Effects of Hot Extrusion and Aging on Microstructure and Mechanical Properties of Mg-Zn-Si-Ca Magnesium Alloy

2013 ◽  
Vol 668 ◽  
pp. 823-829 ◽  
Author(s):  
Xiu Qing Zhang ◽  
Ge Chen ◽  
Yang Wang ◽  
Min Yu Han

Homogenized magnesium alloy Mg-6Zn-Si-0.25Ca has been hot-extruded and then aging treated for improving the magnesium alloy plastic deformation ability and promoting applications of magnesium alloys. In the hot extrusion process, the influences of extrusion parameters for microstructures and mechanical properties of Mg-6Zn-Si-0.25Ca magnesium alloy were investigated. The results show that dynamic recrystallization occurred during hot extrusion. Compared with as-cast alloy, the grains are fined remarkably, and the mechanical properties are enhanced obviously. Twin crystals appeared in grains after hot extrusion, with the extrusion temperature rising, twin crystal structures has been reduced. Aging further increased the mechanical properties of the estruded alloy. The ultimate tensile strength of Mg-6Zn-Si-0.25Ca alloy is about 385 MPa and the elongation is about 11% when extruded at 320°C(extrusion ratio is 10) and aged at 190°C for 8h.

2010 ◽  
Vol 148-149 ◽  
pp. 332-337 ◽  
Author(s):  
Yong Xue ◽  
Zhi Min Zhang ◽  
Li Hui Lang

In the present research, the influences of different extrusion ratios (15, 30, 45, 60, and 75), extrusion temperatures (300 , 340 , 380 , 420 , and 460 ), and subsequent heat treatment on the mechanical properties and microstructure of as-cast ZK60 magnesium alloy have been investigated through the tensile tests and via metallographic observation. The results show that forward extrusion process can refine the microstructure of as-cast ZK60 alloy effectively. If as-cast ZK60 alloys have been extruded with the extrusion ratio 45 at 380 ,420 and 460 , respectively, and then post-heat treatment was conducted, the ZK60 alloy’s strength is higher under T5 than T6 treatment. For as-cast ZK60 alloy processed by extrusion and T5 method, the most appropriate temperature for extrusion processing is 300 , at which its tensile strength are highest provided the extrusion ratio is 30 but yet its plasticity is best provided the extrusion ratio is 45. If forward extrusions were conducted at 380 , mechanical properties of ZK60 alloy have little difference as the extrusion ratio varies. When T6 treatment was conducted for the extruded bars, their mechanical properties were improved little, moreover, the bigger the extrusion ratio is, the higher the tensile strength and elongation of the extruded bars become.


2011 ◽  
Vol 704-705 ◽  
pp. 892-896
Author(s):  
Bao Hong Zhang ◽  
Zhi Min Zhang

In order to study the effect of plastic deformation on microstructure and mechanical properties of as-cast AZ91 magnesium alloy, experiments of hot direct extrusion were performed at different extrusion temperatures and different extrusion ratios. The microstructure and mechanical properties of extruded billets and extrudate were measured. Experimental results show that the grain size of as-cast AZ91 magnesium alloy can be dramatically refined by extrusion. Hot extrusion can obviously improve the mechanical properties of as-cast AZ91 magnesium Alloy, comparing with the pre-extruded billet, the tensile strength, yield strength and elongation of extrudate can be improved by at least 69%, 117% and 150% respectively. As the extrusion temperature increases, the tensile strength and yield strength of extrudate will increase. As the extrusion ratio increases, the tensile strength and yield strength of extrudate will increase at first and then fall. At the time of extrusion temperature of 420°C and extrusion ratio of 45, the highest tensile strength of 381Mpa and yield strength of 303MPa can be achieved for the extrudate.


2013 ◽  
Vol 710 ◽  
pp. 21-24 ◽  
Author(s):  
Jian Gang Lv ◽  
Gao Feng Quan ◽  
Rui Chun Li ◽  
Chun Yuan Shi ◽  
Ying Bo Zhang ◽  
...  

