The Effect of Sintering Temperature on the Physical Properties and Bending Strength of Zirconia Toughened Ceramic

2012 ◽  
Vol 519 ◽  
pp. 273-276
Author(s):  
Ze Quan Hua ◽  
Bin Zhang ◽  
Ji Hua Chen ◽  
Lian Jun Sun ◽  
Ying Zhang
Keyword(s):  
Flexural Strength ◽  
Physical Properties ◽  
Bending Strength ◽  
Sintering Temperature ◽  
Yttria Stabilized Zirconia ◽  
Surface Porosity ◽  
Stabilized Zirconia ◽  
Three Point Bending ◽  
Temperature Range ◽  
Press Method

This research investigated the effect of sintering temperature on the physical properties and bending strength of zirconia toughened ceramic (ZTC). 3mol% yttria-stabilized zirconia compacts were prepared by dry press method and then sintered with different final sintering temperature: 1490°C, 1530°C, 1570°C and 1610°C respectively. The physical properties and three-point bending strength were measured. The results of the test indicated that the density and shrinkage of ZTC increased along with the rise of sintering temperature, while the surface porosity of the samples decreased. The curve of flexural strength is indicated the variolation tendency of falling after rising, being the maximum at 1570°C. The results of this experiment showed that the best sintering temperature of yttria-stabilized zirconia was showed at 1570°C in terms of physical properties and bending strength among the selected temperature range.

Roughness and its effects on flexural strength of dental yttria-stabilized zirconia ceramics

2019 ◽  
Vol 739 ◽  
pp. 149-157 ◽  
Author(s):  
José Eduardo Vasconcellos Amarante ◽  
Marcos Venícius Soares Pereira ◽  
Grace Mendonça de Souza ◽  
Manuel Fellipe R. Pais Alves ◽  
Bruno Galvão Simba ◽  
...  
Keyword(s):  
Flexural Strength ◽  
Yttria Stabilized Zirconia ◽  
Stabilized Zirconia ◽  
Zirconia Ceramics

scholarly journals Flexural strength comparison of self-synthesised porcelain with the sintering temperature of 1150 degree Celsius and 1200 degree Celsius

2018 ◽  
Vol 30 (3) ◽  
pp. 194
Author(s):  
Joseph Gunawan ◽  
Dede Taufik ◽  
Veni Takarini ◽  
Zulia Hasratiningsih
Keyword(s):  
Flexural Strength ◽  
Bending Strength ◽  
Sintering Temperature ◽  
Testing Machine ◽  
Strength Test ◽  
Maturity Level ◽  
Natural Sand ◽  
Sintering Time ◽  
Universal Testing ◽  
Strength Formula

Introduction: Porcelain must have sufficient flexural strength to withstand mastication forces. The flexural strength of porcelain can be influenced by the maturity level of porcelain related to the temperature and sintering time. The purpose of this study was to compare the flexural strength of Indonesian natural sand self-synthesised porcelain with different sintering temperatures. Methods: Self-synthesised porcelain powder, with the composition of 65% Pangaribuan felspar, 25% Belitung silica, 5% Sukabumi kaolin, and 5% potassium salt, were condensed into 10 samples with the size of 7cm x 2cm x 0.4cm. A total of 5 samples were each burned at the temperature of 1150°C and 1200°C. Flexural strength test was performed using the Universal Testing Machine (Netzsch™) with the lowest load of 7.5 kg, and the data obtained was calculated using the bending strength formula. Result: The average flexural strength of self-synthesised porcelain at the sintering temperature of 1150°C was 26.678 MPa, while at the temperature of 1200°C was 39.038 MPa. Conclusion: This study concluded that Indonesian natural sand self-synthesised porcelain had a lower flexural strength at the sintering temperature of 1150°C than at the temperature of 1200°C.Keywords: Flexural strength, self-synthesised porcelain, sintering temperature.

