Precipitate and Age Hardening Response of As-Cast Mg-8Yb-0.5Zr Magnesium Alloy

2011 ◽  
Vol 399-401 ◽  
pp. 17-20
Author(s):  
Wen Bin Yu ◽  
Zhi Qian Chen ◽  
Mang Zhang ◽  
Zhou Yu
Keyword(s):  
Heat Treatment ◽  
Magnesium Alloy ◽  
Grain Boundaries ◽  
Microstructure Evolution ◽  
Solution Heat Treatment ◽  
Artificial Aging ◽  
Precipitation Hardening ◽  
Intermetallic Phase ◽  
Age Hardening ◽  
Maximum Hardness

The precipitation hardening response of as-cast Mg-8Yb-0.5Zr magnesium alloy was investigated in the present work. The microstructure evolution of the alloy illustrated that Mg2Yb intermetallic phase was dissolved by solution heat treatment at 520°C for 12 hours. An apparent precipitation hardening response in Mg-8Yb-0.5Zr was discovered after artificial aging at 150°C, with maximum hardness increment of about 80 percent at the peak condition. It was found that the precipitates of the alloy were in the shape of two conjoined cosh and globe about 50 nm, and precipitated preferentially on grain boundaries and dislocations.

TEM and X-Ray Examinations of Intermetallic Phases and Carbides Precipitation in an Fe-Ni Superalloy during Prolonged Ageing

2013 ◽  
Vol 212 ◽  
pp. 15-20
Author(s):  
Kazimierz J. Ducki ◽  
Jacek Mendala ◽  
Lilianna Wojtynek
Keyword(s):  
Heat Treatment ◽  
Solution Heat Treatment ◽  
Intermetallic Phase ◽  
Intermetallic Phases ◽  
Precipitation Process ◽  
Secondary Phases ◽  
X Ray Diffraction ◽  
Solid Samples ◽  
Structural Investigations ◽  
X Ray

The influence of prolonged ageing on the precipitation process of the secondary phases in an Fe-Ni superalloy of A-286 type has been studied. The samples were subjected to a solution heat treatment at 980°C for 2 h and water quenched, and then aged at temperatures of 715, 750 and 780°C at holding times from 0.5 to 500 h. Structural investigations were conducted using TEM and X-ray diffraction methods. The X-ray phase analyses performed on the isolates were obtained by anodic dissolution of the solid samples. After solution heat treatment the alloy has the structure of twinned austenite with a small amount of undissolved precipitates, such as carbide TiC, carbonitride TiC0.3N0.7, nitride TiN0.3, carbosulfide Ti4C2S2, Laves phase Ni2Si, and boride MoB. The application of ageing causes precipitation processes of γ-Ni3(Al,Ti), G (Ni16Ti6Si7), η (Ni3Ti), β (NiTi) and σ (Cr0.46Mo0.40Si0.14) intermetallic phases, as well as the carbide M23C6. It was found that the main phase precipitating during alloy ageing was the γ intermetallic phase.

scholarly journals The Effect of Elastic Strain and Small Plastic Deformation on Tensile Strength of a Lean Al–Mg–Si Alloy

Metals ◽  
2019 ◽  
Vol 9 (12) ◽  
pp. 1276
Author(s):  
Eva Anne Mørtsell ◽  
Ida Westermann ◽  
Calin Daniel Marioara ◽  
Ketill Olav Pedersen ◽  
Sigmund Jarle Andersen ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Plastic Deformation ◽  
Elastic Strain ◽  
Solution Heat Treatment ◽  
Small Deformation ◽  
Age Hardening ◽  
Strength Increase ◽  
Artificial Ageing ◽  
Small Plastic ◽  
Small Plastic Deformation

Al–Mg–Si alloys are usually formed into their final shape by rolling or extrusion. After extrusion, the aluminium profiles are usually straightened, causing the material to be subjected to a small plastic deformation. This study demonstrates the positive effect on strength that can be obtained from such small deformation levels or from only elastically straining the material. Elastic straining of a lean Al–Mg–Si alloy, when performed immediately after solution heat treatment, enhances the material yield strength after artificial ageing to T6. Transmission electron microscopy shows that this effect can be attributed to a higher number density and finer dispersion of the age-hardening precipitate needles. Furthermore, introducing a small plastic deformation of 1% after solution heat treatment results in a comparable strength increase to elastically straining the material. In this case, however, the strength increase is due to the increased dislocation density, which compensates for a lower density of precipitate needles. Finally, by combining plastic deformation with a succeeding elastic strain, we demonstrate how elastic strain can cause an on-set of dislocation cell formation in this material.

