scholarly journals High-Temperature Precipitation Design-of-Experiments Simulation in Low-Alloy Cr–Mo–Ni Hot Forging Steel

Metals ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 1054
Author(s):  
Roberto Gonzalez-Ojeda ◽  
Octavio Lozada-Flores ◽  
Gonzalo Gonzalez-Reyes ◽  
Jose Manuel Sanchez-Moreno

The role of alloying elements such as Cr, Mo and Mn on low-alloy 8620 steel during hot forging operations is not yet clear, as, during deformation in the 1000~1100 °C temperature range, the austenite grain size remains small, ensuring the capacity of the forged part to be subsequently modified by surface hardening procedures. This work analyzed a deformed bar considering hardness at different geometry zones, along with SEM and TEM microstructures of previous austenite grains and lamellar martensite spacing. Moreover, Thermocalc simulations of M7C3, M23C6 and MnS precipitation were combined with Design of Experiments (DOE) in order to detect the sensitivity and significant variables. The values of the alloying elements’ percentages were drastically modified, as nominal values did not produce precipitation, and segregation at the austenite matrix may have been responsible for short-term, nanometric precipitates producing grain growth inhibition.

2020 ◽  
Vol 837 ◽  
pp. 74-80
Author(s):  
Jun Yuan ◽  
Zhen Yu Han ◽  
Yong Deng ◽  
Da Wei Yang

In view of the special requirements of rails to ensure the safe and stable operation of Railways in China, the formation characteristics of austenite grains in high carbon rail are revealed through industrial exploration, the process of industrial rail heating and rolling is simulated, innovative experimental research methods such as different heating and heat treatment are carried out on the actual rails in the laboratory. Transfer characteristics of austenite grain size, microstructures and key properties of high carbon rail during the process are also revealed. The results show that the austenite grain size of industrial produced U75V rail is about 9.0 grade. When the holding temperature is increased from 800 C to 1300 C, the austenite grain size of high carbon rail steel decreases, the austenite grain are gradually coarsened, and the tensile strength increases slightly. The tensile strength is affected by the heating temperature. With the increase of heating temperature, the elongation and impact toughness of high carbon rail decrease. The heating temperature of high carbon rail combined with austenite grain size shows that the heating temperature has a great influence on austenite grain size, and has the most obvious influence on the toughness of high carbon rail.


Materials ◽  
2020 ◽  
Vol 14 (1) ◽  
pp. 15
Author(s):  
Łukasz Poloczek ◽  
Łukasz Rauch ◽  
Marek Wilkus ◽  
Daniel Bachniak ◽  
Władysław Zalecki ◽  
...  

The paper describes physical and numerical simulations of a manufacturing process composed of hot forging and controlled cooling, which replace the conventional heat treatment technology. The objective was to investigate possibilities and limitations of the heat treatment with the use of the heat of forging. Three steels used to manufacture automotive parts were investigated. Experiments were composed of two sets of tests. The first were isothermal (TTT) and constant cooling rate (CCT) dilatometric tests, which supplied data for the identification of the numerical phase transformation model. The second was a physical simulation of the sequence forging-cooling on Gleeble 3800, which supplied data for the validation of the models. In the numerical part, a finite element (FE) thermal-mechanical code was combined with metallurgical models describing recrystallization and grain growth during forging and phase transformations during cooling. The FE model predicted distributions of the temperature and the austenite grain size in the forging, which were input data for further simulations of phase transformations during cooling. A modified JMAK equation was used to calculate the kinetics of transformation and volume fraction of microstructural constituents after cooling. Since the dilatometric tests were performed for various austenitization temperatures before cooling, it was possible to include austenite grain size as a variable in the model. An inverse algorithm developed by the authors was applied in the identification procedure. The model with optimal material parameters was used for simulations of hot forging and controlled cooling in one of the forging shops in Poland. Distributions of microstructural constituents in the forging after cooling were calculated. As a consequence, various cooling sequences during heat treatment could be analyzed and compared.


2019 ◽  
Vol 944 ◽  
pp. 357-363
Author(s):  
Xiao Dong Zhang ◽  
Dian Xiu Xia ◽  
Shou Ren Wang

The effect of austenitizing temperature on the quenching microstructure and properties of 51CrV4 steel was studied. The results show that with the increase of austenitizing temperature, the austenite grains grow gradually. After quenching, the hardness increased first and then decreased, and the strength increased first and then decreased after tempering at 460°C. When the austenitizing temperature was 880°C, the austenite grains were fine and uniform, about 16μm, the martensite structure was dense, the strength and hardness reached maximum. When the austenitizing temperature was 910°C, the decarburization phenomenon was obvious, and the strength, hardness and plasticity of the test steel decreased obviously. When the austenitizing temperature exceeded 910°C, the austenite grains grow sharply and some grains were abnormally coarse. The austenite grain size reached 20μm and the microstructure was coarser at austenitizing temperature of 950°C. Therefore, in order to ensure uniform grain size and no decarburization under the premise of complete austenitization, the best austenitizing temperature of 51CrV4 steel for good properties is 880°C.