Physical Properties of Vanillin Incorporated Self-Curing Orthodontic Polymethylmethacrylate Resin

2020 ◽  
Vol 853 ◽  
pp. 46-50
Author(s):  
Thongchai Poonpiriya ◽  
Pornrachanee Sawaengkit ◽  
Sroisiri Thaweboon ◽  
Pornkiat Churnjitapirom
Keyword(s):  
Flexural Strength ◽  
Physical Properties ◽  
Flexural Modulus ◽  
Orthodontic Appliances ◽  
Surface Porosity ◽  
Significance Level ◽  
Removable Orthodontic Appliances ◽  
Pmma Resin ◽  
One Way Anova

Polymethylmethacrylate (PMMA) resin is the main polymeric material used in removable orthodontic appliances. However, it can promote the adhesion of microbes due to its surface porosity and from long-term use. While vanillin incorporated PMMA resin has been reported to have antimicrobial effects against Candida albicans, the influence of vanillin incorporation on the physical properties of self-curing orthodontic PMMA resin has not been studied. Objective: To determine the flexural strength and flexural modulus of self-curing orthodontic PMMA resin incorporated with vanillin in different concentrations. Materials and methods: Three groups of self-curing orthodontic PMMA with incorporated vanillin concentrations of 0.1%, 0.5% as well as PMMA without vanillin as a control were prepared with ten specimens per group. Flexural strength and flexural modulus were tested by a 3-point bending machine according to ISO 20795-2:2013 specifications. One-way ANOVA and Tukey’s multiple comparison tests at a p<0.05 significance level were used to analyse the data. Results: The 0.1% vanillin incorporated group met ISO standard requirements (flexural strength = 60.48 MPa, flexural modulus = 1756.60 MPa), while the 0.5% vanillin incorporated group failed to pass this standard (flexural strength = 46.94 MPa, flexural modulus = 1423.49 MPa). The means of both flexural strength and flexural modulus showed significant differences among the three groups. Increasing the concentration of vanillin would decrease the flexural strength and flexural modulus of PMMA resin. Conclusion: The incorporation of vanillin into self-curing orthodontic PMMA resin can affect its physical properties, namely flexural strength and flexural modulus. At a concentration of 0.1% vanillin incorporation, PMMA resin displayed physical properties within the ISO standards.

Microstructure and Mechanical Properties of Multiscale Zirconia Ceramics Prepared by Field Assisted Sintering Technique

2016 ◽  
Vol 697 ◽  
pp. 354-359
Author(s):  
Khalid Eltayeb ◽  
Dong Qin Jin ◽  
Young Hwan Han ◽  
Fei Chen ◽  
Qiang Shen ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Flexural Strength ◽  
Yttria Stabilized Zirconia ◽  
Milling Machine ◽  
Stabilized Zirconia ◽  
Zirconia Ceramics ◽  
Dense Structure ◽  
Zirconia Composites ◽  
20 Nm ◽  
Field Assisted Sintering

Two kinds of powders of 3 mol. % yttria stabilized zirconia (3Y–TZP) with different particles sizes; one was 20 nm denoted by N whereas the other was 0.5 µm denoted by M, were mechanically mixed via ball milling machine using different amounts of N wt. % to obtain multiscale zirconia composite powder. Then the mixed powders were sintered by field assisted sintering technique (FAST). The effect of N content on the microstructure as well as on mechanical properties of zirconia is investigated. Results show that the microstructure of M completely surrounded by N emerged in zirconia composites, and tetragonal phase is presented in all the sintered samples. The obtained zirconia ceramics with 15 wt. % N own a highly dense structure (~ 99.9 % relative density) and high flexural strength of 813.59 MPa wherein a 15 % increase in flexural strength compared to zirconia ceramics without adding N, but the fracture toughness of the composites just lightly decreases. The improved flexural strength of the composites is caused by the multiscale effect.

