Evolution of the Microstructure and Mechanical Properties of the Ultrafine-Grained VT8M-1 during Isothermal Die Forging and Thermal Treatment

2021 ◽  
Vol 1016 ◽  
pp. 418-422
Author(s):  
Grigory Dyakonov ◽  
Tatyana Vitalyevna Yakovleva ◽  
Andrey Stotskiy ◽  
Askar Ibatullin ◽  
Irina Semenova
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Thermal Treatment ◽  
Secondary Phase ◽  
Initial State ◽  
Rotary Swaging ◽  
Α Phase ◽  
Die Forging ◽  
Ultrafine Grained ◽  
Mean Size

The work addresses the microstructural evolution and mechanical properties of the ultrafine-grained (UFG) VT8M-1 subjected to isothermal die forging (IDF) and subsequent thermal treatment. An UFG microstructure with a mean size of secondary grains of about 0.3 μm was processed by a rotary swaging (RS) at Т=780°С. The ultimate tensile strength (UTS) of the alloy increased by 23% as compared to an initial state due to the formation of an UFG microstructure. It has been shown that isothermal die forging of the UFG alloy at Т=780°С leads to the growth of secondary phase grains by 0.7 μm. Subsequent heat treatment of the forged billets leads to hardening of 11%, which can be attributed both to the formation of additional interphase α/β boundaries at the precipitation of a tertiary α-phase and silicide dispersion.

Ultrafine-Grained Treatment Process on FGH4096 Alloy

2009 ◽  
Vol 407-408 ◽  
pp. 694-697 ◽  
Author(s):  
Yong Quan Ning ◽  
Ze Kun Yao ◽  
Hong Zhen Guo ◽  
Tao Yu ◽  
Yi Wen Zhang
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Room Temperature ◽  
Treatment Process ◽  
Secondary Phase ◽  
Ultrafine Grain ◽  
Structure And Properties ◽  
Dual Property ◽  
Ultrafine Grained ◽  
Turbine Disc

Ultrafine-grained treatment (multiple forging and heat treatment) were carried out on FGH4096 alloy to get ultrafine grain with grain being of 1-5μm. OM, SEM, TEM and tensile test were used to study the action of ultrafine-grained treatment on improving structure and properties. The tensile properties of the alloy processed under ultrafine-grained treated have shown quite satisfactory levels, which ultimate strength (UTS) reach 1730Mpa and yield strength (YS) values reach 1470Mpa at room temperature. The apperance of advanced strength has originated chiefly form not only the persence of fine grains, but also structure of grain boundaries and diaperce pricipitations of secondary phase. A better combination of mechanical properties achieved by use of ultrafine-grained treatment makes it possible to explore the dual property turbine disc to its maximum potential for FGH 4096 alloy.

The Effects of Heat Treatment on the Chemical Alterations of Oak Wood

2016 ◽  
Vol 688 ◽  
pp. 44-49 ◽  
Author(s):  
Iveta Čabalová ◽  
František Kačík ◽  
Tereza Tribulová
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
High Performance Liquid Chromatography ◽  
Renewable Energy ◽  
Liquid Chromatography ◽  
Thermal Treatment ◽  
High Performance ◽  
Treated Wood ◽  
National Renewable Energy Laboratory ◽  
Oak Wood

Samples prepared from oak (Quercusrobur L.) wood were exposed to heat treatment at temperatures of 160, 180, 200 and 220 oC for 3, 6, 9 and 12 hours. In both untreated and thermally treated wood there were determined extractives and lignin by National Renewable Energy Laboratory (NREL) procedures, cellulose by Seifert's method, holocellulose according to Wise, hemicelluloses as difference between holocellulose and cellulose. Monosaccharides were determined by high performance liquid chromatography (NREL).The results show that hemicelluloses are less stable at thermal treatment than cellulose. The amounts of lignin and extractives rose by increasing both temperature and time of the treatment while the amounts of hemicelluloses decreased. Thermal treatment also resulted in significant decreases of the yields of non-glucosic saccharides. Degradation of carbohydrates can cause the deterioration of mechanical properties of wood.

