scholarly journals Improvement of Mechanical Properties of Polymer Materials by the Nanosized Ceramic Particles

2021 ◽  
Vol 16 ◽  
pp. 134-141
Author(s):  
O. V. Egorova ◽  
Thant Zin Hein
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Titanium Dioxide Nanoparticles ◽  
Polymer Materials ◽  
Relative Deformation ◽  
Epoxy Nanocomposites ◽  
Composition And Structure ◽  
Scanning Electron ◽  
Film Nanocomposites

As a result of the experiments, epoxy nanocomposites based on titanium dioxide nanoparticles in the form of opaque blue-gray films were obtained. The composition and structure of epoxy nanocomposites were studied by scanning electron microscopy and infrared spectroscopy. The properties of the obtained film nanocomposites were investigated to determine the glass transition temperature, and the mechanical properties of the films were tested in tension, where the tensile strength, elastic modulus, and relative deformation were determined

Electron Microscopic Observation of the Longitudinal Organization of Poly (p-Phenylene Terephthalamide) Fibers

1982 ◽  
Vol 40 ◽  
pp. 680-681
Author(s):  
Li Li-Sheng ◽  
L.F. Allard ◽  
W.C. Bigelow
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Microscopic Observation ◽  
Electron Microscopic Observation ◽  
Electron Microscopic ◽  
Aromatic Polyamides ◽  
Radial Arrangement ◽  
Scanning Electron ◽  
Better Than

The aromatic polyamides form a class of fibers having mechanical properties which are much better than those of aliphatic polyamides. Currently, the accepted morphology of these fibers as proposed by M.G. Dobb, et al. is a radial arrangement of pleated sheets, with the plane of the pleats parallel to the axis of the fiber. We have recently obtained evidence which supports a different morphology of this type of fiber, using ultramicrotomy and ion-thinning techniques to prepare specimens for transmission and scanning electron microscopy.

scholarly journals Analysis of PLA Composite Filaments Reinforced with Lignin and Polymerised-Lignin-Treated NFC

Polymers ◽  
2021 ◽  
Vol 13 (13) ◽  
pp. 2174
Author(s):  
Diana Gregor-Svetec ◽  
Mirjam Leskovšek ◽  
Blaž Leskovar ◽  
Urška Stanković Elesini ◽  
Urška Vrabič-Brodnjak
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Tensile Strength ◽  
Glassy State ◽  
Nanofibrillated Cellulose ◽  
Dynamic Mechanical Properties ◽  
Initial Modulus ◽  
Surface Modified ◽  
Scanning Electron

Polylactic acid (PLA) is one of the most suitable materials for 3D printing. Blending with nanoparticles improves some of its properties, broadening its application possibilities. The article presents a study of composite PLA matrix filaments with added unmodified and lignin/polymerised lignin surface-modified nanofibrillated cellulose (NFC). The influence of untreated and surface-modified NFC on morphological, mechanical, technological, infrared spectroscopic, and dynamic mechanical properties was evaluated for different groups of samples. As determined by the stereo and scanning electron microscopy, the unmodified and surface-modified NFCs with lignin and polymerised lignin were present in the form of plate-shaped agglomerates. The addition of NFC slightly reduced the filaments’ tensile strength, stretchability, and ability to absorb energy, while in contrast, the initial modulus slightly improved. By adding NFC to the PLA matrix, the bending storage modulus (E’) decreased slightly at lower temperatures, especially in the PLA samples with 3 wt% and 5 wt% NFC. When NFC was modified with lignin and polymerised lignin, an increase in E’ was noticed, especially in the glassy state.

scholarly journals Corrosion Behavior and Mechanical Properties of a Nanocomposite Superhydrophobic Coating

Coatings ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 652
Author(s):  
Divine Sebastian ◽  
Chun-Wei Yao ◽  
Lutfun Nipa ◽  
Ian Lian ◽  
Gary Twu
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Atomic Force Microscopy ◽  
Nanocomposite Coating ◽  
Superhydrophobic Coating ◽  
Force Microscopy ◽  
Atomic Force ◽  
Microscopy Images ◽  
Scanning Electron

