 ◽  
Author(s):  
Johannes Mueller ◽  
Karsten Durst ◽  
Dorothea Amberger ◽  
Matthias Göken

The mechanical properties of ultrafine-grained metals processed by equal channel angular pressing is investigated by nanoindentations in comparison with measurements on nanocrystalline nickel with a grain size between 20 and 400 nm produced by pulsed electrodeposition. Besides hardness and Young’s modulus measurements, the nanoindentation method allows also controlled experiments on the strain rate sensitivity, which are discussed in detail in this paper. Nanoindentation measurements can be performed at indentation strain rates between 10-3 s-1 and 0.1 s-1. Nanocrystalline and ultrafine-grained fcc metals as Al and Ni show a significant strain rate sensitivity at room temperature in comparison with conventional grain sized materials. In ultrafine-grained bcc Fe the strain rate sensitivity does not change significantly after severe plastic deformation. Inelastic effects are found during repeated unloading-loading experiments in nanoindentations.


2013 ◽  
Vol 803 ◽  
pp. 226-229
Author(s):  
Da Ran Fang ◽  
Chun Liu ◽  
Feng Fang Liu

Al-3.9wt.%Cu alloy was subjected to equal channel angular pressing (ECAP) and subsequent low temperature annealing treatment, and the corrosion resistance of the samples was investigated by potentiodynamic polarization measurements in 3.5% NaCl solution. The results show that the corrosion rate of the ultrafine-grained alloy increases, in comparison with the coarse-grained alloy. Meanwhile, it is noted that the corrosion resistance of the alloy subjected to ECAP can be improved by relief annealing.


2008 ◽  
Vol 43 (23-24) ◽  
pp. 7409-7417 ◽  
Author(s):  
Matthias Hockauf ◽  
Lothar W. Meyer ◽  
Daniela Nickel ◽  
Gert Alisch ◽  
Thomas Lampke ◽  
...  

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