scholarly journals Investigation of the Effect of Nano Particles on Visco-elastic Behaviour of CFRP Hybrid Nanocomposites

2020 ◽  
Vol 13 (3) ◽  
Author(s):  
Shailesh D. Ambekar ◽  
Vipin K. Tripathi
Keyword(s):  
Storage Modulus ◽  
Loss Modulus ◽  
Dynamic Mechanical Properties ◽  
Mechanical Analysis ◽  
Considerable Change ◽  
Hybrid Nanocomposites ◽  
Nano Particles ◽  
Experimental Result ◽  
Elastic Behaviour ◽  
Dynamic Mechanical

The aim of the study is to do an experimental analysis and investigation of visco-elastic behaviour of CFRP hybrid nanocomposites, which contains the small percentage of nanoclay and nanoZnO particles mixed for the improvement in the various properties of the CFRP composites. Also there is try to focus on the combined effect of another variable, i.e., fiber angle of orientation along with changing the percentage of nano particles.A hand layup method followed by process of vacuum bagging was used to make the samples of composite. Dynamic mechanical analyzer (DMA) was used to inspect the dynamic mechanical properties of CFRP hybrid nanocomposite specimens with changing temperature. The OVAT analysis is carried out for three mentioned variables and studied effect of variables on the various visco elastic properties like flexural storage modulus, loss modulus, Glass transition temperature and tan etc. It is found that due to the presence of nano particles there is tremendous change in the value of storage modulus ,it gets almost doubled, i.e., 200%because of the presence of nano particles. The experimental result also shows the positive effect on the loss modulus because of the nano particle contribution .Similarly there is considerable change in GTT(Glass transmission temperature) and change in length in DMA (Dynamic mechanical analysis ).

Effects of Nano-Silica Addition and Reactive Diluent Addition on Dynamic Mechanical Properties of Epoxy Nanocomposites

2013 ◽  
Vol 853 ◽  
pp. 46-52
Author(s):  
Huey Ling Chang ◽  
Chih Ming Chen
Keyword(s):  
Glass Transition ◽  
Transition Temperature ◽  
Glass Transition Temperature ◽  
Storage Modulus ◽  
Loss Modulus ◽  
Dynamic Mechanical Properties ◽  
Mechanical Analysis ◽  
Reactive Diluent ◽  
Dynamic Mechanical ◽  
Silica Nanopowder

Epoxy resin nanocomposite samples containing 0~3wt.% reactive diluent and 0~3wt.% silica nanopowder are prepared. The preparation process is presented for solvent-free and greenmanufacturing. The storage modulus, loss modulus and glass transition temperature of the various samples are then evaluated via Dynamic Mechanical Analysis (DMA). For samples containing 0wt.% and 3wt.% reactive diluent, respectively, 3wt.% nanoSiO2 addition is found to increase the storage modulus by 51.06 % and 22.22 %, respectively. In addition, it is found that the loss modulus is determined principally by the level of SiO2 addition, whereas the glass transition temperature is determined mainly by the level of reactive diluent addition.

Dynamic mechanical behaviour of kevlar and carbon-kevlar hybrid fibre reinforced polymer composites

2020 ◽  
pp. 095440622097060
Author(s):  
Pragati Priyanka ◽  
Harlal Singh Mali ◽  
Anurag Dixit
Keyword(s):  
Glass Transition ◽  
Transition Temperature ◽  
Glass Transition Temperature ◽  
Dynamic Mechanical Analysis ◽  
Storage Modulus ◽  
Composite Laminates ◽  
Mechanical Analysis ◽  
Textile Composites ◽  
Elastic Behaviour ◽  
Dynamic Mechanical

Comprehensive experimental results of dynamic mechanical analysis (DMA) of polymer reinforced textile composites are presented in the current investigation. Plain and 2x2 twill woven multilayer fabrics of monolithic kevlar and hybrid carbon-kevlar (C-K) are reinforced into the thermoset polymer matrix. Kevlar/epoxy and C-K/epoxy composite laminates are fabricated using an in-house facility of the vacuum-assisted resin infusion process. Variation of the visco-elastic behaviour (storage modulus, damping factor and glass transition temperature, Tg) along with time, temperature and frequency is studied for the composites. Dynamic mechanical analysis is performed under temperature sweep with frequency ranging from 1-50 Hz. Results depict the effect of inter yarn hybridisation of carbon with kevlar yarns on the storage modulus, damping performance, and creep behaviour of dry textile composites. Temperature swept dynamic characterisation is also performed to evaluate the degradation and damping performance of the composite laminates soaked in the deionised water at glass transition temperature Tg, ½ Tg, and ¾ Tg. The morphological study has been performed post the dynamic mechanical analysis using field emission scanning electron microscope.