Heat treatememt effect on microstructure and mechanical properties of precipitation hardening elinvar alloy

2021 ◽  
pp. 68-73
Author(s):  
G.V. Shlyakhova ◽  
◽  
A.V. Bochkareva ◽  
M.V. Nadezhkin ◽  
◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Phase Composition ◽  
Structural Analysis ◽  
Thermal Treatment ◽  
Precipitation Hardening ◽  
Physical And Mechanical Properties ◽  
Alloy Structure ◽  
Treatment Mode ◽  
Elinvar Alloy

This study presents experimental results of structural analysis, such as phase composition, grains size assessment, strength and hardness of Ni-SPAN-C alloy 902 after various heat treatment modes (hardening and aging for stress relaxation). A thermal treatment mode has been selected to obtain higher physical and mechanical properties of the elinvar alloy. It is shown that the improvement of the alloy structure in thermal treatment occurs due to the thermic stresses, as well as the formation and dissolution of intermetallides.

scholarly journals The Effect of Heat Treatment on the Microstructure and Mechanical Properties of the Novel Low-Cost Ti-3Al-5Mo-4Cr-2Zr-1Fe Alloy

Materials ◽  
2020 ◽  
Vol 13 (17) ◽  
pp. 3798
Author(s):  
Meng Sun ◽  
Dong Li ◽  
Yanhua Guo ◽  
Ying Wang ◽  
Yuecheng Dong ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Aging Time ◽  
Volume Fraction ◽  
Low Cost ◽  
Solution Treatment ◽  
Solution Temperature ◽  
The Novel ◽  
Α Phase ◽  
The Cost

In order to reduce the cost of titanium alloys, a novel low-cost Ti-3Al-5Mo-4Cr-2Zr-1Fe (Ti-35421) titanium alloy was developed. The influence of heat treatment on the microstructure characteristics and mechanical properties of the new alloy was investigated. The results showed that the microstructure of Ti-35421 alloy consists of a lamina primary α phase and a β phase after the solution treatment at the α + β region. After aging treatment, the secondary α phase precipitates in the β matrix. The precipitation of the secondary α phase is closely related to heat treatment parameters—the volume fraction and size of the secondary α phase increase when increasing the solution temperature or aging time. At the same solution temperature and aging time, the secondary α phase became coarser, and the fraction decreased with increasing aging temperature. When Ti-35421 alloy was solution-treated at the α + β region for 1 h with aging surpassing 8 h, the tensile strength, yield strength, elongation and reduction of the area were achieved in a range of 1172.7–1459.0 MPa, 1135.1–1355.5 MPa, 5.2–11.8%, and 7.5–32.5%, respectively. The novel low-cost Ti-35421 alloy maintains mechanical properties and reduces the cost of materials compared with Ti-3Al-5Mo-5V-4Cr-2Zr (Ti-B19) alloy.

scholarly journals Influence of the energy electron beam exposure regimes on the structure and mechanical properties of composite coatings

2020 ◽  
pp. 23-27
Author(s):  
T.A. Krylova ◽  
◽  
Y.A. Chumakov ◽  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Wear Resistance ◽  
Electron Beam ◽  
Structural Changes ◽  
Composite Coatings ◽  
Initial State ◽  
Austenitic Structure ◽  
Solid Carbide ◽  
Soft Ferrite

The effect of heat treatment on the structure and properties of composite coatings based on chromium carbide with titanium carbide fabricated by non-vacuum electron beam cladding without has been studied. It was shown that tempering leads to a decrease in microhardness and wear resistance, which is associated with the decomposition of the austenitic structure with the formation of a soft ferrite-carbide structure. The post heat treatment tempering was showed to decrease of microhardness and wear resistance, which leads to the decomposition of the austenitic structure with the formation of a soft ferrite-carbide structure. The bulk quenching of coatings after tempering leads to an increase in microhardness comparable to the values of microhardness in the initial state after electron beam cladding, due to the formation of high hard martensite. The wear resistance of composite coatings after tempering is lower than after cladding due to brittle martensite, which is not able to hold solid carbide particles. The composite coatings obtained at the optimal processing conditions have a combination of improved properties and do not require additional heat treatment, resulting in structural changes, causing a decrease in mechanical properties.