In this work, a mechanically durable anticorrosion superhydrophobic coating is developed using a nanocomposite coating solution composed of silica nanoparticles and epoxy resin. The nanocomposite coating developed was tested for its superhydrophobic behavior using goniometry; surface morphology using scanning electron microscopy and atomic force microscopy; elemental composition using energy dispersive X-ray spectroscopy; corrosion resistance using atomic force microscopy; and potentiodynamic polarization measurements. The nanocomposite coating possesses hierarchical micro/nanostructures, according to the scanning electron microscopy images, and the presence of such structures was further confirmed by the atomic force microscopy images. The developed nanocomposite coating was found to be highly superhydrophobic as well as corrosion resistant, according to the results from static contact angle measurement and potentiodynamic polarization measurement, respectively. The abrasion resistance and mechanical durability of the nanocomposite coating were studied by abrasion tests, and the mechanical properties such as reduced modulus and Berkovich hardness were evaluated with the aid of nanoindentation tests.

Research on compatibility and surface of high impact bio-based polyamide

2021 ◽  
pp. 095400832110055
Author(s):  
Yang Wang ◽  
Yuhui Zhang ◽  
Yuhan Xu ◽  
Xiucai Liu ◽  
Weihong Guo
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Differential Scanning Calorimetry ◽  
Crystallization Behavior ◽  
High Impact ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Scanning Electron

The super-tough bio-based nylon was prepared by melt extrusion. In order to improve the compatibility between bio-based nylon and elastomer, the elastomer POE was grafted with maleic anhydride. Scanning Electron Microscopy (SEM) and Thermogravimetric Analysis (TGA) were used to study the compatibility and micro-distribution between super-tough bio-based nylon and toughened elastomers. The results of mechanical strength experiments show that the 20% content of POE-g-MAH has the best toughening effect. After toughening, the toughness of the super-tough nylon was significantly improved. The notched impact strength was 88 kJ/m2 increasing by 1700%, which was in line with the industrial super-tough nylon. X-ray Diffraction (XRD) and Differential Scanning Calorimetry (DSC) were used to study the crystallization behavior of bio-based PA56, and the effect of bio-based PA56 with high crystallinity on mechanical properties was analyzed from the microstructure.

scholarly journals Effect of Annealing Process on the Mechanical Properties of X70 Pipeline Steel

2018 ◽  
Vol 186 ◽  
pp. 02001
Author(s):  
Teng-wei Zhu ◽  
Cheng-liang Miao ◽  
Zheng Cheng ◽  
Zhipeng Wang ◽  
Yang Cui ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Tensile Strength ◽  
Annealing Temperature ◽  
Pipeline Steel ◽  
Annealing Process ◽  
X70 Pipeline Steel ◽  
Grain Sizes ◽  
Scanning Electron

The influence of the mechanical properties of X70 pipeline steel under different annealing temperature was studied. The corresponding microstructure was investigated by the Field Emission Scanning Electron Microscopy. The results showed that the yield strength and the tensile strength both experienced from rise to decline with the increase of annealing temperature. The grain sizes were coarse and a large amount of cementite precipitated due to preserving temperature above 550 °, which induced matrix fragmentation and deteriorate the -10 ° DWTT Toughness. There were little changes on the microstructure and mechanical properties when the annealing temperature was under 500 °.

scholarly journals Antibacterial activity of zinc oxide nanoparticles obtained by pulsed laser ablation in water and air

2018 ◽  
Vol 243 ◽  
pp. 00017 ◽  
Author(s):  
Daria Goncharova ◽  
Ekaterina Gavrilenko ◽  
Anna Nemoykina ◽  
Valery Svetlichnyi
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Antibacterial Activity ◽  
Laser Ablation ◽  
Zno Nanoparticles ◽  
Antibacterial Properties ◽  
Pulsed Laser ◽  
Pulsed Laser Ablation ◽  
Composition And Structure ◽  
Scanning Electron

The paper studies physicochemical and antibacterial properties of ZnO nanoparticles obtained by pulsed laser ablation in water and air. Their composition and structure were studied by X-ray diffraction, transmission and scanning electron microscopy. Antibacterial activity of the nanoparticles was examined by its affection on Gram-positive Staphylococcus aureus (S.aureus). The dependence of nanoparticles’ physical and chemical antibacterial properties on the conditions of the ablation was shown. The model materials for the antibacterial bandage were made of cotton, filter paper and biodegradable polymer scaffolds (poly-l-lactide acid), and then they were coated with the obtained ZnO nanoparticles. The model bandage materials were examined by the scanning electron microscopy method and their antibacterial activity (ISO 20743:2013) was determined. High activity of all the samples against S.aureus was proved.

