Fabric Finishing with Flame Retardant Coating

2016 ◽  
Vol 721 ◽  
pp. 409-413 ◽  
Author(s):  
Arita Micule ◽  
Skaidrite Reihmane ◽  
Ilze Baltina

Due to its wide application improvement of fire protection of materials has always been topical. Aim of the research is to render textile materials less flammable in an economically and environmentally friendly manner using modified commercial products. Plain wave cotton fabric pretreated with cyclic phosphonate flame retardant (FR) Itoflam PES was used in experiments. Printing pastes Printperfect LAC 60, Tubiscreen EX-TS and Printperfect EX-AR with additive antimony trioxide (Sb2O3) were used for additional treatment of cotton fabric via flat screen coating method. FR properties, physico – mechanical characteristics (tensile strength, elongation, stiffness, abrasion resistance) were examined. It is concluded that foamed coating increases the stiffness and abrasion resistance of material. Recommendations for material application are given.

Polymers ◽  
2020 ◽  
Vol 12 (7) ◽  
pp. 1575
Author(s):  
Huong Nguyen Thi ◽  
Khanh Vu Thi Hong ◽  
Thanh Ngo Ha ◽  
Duy-Nam Phan

Cotton fabric treated by Pyrovatex CP New (PCN) and Knittex FFRC (K-FFRC) using the Pad-dry-cure method showed an excellent fire-retardant effect. However, it needed to be cured at high temperatures for a long time leading to a high loss of mechanical strength. In this study, atmospheric-pressure dielectric barrier discharge (APDBD) plasma was applied to the cotton fabric, which then was treated by flame retardants (FRs) using the pad–dry-cure method. The purpose was to have a flame-retardant cotton fabric (limiting oxygen index (LOI) ≥ 25) and a mechanical loss of the treated fabric due to the curing step as low as possible. To achieve this goal, 10 experiments were performed. The vertical flammability characteristics, LOI value and tensile strength of the treated fabrics were measured. A response model between the LOI values of the treated fabric and two studied variables (temperature and time of the curing step) was found. It was predicted that the optimal temperature and time-to-cure to achieve LOI of 25 was at 160 °C for 90 s, while the flame-retardant treatment process without plasma pretreatment, was at 180 °C and 114 s. Although the curing temperature and the time have decreased significantly, the loss of mechanical strength of the treated fabric is still high. The tensile strength and scanning electron microscopy (SEM) images of the fabric after plasma activation show that the plasma treatment itself also damages the mechanical strength of the fabric. X-ray photoelectron spectroscopy (XPS) spectra of the fabric after plasma activation and energy-dispersive spectroscopy (EDS) analysis of the flame retardant-treated (FRT) fabric clarified the role of plasma activation in this study.


2009 ◽  
Vol 16 (05) ◽  
pp. 715-721 ◽  
Author(s):  
CHAOXIA WANG ◽  
LI CHEN

The silica sol was applied onto 1, 2, 3, 4-butanetetracarboxylic acid (BTCA) finished cotton fabrics with the attempt to improve the physical properties especially the tensile strength which had a big loss in the previous anti-crease finishing processing. The parameters including the dosage of the coupling agent, the concentration and pH of the sol and the processing methods were studied in detail. Compared to the sample finished with BTCA, 11.8% of the increase in the crease recovery angle and 18.6% of the enhancement in the tensile strength of the cotton fabric also treated with silica sol in the better selected conditions were obtained. The abrasion resistance was also improved.


2019 ◽  
Vol 50 (3) ◽  
pp. 278-292 ◽  
Author(s):  
Khaled Mostafa ◽  
Heba Ameen ◽  
Mahmoud Morsy ◽  
Amal el-ebiassy ◽  
Azza El-Sanabary ◽  
...  

To minimize the serious defects of durable press finishing of cellulosic textiles with respect to the great loss in strength properties, new pioneering strengthening approach of cotton fabric based on our previously prepared starch nanoparticles of size around 80–100 nm was used. For this purpose, cotton fabrics were treated with different concentrations of starch nanoparticles via coating technique using pad-dry-cure method, at which the starch nanoparticles are attached to the fabrics with the use of a padder adjusted to appropriate pressure and speed, followed by drying and curing. Fabric stiffness, surface roughness, tensile strength, elongation at break, abrasion resistance, wrinkle recovery angles, add-on %, and degree of whiteness as well as durability of treated fabrics were fully explored. SEM was used for detecting the change in surface morphology of reinforced coated fabric. The results obtained reflect the following findings: (a) all fabric performance like tensile strength, stiffness, wrinkle recovery angle, abrasion resistance and add on % were improved for coated fabrics with starch nanoparticles in comparison with untreated fabric, except that of surface roughness; (b) SEM confirmed the change in surface morphology of cotton fabric after reinforcement treatment using starch nanoparticles; (c) the dry wrinkle recovery angle and tensile strength of cotton fabrics treated in presence of 30 g/l starch nanoparticles are slightly decreased after 10 washing cycles as compared with untreated fabric; and (d) starch nanoparticles introduce an advance in textile finishing with respect to the above-mention fabric performance except that of surface roughness.