According to the profile section of transport equipment, the wide and hollow AZ31 magnesium alloy profiles was self-designed. Extrusion molding performance of the profiles, the law of microstructure and mechanical properties were studied when billets pretreatment and extrusion temperature were changed. The conclusions are as follows: (1) The grains of AZ31 profiles extruded by pre-extrusion billet are smaller and the strength is better, its maximum tensile strength is 280MPa. (2) Other processes being equal, the grains of AZ31 profiles are smaller and strength is higher, but the plastic is bad, when the extrusion temperature is 300°C. However, both strength and ductility of AZ31 profiles are better, when the extrusion temperature is 350°C. (3) Wide and Hollow AZ31 profiles perform significant heterogeneity and anisotropic characteristics on mechanical properties.


2009 ◽  
Vol 23 (06n07) ◽  
pp. 990-995 ◽  
Author(s):  
GUOQING CHEN ◽  
JUNHUI SONG ◽  
XUESONG FU ◽  
YUXIAN ZHAO ◽  
WENLONG ZHOU

This paper describes the effect of hot extrusion on the microstructure and mechanical properties of electromagnetic continuous cast (EMC) AZ31 alloy. The microstructure, mechanical properties and fracture surfaces of AZ31 alloy before and after extrusion were investigated. The results demonstrate that extrusion processing gives rise to a strong basal texture. The grains are significantly refined and the average grain size of localized fine grain area is 2μm. Compared with EMC ingots, as-extruded specimens have much finer grain size and more uniform microstructure, and the second phase ( Mg 17 Al 12) becomes smaller and distributes more uniformly. The mechanical properties of the deformed AZ31 were improved after hot-extrusion. When the extrusion ratio was 10, the yield strength, ultimate tensile strength and reduction in cross-sectional area of as-extruded AZ31 alloy were 248MPa, 306MPa and 28.44%, which were respectively enhanced by 78.4%, 41% and 45.25%, compared with those of as-cast samples. With the increase of extrusion ratio, the grain refining effect was more significant and the microstructure was more uniform. The yield strength, ultimate tensile strength and reduction in cross-sectional area increased obviously with increasing the extrusion ratio. The observation on fracture surfaces demonstrates that the fracture mode changes from ductile-brittle fracture to ductile fracture after extrusion.


2017 ◽  
Vol 894 ◽  
pp. 21-24 ◽  
Author(s):  
S.Nю Ab Rahim ◽  
Mohd Amri Lajis

In the present work, aluminum AA6061 chip metals were extruded by hot extrusion and the effect of extrusion parameters on the mechanical properties and surface integrity were investigated. The objective of the present studies it to analyze the mechanical and structural properties of 6061 after plastic consolidation by hot extrusion. Tensile test results showed that material extruded using temperature 550°C exhibit higher ultimate tensile strength (UTS) compared with temperature of 400°C. Fracture surfaces shown that ductile fracture mode occurred at condition 500°C and 2 hours, and brittle fracture occurred at condition 400°C.


2010 ◽  
Vol 97-101 ◽  
pp. 565-569
Author(s):  
J.M. Yu ◽  
Zhi Min Zhang ◽  
Bao Hong Zhang ◽  
Qiang Wang

The effects of extrusion ratios (15, 30, 45and 60) on microstructure and mechanical properties of ZK60 magnesium alloy after T5 treatment were investigated. The results show that mechanical properties increase with the increase of extrusion ratios from 15 to 45.However, when the extrusion ratio is increase to 60, each mechanical property is decreased severly.By comparison,in the extrusion ratio of 30, ZK60 magnesium alloy after T5 treatment has excellent comprehensive mechanical properties.Different degrees of dynamic recrystallization appeared in the extrusion process and induced precipitation of second phase.The precipitation of the second phase is beneficial to the grain refinement and meanwhile to the promotion of the strength.


2011 ◽  
Vol 291-294 ◽  
pp. 1082-1086
Author(s):  
Yao Jin Wu ◽  
Zhi Ming Zhang ◽  
Bao Cheng Li ◽  
Bao Hong Zhang ◽  
Jian Min Yu ◽  
...  