scholarly journals Dynamic Mechanical Properties of Hybrid Layered Silicates/Kaolin Geopolymer Filler in Epoxy Composites

2017 ◽  
Vol 54 (3) ◽  
pp. 543-545 ◽  
Author(s):  
Yusrina Mat Daud ◽  
Kamarudin Hussin ◽  
Azlin Fazlina Osman ◽  
Che Mohd Ruzaidi Ghazali ◽  
Mohd Mustafa Al Bakri Abdullah ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
High Speed ◽  
Hybrid Composites ◽  
Loss Modulus ◽  
Dynamic Mechanical Properties ◽  
Mechanical Analysis ◽  
Layered Silicates ◽  
Epoxy Composites ◽  
Damping Factor ◽  
Dynamic Mechanical

Preparation epoxy based hybrid composites were involved kaolin geopolymer filler, organo-montmorillonite at 3phr by using high speed mechanical stirrer. A mechanical behaviour of neat epoxy, epoxy/organo-montmorillonite and its hybrid composites containing 1-8phr kaolin geopolymer filler was studied upon cyclic deformation (three-point flexion mode) as the temperature is varies. The analysis was determined by dynamic mechanical analysis (DMA) at frequency of 1.0Hz. The results then expressed in storage modulus (E�), loss modulus (E�) and damping factor (tan d) as function of temperature from 40 oC to 130oC. Overall results indicated that E�, E�� and Tg increased considerably by incorporating optimum 1phr kaolin geopolymer in epoxy organo-montmorillonite hybrid composites.

Thermal stability and dynamic mechanical behavior of functional multiphase boride ceramics/epoxy composites

2019 ◽  
Vol 39 (6) ◽  
pp. 508-514
Author(s):  
Yannan He ◽  
Zhiqiang Yu
Keyword(s):  
Mechanical Properties ◽  
Thermal Stability ◽  
Loss Modulus ◽  
Dynamic Mechanical Properties ◽  
Mechanical Analysis ◽  
Epoxy Composites ◽  
Scanning Calorimetry ◽  
Element Analysis ◽  
Reaction Heat ◽  
Dynamic Mechanical

Abstract The thermal and dynamic mechanical properties of epoxy composites filled with zirconium diboride/nano-alumina (ZrB2/Al2O3) multiphase particles were investigated by means of differential scanning calorimetry, dynamic thermo-mechanical analysis, and numerical simulation. ZrB2/Al2O3 particles were surface organic functional modified by γ-glycidoxypropyltrimethoxysilane for the improvement of their dispersity in epoxy matrix. The results indicated that the curing exotherm of epoxy resin decreased significantly due to the addition of ZrB2/Al2O3 multiphase particles. In comparison to the composites filled with unmodified particles, the modified multiphase particles made the corresponding filling composites exhibit lower curing reaction heat, lower loss modulus, and higher storage modulus. Generally speaking, the composites filled with 5 wt% modified multiphase particles presented the best thermal stability and thermo-mechanical properties due to the better filler-matrix interfacial compatibility and the uniform dispersity of modified particles. Finite element analysis also suggested that the introduction of modified ZrB2/Al2O3 multiphase particles increased the stiffness of the corresponding composites.

PLA-coated sisal fibre-reinforced polyester composite: Water absorption, static and dynamic mechanical properties

2018 ◽  
Vol 53 (1) ◽  
pp. 65-72 ◽  
Author(s):  
MK Gupta ◽  
Rohit Singh
Keyword(s):  
Mechanical Properties ◽  
Water Absorption ◽  
Loss Modulus ◽  
Alkali Treatment ◽  
Dynamic Mechanical Properties ◽  
Mechanical Analysis ◽  
Static Properties ◽  
Physical Treatment ◽  
Sisal Fibre ◽  
Dynamic Mechanical

In the present work, a novel physical treatment (PLA coating) of sisal fibres and its influence on the water absorption, static and dynamic mechanical properties of its composites has been presented. The treated sisal fibres were used consisted of alkali treatment and PLA coating to fabricate its polyester-based composites by hand lay-up technique keeping constant fibres content as 20 wt.% . Water absorption analysis was carried out in terms of water uptake (%), and sorption, diffusion and permeability coefficient. In addition, static properties were examined in terms of tensile, flexural and impact test, and dynamic mechanical analysis was performed in terms of storage modulus [Formula: see text], loss modulus [Formula: see text], damping [Formula: see text] and glass transition temperature [Formula: see text]. It was reported that the PLA-coated sisal composites showed the best performance in water absorption, mechanical and dynamic mechanical properties than pure sisal and alkali-treated sisal composites. There were 33%, 49%, 48%, and 27% improvement in water resistance, tensile strength, flexural strength and impact strength, respectively, of PLA-coated sisal composites as compared to that of pure sisal composite.