Metals ◽  
2018 ◽  
Vol 8 (12) ◽  
pp. 988 ◽  
Author(s):  
Liangyun Lan ◽  
Zhiyuan Chang ◽  
Penghui Fan

The simulation welding thermal cycle technique was employed to generate different sizes of prior austenite grains. Dilatometry tests, in situ laser scanning confocal microscopy, and transmission electron microscopy were used to investigate the role of prior austenite grain size on bainite transformation in low carbon steel. The bainite start transformation (Bs) temperature was reduced by fine austenite grains (lowered by about 30 °C under the experimental conditions). Through careful microstructural observation, it can be found that, besides the Hall–Petch strengthening effect, the carbon segregation at the fine austenite grain boundaries is probably another factor that decreases the Bs temperature as a result of the increase in interfacial energy of nucleation. At the early stage of the transformation, the bainite laths nucleate near to the grain boundaries and grow in a “side-by-side” mode in fine austenite grains, whereas in coarse austenite grains, the sympathetic nucleation at the broad side of the pre-existing laths causes the distribution of bainitic ferrite packets to be interlocked.


Author(s):  
Sebastian Gnapowski ◽  
Elżbieta Kalinowska- Ozgowicz ◽  
Mariusz Sniadkowski ◽  
Aleksandra Pietraszek

This paper presents the results of investigations of the effects of hot deformation parameters in compression investigation on the austenite grain size in HSLA steel (0.16% C, 0.037% Nb, 0.004% Ti, 0.0098% N). The axisymmetric compression investigations were performed on cylindrical investigation specimens of d=1.2 using the Gleeble 3800 simulator. The strain rate=1s-1÷15.9s-1 and strain degree ε=1.2. Before deformation, the research specimens were austenitized at TA = 1100 ÷ 1250 °C. Metallographic observations of the primary austenite grains were conducted with an optical microscope, while the structure of dynamically recrystallized austenite, inherited by martensite, was examined by EBSD technique using a scanning electron microscope. Based on the analysis of investigation results, it was found that the size of dynamically recrystallized austenite grains in HSLA steel were clearly affected by hot compression parameters. In contrast, no significant impact of austenitising temperature on their size was found.


2020 ◽  
Vol 299 ◽  
pp. 482-486
Author(s):  
Mikhail V. Maisuradze ◽  
Maksim A. Ryzhkov

The high strength silicon steel HY-TUF, applied for manufacturing of the heavy loaded aerospace and engineering parts, was investigated. The effect of the heating temperature in the range 900...1000 °C on the austenite grain size was studied. The steel under consideration had a significant scatter of the austenite grain size. The most intensive growth of the austenite grains was observed in the temperature range 975...1000 °C.


2014 ◽  
Vol 1063 ◽  
pp. 28-31
Author(s):  
Kuan Hui Hu ◽  
Xiang Dong Liu ◽  
Guan Wen Feng ◽  
Rong Dong Han

Strength, microstructure and austenitic grain size of a hot formed steel WHT1300HF after simulative hot stamping were studied by using universal testing machine for materials and optical microscopy. The results show that the yield strength of the hot stamping parts presented the tendency of earlier decrease and later increase with the extension of holding time, tensile strength was first reduced and then hold above 1400 MPa. In addition, the microstructure of the hot stamping parts was lath martensite, and martensite lath length and packet width increases with the heating temperature increased from 850 °C to 1050 °C. Especially, the effect of heat temperature on the original austenite grain size was more obvious, such as the austenite grains grew up quickly with the increase of heating temperature, and the original austenite grain diameter was 37.8 μm when the temperature reached 1050 °C.


2009 ◽  
Vol 289-292 ◽  
pp. 109-117 ◽  
Author(s):  
Mohamad Esmailian

The effect of austenite grain size on the austenite to ferrite transformation temperature and different ferrite morphologies and growth behaviour in one Nb-microalloyed (HSLA) steel has been investigated. Three different austenite grain sizes were selected and cooled for obtaining austenite to ferrite and growth behaviour of ferrite. Moreover, samples with specific austenite grain size have been quenched, partially, for investigation of the microstructural evolution. The optical microscopy observation suggested that the nucleation site of ferrite is on edge and inside of austenite grains in Nb- microalloyed steels. Micrographs of different ferrite morphologies show that at high temperatures, where diffusion rates are higher, grain boundary ferrite nucleates both at the edge and corner of austenite grains and grows into both austenite grains. As the temperature is lowered and the driving force for ferrite formation increases, intragranular sites inside the austenite grains become operative as nucleation sites and suppress the grain boundary ferrite growth. With more undercooling,intragranular ferrites are seen to nucleate and grow more extensively , indicating the beginning of displacive transformation. Furthermore, growth rate of intragranular ferrite shows that by increasing of austenite grain size, the growth rate of intragranular ferrite increases extensively and growth rate of grain boundary ferrite decreases. The growth kinetics of grain boundary ferrite shows that this transformation is controlled by the diffusion of carbon in the austenite ahead of the interface.


2015 ◽  
Vol 817 ◽  
pp. 731-735
Author(s):  
Peng Yu ◽  
Lin Zhang ◽  
Lin Xiu Du ◽  
Jun Hu

We use the cellular automaton (CA) modeling to investigate the ferrite nucleation on the austenite grains. On the basis of the thermodynamics and kinetics of phase transformation from austenite to ferrite, the CA modeling demonstrates that the size of nucleated ferrite grains is increased with increasing of cooling rates, and nucleation process is finished instantly at a given cooling rate. The initial austenite grain size plays an important role in the obtained ferrite nucleation number, and the potential nucleation cells are increased.


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