In the present research, the influences of different extrusion ratios (15, 30, 45, 60, and 75) and extrusion temperature (300°C, 330°C, 360°C, 390°C, 420°C) on the mechanical properties and microstructure changes of AZ80 magnesium alloy have been investigated through tensile test and via ZEISS digital metallographic microscope observation. Research indicates that the alloy’s plasticity gradually decreases as the temperature increases, and that the alloy’s tensile strength varies with the extrusion ratio. At 330°C, the alloy’s particle grain is small and a small amount of black hard and brittle second-phase β (Mg17Al12) are precipitated uniformly along the grain boundary causing the gradual increase of the alloy’s tensile strength. When the extrusion temperature is up to 390°C, the grain size increases significantly, but the second phase precipitation along grain boundaries transforms into continuous and uniform-distribution precipitation within the grain. In this case, when the extrusion ratio is 60, the alloy’s tensile strength reaches its peak 390 Mpa. As the extrusion temperature increases, inhomogeneous precipitation of the second-phase along grain boundaries increases, causing the decrease of the alloy’s strength. At the same temperature, both the tensile strength and plasticity increases firstly and then decreases as extrusion ratio increases. With the gradual increase of the refinement grain, the dispersed precipitates increase and the alloy’s tensile strength and plasticity reach their peaks when the extrusion temperature is 390°C. As the grain grows, the second phase becomes inhomogeneous distribution, and the alloy’s strength and plasticity gradually decrease.


2020 ◽  
Vol 10 (15) ◽  
pp. 5345
Author(s):  
Sayed Amer ◽  
Olga Yakovtseva ◽  
Irina Loginova ◽  
Svetlana Medvedeva ◽  
Alexey Prosviryakov ◽  
...  

The microstructure, phase composition, and mechanical properties during heat treatment and rolling of the novel Al-5.0Cu-3.2Er-0.9Mn-0.3Zr alloy were evaluated. A new quaternary (Al,Cu,Mn,Er) phase with possible composition Al25Cu4Mn2Er was found in the as-cast alloy. Al20Cu2Mn3 and Al3(Zr,Er) phases were nucleated during homogenization, and θ″(Al2Cu) precipitates were nucleated during aging. The metastable disc shaped θ″(Al2Cu) precipitates with a thickness of 5 nm and diameter of 100–200 nm were nucleated mostly on the Al3(Zr,Er) phase precipitates with a diameter of 35 nm. The hardness Vickers (HV) peak was found after the annealing of a rolled alloy at 150 °C due to strengthening by θ″(A2Cu) precipitates, which have a larger effect in materials hardness than do the softening processes. The novel Al-Cu-Er-Mn-Zr alloy has a yield strength (YS) of 320–332 MPa, an ultimate tensile strength (UTS) of 360–370 MPa, and an El. of 3.2–4.0% in the annealed alloy after rolling condition.


2017 ◽  
Vol 898 ◽  
pp. 124-130 ◽  
Author(s):  
Shu Min Xu ◽  
Xin Ying Teng ◽  
Xing Jing Ge ◽  
Jin Yang Zhang

In this paper, the microstructure and mechanical properties of the as-cast and heat treatment of Mg-Zn-Nd alloy was investigated. The alloy was manufactured by a conventional casting method, and then subjected to a heat treatment. The results showed that the microstructure of as-cast alloy was comprised of α-Mg matrix and Mg12Nd phase. With increase of Nd content, the grain size gradually decreased from 25.38 μm to 9.82 μm. The ultimate tensile strength and elongation at room temperature of the Mg94Zn2Nd4 alloy can be reached to 219.63 MPa and 5.31%. After heat treatment, part of the second phase dissolved into the magnesium matrix and the grain size became a little larger than that of the as-cast. The ultimate tensile strength was declined by about 2.5%, and the elongation was increased to 5.47%.


2011 ◽  
Vol 335-336 ◽  
pp. 783-786
Author(s):  
Fu Yin Han ◽  
Lin Hai Tian ◽  
Hong Xia Wang ◽  
Wei Liang ◽  
Wen Xian Wang

Sr added ignition-proof AZ91D-0.3Be magnesium alloy was prepared. The influence of Sr content on microstructure and mechanical properties of the alloy was studied. Results show that the microstructure of ignition-proof AZ91D-0.3Be magnesium alloy is refined by a small amount of Sr addition. It is due to that the enrichment of a few Sr atoms in solid liquid interface in the process of magnesium alloy solidification inhibits grain growth and accelerates more nucleation. However, with increasing of Sr addition the microstructure is coarsened. By 0.01% Sr addition the tensile strength of as-cast experimental alloy is increased by about 25% and that of both the solid-solution and aged alloy is increased by about 40%. The elongation of as-cast alloy is increased by about 20% and that of solid-solution alloy increased by about 30%.


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