scholarly journals The Effect of Bi-Functionalized MMT on Morphology, Thermal Stability, Dynamic Mechanical, and Tensile Properties of Epoxy/Organoclay Nanocomposites

Polymers ◽  
2019 ◽  
Vol 11 (12) ◽  
pp. 2012 ◽  
Author(s):  
Siew Sand Chee ◽  
Mohammad Jawaid
Keyword(s):  
Thermal Stability ◽  
Tensile Properties ◽  
In Situ Polymerization ◽  
Loss Modulus ◽  
Mechanical Analysis ◽  
Decomposition Temperature ◽  
Filler Loading ◽  
Hybrid Nanocomposites ◽  
Dynamic Mechanical ◽  
Link Density

In this work, the optimum filler loading to prepare epoxy/organoclay nanocomposites by the in-situ polymerization method was studied. Bi-functionalized montmorillonite at different filler loading (0.5, 1.0, 2.0, 4.0 wt %) was dispersed in epoxy resin by using a high shear speed homogenizer. The effect on morphology, thermal, dynamic mechanical, and tensile properties of the epoxy/organoclay nanocomposites were studied in this work. Wide-angle X-ray scattering (WAXS) and field emission scanning electron microscope (FESEM) studies revealed that possible intercalated structures were obtained in epoxy/organoclay nanocomposites. Thermogravimetric analysis (TGA) shows that epoxy/organoclay nanocomposites exhibit higher thermal stability at the maximum and final decomposition temperature, as well as higher char content, compared to pristine epoxy. The dynamic mechanical analysis (DMA) indicate that storage modulus (E′), loss modulus (E″), cross-link density and glass transition temperature (Tg) of the nanocomposites were improved with organoclay loading up to 1 wt %. Beyond this loading limit, the deterioration of properties was observed. A similar trend was also observed on tensile strength and modulus. We concluded from this study that organoclay loading up to 1 wt % is suitable for further study to fabricate hybrid nanocomposites for various applications.

scholarly journals Viscoelastic Properties of Contemporary Bulk-fill Restoratives: A Dynamic-mechanical Analysis

2018 ◽  
Vol 43 (3) ◽  
pp. 307-314 ◽  
Author(s):  
JEX Ong ◽  
AU Yap ◽  
JY Hong ◽  
AH Eweis ◽  
NA Yahya
Keyword(s):  
Dynamic Mechanical Analysis ◽  
Storage Modulus ◽  
Loss Tangent ◽  
Viscoelastic Properties ◽  
Loss Modulus ◽  
Artificial Saliva ◽  
Mechanical Analysis ◽  
Distilled Water ◽  
Glass Ionomer ◽  
Dynamic Mechanical

SUMMARY This study investigated the viscoelastic properties of contemporary bulk-fill restoratives in distilled water and artificial saliva using dynamic mechanical analysis. The materials evaluated included a conventional composite (Filtek Z350), two bulk-fill composites (Filtek Bulk-fill and Tetric N Ceram), a bulk-fill giomer (Beautifil-Bulk Restorative), and two novel reinforced glass ionomer cements (Zirconomer [ZR] and Equia Forte [EQ]). The glass ionomer materials were also assessed with and without resin coating (Equia Forte Coat). Test specimens 12 × 2 × 2 mm of the various materials were fabricated using customized stainless-steel molds. After light polymerization/initial set, the specimens were removed from the molds, finished, measured, and conditioned in distilled water or artificial saliva at 37°C for seven days. The materials (n=10) were then subjected to dynamic mechanical testing in flexure mode at 37°C and a frequency of 0.1 to 10 Hz. Storage modulus, loss modulus, and loss tangent data were subjected to normality testing and statistical analysis using one-way analysis of variance/Dunnett's test and t-test at a significance level of p < 0.05. Mean storage modulus ranged from 3.16 ± 0.25 to 8.98 ± 0.44 GPa, while mean loss modulus ranged from 0.24 ± 0.03 to 0.65 ± 0.12 GPa for distilled water and artificial saliva. Values for loss tangent ranged from 45.7 ± 7.33 to 134.2 ± 12.36 (10−3). Significant differences in storage/loss modulus and loss tangent were observed between the various bulk-fill restoratives and two conditioning mediums. Storage modulus was significantly improved when EQ and ZR was not coated with resin.