Fatigue Behavior of Age-Hardening Cu-6Ni-1.5Si Alloys with Different Grain Sizes

2021 ◽  
Vol 1016 ◽  
pp. 125-131
Author(s):  
Masahiro Goto ◽  
T. Yamamoto ◽  
S.Z. Han ◽  
J. Kitamura ◽  
J.H. Ahn ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Grain Size ◽  
Fatigue Strength ◽  
Solution Heat Treatment ◽  
Fatigue Behavior ◽  
Fatigue Tests ◽  
The Other ◽  
Age Hardening ◽  
Grain Sizes ◽  
Thermomechanical Processes

On the thermomechanical treatments of Cu-Ni-Si alloy, cold-rolling (CR) before solution heat treatment (SHT) is commonly conducted to eliminate defects in a casting slab. In addition, a rolling is applied to reduce/adjust the thickness of casting slab before SHT. In a heavily deformed microstructure by CR, on the other hand, grain growth during a heating in SHT is likely to occur as the result of recrystallization. In general, tensile strength and fatigue strength tend to decrease with an increase in the grain size. However, the effect of difference in grain sizes produced by with and without CR before SHT on the fatigue strength is unclear. In the present study, fatigue tests of Cu-6Ni-Si alloy smooth specimens with a grain fabricated through different thermomechanical processes were conducted. The fatigue behavior of Cu-Ni-Si alloy was discussed.

Formation of a Novel X Phase in Mg–Gd–Zn–Zr Alloy

2010 ◽  
Vol 654-656 ◽  
pp. 623-626 ◽  
Author(s):  
Y.J. Wu ◽  
Li Ming Peng ◽  
X.Q. Zeng ◽  
D.L. Lin ◽  
W.J. Ding
Keyword(s):  
Heat Treatment ◽  
Solid Solution ◽  
Phase Transformation ◽  
Grain Boundaries ◽  
Solution Heat Treatment ◽  
Long Period ◽  
Β Phase ◽  
Lpso Structure ◽  
Zr Alloy ◽  
Zr Alloys

The coherent fine-lamellae consisting of the 2H-Mg and the 14H-type long period stacking ordered (LPSO) structure within α'-Mg matrix have been observed in an as-cast Mg–Gd–Zn–Zr alloy. During subsequent solid solution heat treatment at 773 K, in addition to the lamellae within matrix, a novel lamellar X phase [Mg–(8.37±1.0)Zn–(11.32±1.0)Gd] with the 14H-type LPSO structure was transformed from the dendritical β phase. The 14H-type LPSO structure existing in Mg–Gd–Zn–Zr alloys derives from two variant ways: formation of the 14H-type LPSO structure comes from two variant means: i.e., the formation within matrix and the phase transformation from the β phase to the X phase in grain boundaries.

scholarly journals The Influence of Post-Heat-Treatments on the Tensile Strength and Surface Hardness of Selective Laser Melted AlSi10Mg

2017 ◽  
Vol 370 ◽  
pp. 171-176 ◽  
Author(s):  
Leonhard Hitzler ◽  
Amandine Charles ◽  
Andreas Öchsner
Keyword(s):  
Heat Treatment ◽  
Tensile Strength ◽  
Precipitation Hardening ◽  
Elevated Temperatures ◽  
Surface Hardness ◽  
Heat Treatments ◽  
Age Hardening ◽  
Material Strength ◽  
Post Heat Treatment ◽  
Treatment Procedure

Recent investigations revealed major fluctuations in the material properties of selective laser melted AlSi10Mg, which corresponded with the varying precipitation-hardening state of the microstructure, caused by the differing dwell times at elevated temperatures. It was indicated that a subsequent heat treatment balances the age-hardening and results in a homogenized material strength. In order to further investigate this statement selective laser melted AlSi10Mg samples were subject to multiple post-heat-treatments. Subsequently, the surface hardness and tensile strength was determined and compared with the as-built results. The post-heat-treatment led to an arbitrary occurrence of rupture, indicating a successful homogenization, coupled with a remarkable improvement in ductility, but to the costs of a lowered tensile strength, which was highly dependent on the chosen heat-treatment procedure.

scholarly journals Effect of Artificial Aging, Delayed Aging, and Pre-Aging on Microstructure and Properties of 6082 Aluminum Alloy

Metals ◽  
2019 ◽  
Vol 9 (2) ◽  
pp. 173 ◽  
Author(s):  
Xin He ◽  
Qinglin Pan ◽  
Hang Li ◽  
Zhiqi Huang ◽  
Shuhui Liu ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Tensile Strength ◽  
Aluminum Alloy ◽  
Solution Heat Treatment ◽  
Room Temperature ◽  
Artificial Aging ◽  
Experimental Results ◽  
Negative Effects ◽  
Short Term ◽  
6082 Aluminum Alloy

Three different aging treatments including single-aging, delayed-aging, and pre-aging were carried out on 6082 extruded profiles after solution heat treatment, then their hardness, tensile strength, and microstructure were tested. The experimental results reveal that the properties and microstructure changes during single-aging. Based on this, the negative effects of room temperature delay and the results of short-term pre-aging treatments used in the experiment to improve this phenomenon have been concluded.

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