2008 ◽  
Vol 15 (06) ◽  
pp. 833-839 ◽  
Author(s):  
CHAOXIA WANG ◽  
MAO LI ◽  
MIN WU ◽  
LI CHEN

The properties of the cotton fabric with water-repellence finishing by sol method with the hexadecyltrimethoxysilane as additive were observed. The cotton fabrics were immersed in the prepared sols with double dip and double nip dried at 90°C, annealed at 160°C for 3 min. The water repellence and the physical properties such as gas permeability, bending properties, beetling properties, tensile strength, elongation at break, abrasion resistance, and anti-crease properties of the cotton fabrics were investigated. The results showed that anti-crease and tensile strength were improved. However, the abrasion resistance of the cotton fabrics decreased in some way. Both the bending and beetling properties measurement proved that the handle of the treated cotton fabrics changed stiffness. For the dyed fabrics by the water-repellent finishing, the hue was slightly changed, the deeper color was achieved. There is no adverse effect for treated fabric by water-repellent finishing on the fastness.


2020 ◽  
Vol 7 (4) ◽  
pp. 9-14
Author(s):  
Pengshuang He ◽  
Chaohong Dong ◽  
Xiaoyan Chen ◽  
Peng Wang ◽  
Zhou Lu ◽  
...  

Flame resistant cotton fabric is usually dyed first, and is then treated with a flame retardant by the pad-dry-cure technique. In this research, cotton fabric was treated with 2-(2-aminoethyl hydrogen phosphite)-4,6-dichloro-1,3,5-triazine (APDCT). APDCT contains s-triazine groups, which are the same used by reactive dyes. This process allows cotton fabric dyeing and flame retardant treatment to occur simultaneously, while decreasing treatment temperature, improving efficiency, and saving energy. Optimal treatment was determined by the percent dye uptake, fixation, and fabric flame resistance. The color fastness to rubbing of the treated cotton fabric was almost unchanged. The tensile strength of the treated cotton fabric was slightly reduced.


2021 ◽  
Vol 72 (03) ◽  
pp. 315-323
Author(s):  
NGUYEN THI HUONG ◽  
VU THI HONG KHANH ◽  
NGUYEN PHAM DUY LINH

In this study, the flame-retardant treatment for cotton fabric has been done by using the commercial organophosphoruscompounds labelled Pyrovatex CP New (PR). Knittex FFRC (K), a formaldehyde-free crosslinking agent, has been usedto enhance the link between Pyrovatex CP New and Cellulose molecules. The flame-retardant treatment process forcotton fabric has been done by the pad-dry-cure technique. The purpose of the study is to predict the optimal PyrovatexCP New and Knittex FFRC concentrations with the highest fire resistance efficiency, minimum loss for mechanicalproperties and minimum formaldehyde release for the treated fabric. To achieve this goal, the response surfacemethodology (RSM) was used to find the relationship between the controlled experimental factors and the observedresults. The central composite design type face centred (CCF) was applied as experimental design. According to thisexperimental design, 10 experiments were carried out. The chemical uptake rate, vertical flammability characteristics,LOI value, tensile strength and formaldehyde-free content of the untreated and treated samples were determined. Fourresponse models between the reagent concentrations and the add-on amount, LOI value, warp and weft tensile strengthof the treated fabric were obtained by the assistance of software Design-Expert V 10.0.8. The R-squared values of thesemodels were above 80% confirming their significances. The optimal conditions when combining three parameters (LOI,warp tensile strength and weft tensile strength) were selected as 450 g/l Pyrovatex CP New and 107,575 g/l KnittexFFRC with the assistance of Design-Expert software


Coatings ◽  
2021 ◽  
Vol 11 (10) ◽  
pp. 1147
Author(s):  
Jingda Huang ◽  
Mengmeng Li ◽  
Changying Ren ◽  
Wentao Huang ◽  
Qiang Wu ◽  
...  

Cotton fabric, as an important material, is suffering from some defects such as flammability, easy pollution and so on; therefore, it is important to make a flame-retardant and superhydrophobic modification on cotton fabric. In this study, we demonstrated a preparation of high-efficiency flame-retardant and superhydrophobic cotton fabric with double coated construction by a simple multi-step dipping. First, the fabric was immersed in branched poly(ethylenimine) (BPEI) and ammonium polyphosphate (APP) water dispersions successively, and then immersed in polydimethylsiloxane (PDMS)/cellulose nanocrystals (CNC)-SiO2 toluene dispersion to form a BPEI/APP/PDMS/CNC-SiO2 (BAPC) composite coating on the surface of the cotton fabric. Here, the hydrophobic modified CNC-SiO2 rods were used to construct the superhydrophobic layer and the BPEI/APP mixture was used as the flame-retardant layer, as well as SiO2 particles which could further improve the flame-retardant effect. PDMS was mainly used as an adhesive between the BPEI/APP layer and the CNC-SiO2 layer. The resulting cotton fabric shows outstanding flame-retardant properties, in that the value of oxygen index meter (LOI) reaches 69.8, as well as excellent superhydrophobicity, in that the water contact angle (WCA) is up to 156.6°. Meanwhile, there is a good abrasion resistance, the superhydrophobicity is not lost until the 16th abrasion cycles and the flame retardant retains well, even after 100 abrasion cycles in an automatic vertical flammability cabinet under a pressure of 8.8 kPa.


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