Study on Dynamic Mechanical Properties of n-HA/PA66 Composites

2011 ◽  
Vol 418-420 ◽  
pp. 1511-1515
Author(s):  
Lin Cheng ◽  
Xiang Zhang ◽  
Yu Bao Li
Keyword(s):  
Mechanical Properties ◽  
Storage Modulus ◽  
Loss Modulus ◽  
Physiological Saline ◽  
Dynamic Mechanical Properties ◽  
Intrinsic Properties ◽  
Polyamide 66 ◽  
Dynamic Mechanical ◽  
Reinforcing Effects

The dynamic mechanical properties of nano-hydroxyapatite (n-HA) reinforced polyamide 66 (PA66) biocomposites were studied with reference to the effect of n-HA content, frequency and physiological saline. The intrinsic properties of the components, morphology of the system and the nature of interface between the phases determine the dynamic mechanical properties of the composite. The storage modulus (E') values of n-HA/PA66 composites were much higher than those of pure PA66, indicating that the incorporation of n-HA in PA66 matrix induced reinforcing effects obviously. And the E' values of composites increased with increasing of n-HA content. The loss modulus (E") of the composite with 30wt% n-HA was higher that those of pure PA66 and the composite with 40wt% n-HA below 55°C, however, above 55°C, the E" values enhanced with increase of n-HA content. Both frequency and physiological saline had obvious effects on the dynamic mechanical properties for n-HA/PA66 composite. E' and E" values enhanced with increase of frequency, but tanδ values decreased with increasing of frequency. After soaked in physiological saline, the E' and E" values of the composite decreased.

scholarly journals Enhancement of Mechanical and Dynamic Mechanical Properties of Hydrophilic Nanoclay Reinforced Polylactic Acid/Polycaprolactone/Oil Palm Mesocarp Fiber Hybrid Composites

2014 ◽  
Vol 2014 ◽  
pp. 1-8 ◽  
Author(s):  
Chern Chiet Eng ◽  
Nor Azowa Ibrahim ◽  
Norhazlin Zainuddin ◽  
Hidayah Ariffin ◽  
Wan Md. Zin Wan Yunus ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Polylactic Acid ◽  
Oil Palm ◽  
Hybrid Composites ◽  
Loss Modulus ◽  
Impact Resistance ◽  
Dynamic Mechanical Properties ◽  
Mechanical Analysis ◽  
Dynamic Mechanical ◽  
The Fourier Transform

In previous studies, the effect of the addition of 1 wt% hydrophilic nanoclay on polylactic acid (PLA)/polycaprolactone (PCL)/oil palm mesocarp fiber (OPMF) biocomposites was investigated by tensile properties, thermogravimetric analysis (TGA), and scanning electron microscopy (SEM). The current studies focus on the effect of addition of 1 wt% hydrophilic nanoclay on mechanical (flexural and impact properties) and dynamic mechanical properties of composites. The composites were characterized by the Fourier transform infrared spectroscopy (FTIR) and dynamic mechanical analysis (DMA). FTIR spectra show that peak shifting occurs when 1 wt% hydrophilic nanoclay was added to composites. The addition of 1 wt% hydrophilic nanoclay successfully improves the flexural properties and impact resistance of the biocomposites. The storage modulus of biocomposites was decreased when nanoclay was added which indicates that the stiffness of biocomposites was reduced. The loss modulus curve shows that the addition of nanoclay shift twotgin composites become closer to each other which indicates that the incorporation of nanoclay slightly compatibilizes the biocomposites. Tanδindicated that hybrid composites dissipate less energy compared to biocomposites indicate that addition of clay to biocomposites improves fiber/matrix adhesion. Water sorption test shows that the addition of nanoclay enhances water resistance of composites.

Thermal and dynamic mechanical analysis of hybrid jute/sisal fibre reinforced epoxy composite

2016 ◽  
Vol 232 (9) ◽  
pp. 743-748 ◽  
Author(s):  
MK Gupta
Keyword(s):  
Thermal Properties ◽  
Storage Modulus ◽  
Hybrid Composites ◽  
Loss Modulus ◽  
Dynamic Mechanical Properties ◽  
Decomposition Temperature ◽  
Mechanical And Thermal Properties ◽  
Scanning Calorimetry ◽  
Sisal Fibre ◽  
Dynamic Mechanical

The aim of the present study is to investigate the dynamic mechanical and thermal properties of hybrid jute/sisal fibre reinforced epoxy composites. The hybrid composites were prepared by hand layup technique having total fibre loading of 30% by weight with different weight ratios of jute and sisal fibres. Dynamic mechanical properties such as storage modulus ([Formula: see text]), loss modulus ([Formula: see text]) and damping ([Formula: see text]) were investigated in the temperature range of 30–200 ℃. The thermal stability of the prepared composites was studied using thermogravimetric analysis. Other thermal properties such as glass transition temperature ( Tg), crystallization temperature ( Tc) and decomposition temperature ( Td) were also obtained by differential scanning calorimetry. The results indicated a positive effect of hybridization in terms of increase in dynamic mechanical and thermal properties. Storage modulus, loss modulus and Tg were found to be higher for hybrid composite having a higher percentage of jute fibres.

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