Hierarchical Design and Nanomechanics of the Calcified Byssus of Anomia simplex

2009 ◽  
Vol 1187 ◽  
Author(s):  
Jakob R Eltzholtz ◽  
Marie Krogsgaard ◽  
Henrik Birkedal
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Mechanical Performance ◽  
Blue Mussel ◽  
Hierarchical Design ◽  
Reduced Modulus ◽  
Different Types ◽  
Microscopy Images ◽  
Scanning Electron

AbstractBiology has evolved several strategies for attachment of sedentary animals. In the bivalves, byssi abound and the best known example being the protein-based byssus of the blue mussel and other Mytilidae. In contrast the bivalve Anomia sp. has a single calcified thread. The byssus is hierarchical in design and contains several different types of structures as revealed by scanning electron microscopy images. The mechanical properties of the byssus are probed by nanoindentation. It is found that the mineralized part of the byssus is very stiff with a reduced modulus of about 67 GPa and a hardness of ˜3.7 GPa. This corresponds to a modulus roughly 20% smaller than that of pure calcite and a hardness that is about 20% larger than pure calcite. The results reveal the importance of microstructure on mechanical performance.

scholarly journals Polymeric Composites Based on Polyurea Matrix Reinforced with Carbon Nanotubes

2017 ◽  
Vol 54 (1) ◽  
pp. 41-44 ◽  
Author(s):  
Maria Adina Vulcan ◽  
Celina Damian ◽  
Paul Octavian Stanescu ◽  
Eugeniu Vasile ◽  
Razvan Petre ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Carbon Nanotubes ◽  
Thermal Stability ◽  
Scanning Electron Microscopy ◽  
Tensile Tests ◽  
Mechanical Analysis ◽  
Multi Walled Carbon Nanotubes ◽  
Walled Carbon Nanotubes ◽  
Scanning Electron

This paper deals with the synthesis of polyurea and its use as polymer matrix for nanocomposites reinforced with multi-walled carbon nanotubes (MWCNT). Two types of materials were obtained during this research, the first cathegory uses the polyurea as matrix and the second one uses a mixture between epoxy resin and polyurea. The nanocomposites were characterized by Thermogravimetric Analysis (TGA), Dynamic Mechanical Analysis (DMA), Scanning Electron Microscopy (SEM) and Tensile Tests .The elastomeric features of nanocomposites were highlighted by the results which showed low value of Tg. Also higher thermal stability with ~40oC compared with commercial products (M20) were observed, but lower mechanical properties compared to neat polyurea.

scholarly journals Surface Hybrid Nanocomposite Produced by Friction Stir Processing: Microstructural Evolution, Mechanical Properties and Tribological Behavior

2021 ◽  
Author(s):  
Saeed Ahmadifard ◽  
Nasir Shahin ◽  
Mojtaba Vakili-azghandi ◽  
Shahab Kazemi
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Friction Stir Processing ◽  
Travel Speed ◽  
Hybrid Nanocomposites ◽  
Max Phase ◽  
Hybrid Nanocomposite ◽  
Friction Stir ◽  
Scanning Electron

Abstract This study investigates the effects of incorporating Ti3AlC2 MAX phase into Al7075-T6 alloy by friction stir processing as well as adding Al2O3 nanoparticles to obtain a surface hybrid nanocomposite. These composites were successfully prepared by friction stir processing with a rotational speed of 1000 rpm and a travel speed of 28 mm/min after 3 passes. Optical, atomic force and scanning electron microscopy as well as microhardness, tensile and wear tests utilized to characterize the fabricated surface hybrid nanocomposites. Results showed that the maximum tensile strength and hardness value were achieved for Al-100% Al2O3 composite due to more grain refinement and effective dispersion of nanoparticles. Due to its laminar structure, Ti3AlC2 MAX phase enhanced better tribological characterization whereas Al2O3 nanoparticles cause better mechanical properties. Scanning electron microscopy tests revealed that the wear mechanism changes from adhesive for Al7075 alloy to adhesive-abrasive for the nanocomposite specimens.

Sign in / Sign up

Export Citation Format

Share Document