Crack Filling of Cover Glasses by Sol-Gel Coatings

2013 ◽  
Vol 797 ◽  
pp. 700-705 ◽  
Author(s):  
Kung Jeng Ma ◽  
Hsi Hsin Chien ◽  
Su Wei Huang ◽  
Shi Chang Chen ◽  
Choung Lii Chao

Strengthening of glass sheets through the process of ion exchange have been widely used in thinner cover glass for smart phone. The compressive stress improves the ability of the glass surface to withstand damage from mechanical impact. However, the presence of the damage resistant layer makes conventional mechanical and laser cutting of the ion-exchanged glass difficult. Normally, the cutting process will lead to spontaneous glass sheet breakage or shattering. Even successful in some samples, the underlying central tension is exposed on the edge, and the mechanical strength and durability of this edge is degraded. The repair of edge cracks becomes an extremely important issue for the development of single glass based smart phone. The ion exchanged glass plates (Corning IOX-FS) with a thickness of 0.7 mm were selected as the substrate materials. After cutting ion exchanged glass by high penetration diamond scribing wheels, the edge of glass plates can be protected or strengthened with silica sol using roll coating process. It was observed that the strength could be improved achieving 210 % compared to the strength of uncoated glass sheets. The sol-gel coating could improve the strength of the glass mainly by the mechanisms of filling in edge flaws or blunting crack tips. The effects of silica sol and processing parameters of roll coating process on the cracks filling effects were investigated.

2014 ◽  
Vol 26 (7) ◽  
pp. 72005
Author(s):  
张日东 Zhang Ridong ◽  
严鸿维 Yan Hongwei ◽  
吕海兵 Lü Haibing ◽  
张尽力 Zhang Jinli ◽  
晏良宏 Yan Lianghong ◽  
...  

2014 ◽  
Vol 597 ◽  
pp. 165-169
Author(s):  
Jie Hong Lei ◽  
Ri Dong Zhang

The porous sol-gel silica thin films were prepared on silicon substrate by the dip coating process. The surface roughness and microstructure of the film was measured by optical microscopy and AFM .Coating thickness and refractive index were measured by ellipsometry method. Influence of withdrawal speed and concentration of colloid was investigated for the thickness of silica. The relation of the thickness and withdrawal speed was fitted by the linear and power functions, and the results were analyzed and compared. It was found that the films with the same thickness prepared by different concentrations of colloid have different refractive indexes. The experimental results indicated that the thickness and refractive index of the film can be controlled by changing the withdrawal speed and colloid concentration.


2019 ◽  
Vol 7 (3) ◽  
Author(s):  
Venkata Rajesh Saranam ◽  
Chih-Hung Chang ◽  
Brian K. Paul

Foam-core meniscus coating is being used to retrofit 100 nm-scale sol–gel anti-reflective coatings (ARCs) onto in-field solar panels through the deposition, evaporation, and curing of wet films. Advantages of this technique include the means to control fluid flow relative to substrate motion and the ability to conform to large, warped substrates. While simple in practice, no models exist for predicting critical outcomes such as film thickness. In this paper, preliminary experiments are used to identify important process parameters, and an analytical model is developed and validated for predicting the thickness of silica sol–gel films deposited on solar glass.


2006 ◽  
Vol 309-311 ◽  
pp. 759-762 ◽  
Author(s):  
Shula Radin ◽  
Javad Parvizi ◽  
Paul Ducheyne

Previously, the properties of room temperature processed silica sol gel (also called xerogels) as resorbable and biocompatible controlled release systems were described. It was demonstrated that drugs and macromolecules with a variety of properties and characteristics could be released in a controlled manner. In this study, we focus on the synthesis of antibacterial thin solgel films on intramedullary nails and fracture fixation materials. We determine the effect of processing parameters on the in vitro properties and demonstrated a time- and load- dependent release of vancomycin from the film. This study suggests that thin sol-gel films hold great promise for the prevention and treatment of bone infections.


RSC Advances ◽  
2021 ◽  
Vol 11 (13) ◽  
pp. 7732-7737
Author(s):  
Fenying Wang ◽  
Dan Wang ◽  
Tingting Wang ◽  
Yu Jin ◽  
Baoping Ling ◽  
...  

Fluorescent molecularly imprinted polymer (FMIP) gains great attention in many fields due to their low cost, good biocompatibility and low toxicity. Here, a high-performance FMIP was prepared based on the autocatalytic silica sol–gel reaction.


2005 ◽  
Vol 885 ◽  
Author(s):  
Krithi Shetty ◽  
Shihuai Zhao ◽  
Wei Cao ◽  
Naidu V. Seetala ◽  
Debasish Kuila

ABSTRACTThe goal of this research is to investigate the activities of a non-noble nano-catalyst (Ni/SiO2) using Si-microreactors for steam reforming of methanol to produce hydrogen for fuel cells. The supported catalyst was synthesized by sol-gel method using Ni (II) salts and Si(C2H5O)4 as starting materials. EDX results indicate that the actual loading of Ni (5-6%) is lower than the intended loading of 12 %. The specific surface area of the silica sol-gel encapsulated Ni nano-catalyst is 452 m2/g with an average pore size of ∼ 3 nm. Steam reforming reactions have been carried out in a microreactor with 50 µm channels in the temperature range of 180-240 °C and atmospheric pressure. Results show 53% conversion of methanol with a selectivity of 74 % to hydrogen at 5 l/min and 200 °C. The magnetic properties of the catalysts were performed using a Vibrating Sample Magnetometer (VSM) to study the activity of the catalysts before and after the steam reforming reactions. The VSM results indicate much higher activity in the microreactor compared to macro-reactor and Ni forms non-ferromagnetic species faster in the microreactor.


1987 ◽  
Vol 153 (Part_1_2) ◽  
pp. 27-36 ◽  
Author(s):  
H. Rosenberger ◽  
H. Bürger ◽  
H. Schütz ◽  
G. Scheler ◽  
G. Maenz

2002 ◽  
Vol 748 ◽  
Author(s):  
C. L. Zhao ◽  
Z. H. Wang ◽  
W. Zhu ◽  
O. K. Tan ◽  
H. H. Hng

ABSTRACTLead zirconate titanate (PZT) films are promising for acoustic micro-devices applications because of their extremely high electromechanical coupling coefficients and excellent piezoelectric response. Thicker PZT films are crucial for these acoustic applications. A hybrid sol-gel technology has been developed as a new approach to realize simple and cost-effective fabrication of high quality PZT thick films. In this paper, PZT53/47 thick films with a thickness of 5–50 μm are successfully deposited on Pt-coated silicon wafer by using the hybrid sol-gel technology. The obtained PZT thick films are dense, crack-free, and have a nano-sized microstructure. The processing parameters of this technology have been evaluated. The microstructure of the film has been observed using field-emission scanning electron microscopy and the crystallization process has been monitored by the X-ray diffraction. The thick films thus made are good candidates for fabrication of piezoelectric diaphragm which will be an essential element of microspeaker and microphone arrays.


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