High-T NOx Sensing Elements Using Conductive Oxides and Pt

2004 ◽  
Author(s):  
David L. West ◽  
Fred C. Montgomery ◽  
Timothy R. Armstrong
Keyword(s):  
Yttria Stabilized Zirconia ◽  
Step Response ◽  
Stabilized Zirconia ◽  
Temperature Range ◽  
Pt Electrodes ◽  
Recovery Times ◽  
Response And Recovery ◽  
Primary Variable

Development of NOx sensing elements intended for operation at T ∼600 °C are described. The elements were fabricated by depositing co-planar La1-x Srx BO3 (B = Cr, Fe) and Pt electrodes on yttria-stabilized zirconia substrates. Characterization of the elements included response to NO2 and NO as well as the [O2] dependence of the NO2 response. Much stronger (∼ 40 mV for 450 ppm NO2 in 7 vol% O2 at 600 °C) sensing responses were observed for NO2 than NO, indicating these elements are best suited for detection of NO2. Pronounced asymmetries were observed between the NO2 step response and recovery times for the elements, with temperature being the primary variable governing the recovery times in the temperature range 500–700 °C.

scholarly journals Physical and Electrical Properties of Yttria-Stabilized Zirconia Thin Films Prepared by Radio Frequency Magnetron Sputtering

10.14311/1743 ◽  
2013 ◽  
Vol 53 (2) ◽  
Author(s):  
Dmitriy A. Golosov ◽  
Sergey M. Zavatskiy ◽  
Sergey N. Melnikov
Keyword(s):  
Magnetron Sputtering ◽  
Radio Frequency ◽  
Xrd Analysis ◽  
Radio Frequency Magnetron ◽  
Yttria Stabilized Zirconia ◽  
Radio Frequency Magnetron Sputtering ◽  
Stabilized Zirconia ◽  
Temperature Range ◽  
Mobile Ions ◽  
Deposited Films

This paper presents the electrophysical characteristics of a 7 mol.% yttria-stabilized zirconia (YSZ) thin film deposited by radio-frequency magnetron sputtering. In order to form the crystallinestructure, the deposited films were annealed in air over a temperature range of 700 ÷ 900 °C. By XRD analysis it was established that as the deposited films were amorphous, they crystallized into a pure cubic structure as a result of annealing in air at a temperature above 820 °C.The electrophysical properties of YSZ films were investigated on structures such¨as Ni/YSZ/Pt/Ti/Si and Ni/YSZ/Si. Film features ? > 20 and tg ? < 0.05 were obtained. An estimate of the capacity-voltage characteristic proved that the Ni/YSZ/Si structures possessed a hysteresis. This hysteresis resulted from the drift of the mobile ions in the YSZ film. High-temperature ionic conductivity of the stabilized zirconia was determined by the measurements of the electric resistivity of the YSZ films at 1 kHz over the temperature range from ambient to 800 °C. The YSZ film conductivity obtained was 1.96 × 10-2 S/cm under 800 °C.

Thermal Cycling Effect on Mechanical Properties of Yttria-Stabilized Tetragonal Zirconia

2013 ◽  
Vol 538 ◽  
pp. 121-124
Author(s):  
Jing Zhang
Keyword(s):  
Mechanical Properties ◽  
Phase Transition ◽  
Thermal Expansion ◽  
Flexural Strength ◽  
Thermal Cycling ◽  
Tetragonal Zirconia ◽  
Yttria Stabilized Zirconia ◽  
Stabilized Zirconia ◽  
Optical Applications ◽  
The Stability

Yttria-stabilized zirconia (YSZ) is an important material in the area of energy and optical applications. In this study, the mechanical properties (Young’s modulus, Vickers hardness, flexural strength, and coefficient thermal expansion) and physical properties (phase transition) of yttria-stabilized tetragonal zirconia polycrystalline (Y-TZP) was reported. The effect of thermal cycling on the mechanical properties and the stability was also evaluated.

Fabrication of TiAl Intermetallic by Spark Plasma Sintering

2007 ◽  
Vol 336-338 ◽  
pp. 1050-1052 ◽  
Author(s):  
Hai Tao Wu ◽  
Yun Long Yue ◽  
Wei Bing Wu ◽  
Hai Yan Yin
Keyword(s):  
Mechanical Properties ◽  
Intermetallic Compounds ◽  
Spark Plasma Sintering ◽  
Bending Strength ◽  
Sintering Temperature ◽  
Three Point Bending ◽  
The Poor ◽  
High Relative Density ◽  
Plasma Sintering ◽  
Spark Plasma

The γ-TiAl intermetallic compounds were produced at the temperature ranging from 850°C to 1050°C by the Spark Plasma Sintering (SPS) process. The effects of sintering temperature and holding time on the mechanical properties of γ-TiAl intermetallic compounds were investigated. The γ-TiAl intermetallic compounds sintered at 1050°C for 10 min showed a high relative density more than 98%, and had the best three-point bending strength of 643MPa, fracture toughness of 12 MPa·m1/2 and microhardness of 560MPa. The microstructural observations indicated typical characteristics of intergranular fracture, which meant the poor ductility of γ-TiAl intermetallic compounds.

Synthesis and Properties of Composite Stabilized ZrO2

2013 ◽  
Vol 544 ◽  
pp. 68-71
Author(s):  
Jing Hui Cui ◽  
Tao Feng ◽  
Jin Feng Xia ◽  
Dan Yu Jiang ◽  
Ge Ming Liu ◽  
...  
Keyword(s):  
High Temperature ◽  
Sintering Temperature ◽  
Decomposition Temperature ◽  
Yttria Stabilized Zirconia ◽  
Stabilized Zirconia ◽  
Muffle Furnace ◽  
Flexure Strength ◽  
Different Temperatures ◽  
Zirconia Electrolyte

Through Mechanical grounding method, CaZrO3 – 8YSZ(8% in mol yttria stabilized zirconia) electrolyte samples with different amounts of CaZrO3 at 10wt%, 20wt%, 30wt% were sintered at different temperatures in Muffle furnace. The decomposition temperature of CaZrO3 is 825°C-900°C under one atmosphere. At high temperature, CaZrO3 decomposes into CaO and ZrO2. So Y2O3-CaO-ZrO2 complex is composed. The effects of the sintering temperature and the contents of the CaZrO3 on the conductivity, porosity, flexure strength, hardness were investigated. XRD and SEM were used to analyse the compositions and microcosmic morphology.

Performance Investigation of Dual Layer Yttria-Stabilized Zirconia–Samaria-Doped Ceria Electrolyte for Intermediate Temperature Solid Oxide Fuel Cells

2016 ◽  
Vol 13 (1) ◽  
Author(s):  
Ryan J. Milcarek ◽  
Kang Wang ◽  
Michael J. Garrett ◽  
Jeongmin Ahn
Keyword(s):  
Fuel Cell ◽  
Buffer Layer ◽  
Sintering Temperature ◽  
Solid Oxide ◽  
Yttria Stabilized Zirconia ◽  
Cell Performance ◽  
Doped Ceria ◽  
Oxide Fuel ◽  
Stabilized Zirconia ◽  
Fuel Cell Performance

The performance of yttria-stabilized zirconia (YSZ)–samaria-doped ceria (SDC) dual layer electrolyte anode-supported solid oxide fuel cell (AS-SOFC) was investigated. Tape-casting, lamination, and co-sintering of the NiO–YSZ anode followed by wet powder spraying of the SDC buffer layer and BSCF cathode was proposed for fabrication of these cells as an effective means of reducing the number of sintering stages required. The AS-SOFC showed a significant fuel cell performance of ∼1.9 W cm−2 at 800 °C. The fuel cell performance varies significantly with the sintering temperature of the SDC buffer layer. An optimal buffer layer sintering temperature of 1350 °C occurs due to a balance between the YSZ–SDC contact and densification at low sintering temperature and reactions between YSZ and SDC at high sintering temperatures. At high sintering temperatures, the reactions between YSZ and SDC have a detrimental effect on the fuel cell performance resulting in no power at a sintering temperature of 1500 °C.

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