The Influence of Severe Plastic Deformation Process on Structure and Properties of AZ 31 Alloy after Selected Heat Treatment

2018 ◽  
Vol 275 ◽  
pp. 134-146
Author(s):  
Stanislav Rusz ◽  
Ondřej Hilšer ◽  
Stanislav Tylšar ◽  
Lubomír Čížek ◽  
Tomasz Tański ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Plastic Deformation ◽  
Severe Plastic Deformation ◽  
Structure Refinement ◽  
Hardness Measurement ◽  
Az31 Alloy ◽  
Strength Properties ◽  
Aviation Industry ◽  
Initial State

The technology of structure refinement in materials with the aim of achieving substantial mechanical properties and maintaining the required plasticity level is becoming increasingly useful in industrial practice. Magnesium alloys are very progressive materials for utilization in practice thanks to their high strength-to-weight ratios (tensile strength/density). The presented paper analyses the effect of the input heat treatment of the AZ31 alloy on the change of structure and strength properties through the process of severe plastic deformation (SPD), which finds an increasing utilization, especially in the automotive and aviation industry. For the study of the influence of the SPD process (ECAP method) on the properties of the AZ31 alloy, two types of thermal treatment of the initial state of the structure were selected. The analysis of the structure of the AZ31 alloy was performed in the initial state without heat treatment and subsequently after heat treatment. In the next part, the influence of the number of passes on the strengthening curves was evaluated. Mechanical properties of the AZ31 alloy after ECAP were evaluated by hardness measurement and completed by structure analysis.

Formability of Ultrafine-Grained AA6016 Sheets Processed by Accumulative Roll Bonding

2012 ◽  
Vol 504-506 ◽  
pp. 575-580 ◽  
Author(s):  
Tina Hausöl ◽  
Christian W. Schmidt ◽  
Verena Maier ◽  
Wolfgang Böhm ◽  
Hung Nguyen ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Laser Heat Treatment ◽  
Bending Tests ◽  
Roll Bonding ◽  
Laser Heat ◽  
Heat Treated ◽  
Ultrafine Grained ◽  
Ultrafine Grained Microstructure ◽  
Bending Behaviour

Aluminium alloy AA6016 was accumulative roll bonded up to eight cycles in order to produce an ultrafine-grained microstructure. The formability of these sheets was investigated by means of bending tests. Furthermore the influence of a local laser heat treatment at the bending edge is observed. The strength of the UFG samples is increased by a factor of around two compared to the conventionally grained T4 condition which also results in up to 50 % higher punch forces needed for bending of ARB processed samples. An anisotropic bending behaviour is observed. By applying a tailored laser heat treatment along the bending edge prior to the bending tests a local recrystallization and recovery at the deformation zone of the samples is achieved. Thus, ductility is increased locally whereby bending to an angle of 80° is possible with lower forming forces compared to the non-heat treated specimens. The results are compared to previous studies on mechanical properties and formability investigations of ARB processed AA6016.

Microstructure and Mechanical Properties of Ti-6Al-4V Alloy Samples Fabricated by Selective Laser Melting

2018 ◽  
Vol 770 ◽  
pp. 179-186 ◽  
Author(s):  
Jing Bo Gao ◽  
Xiao Li Zhao ◽  
Ju Kun Yue ◽  
Meng Chao Qi ◽  
De Liang Zhang
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Crystal Growth ◽  
Yield Strength ◽  
Selective Laser Melting ◽  
Lamellar Structure ◽  
Growth Direction ◽  
Laser Melting ◽  
Α Phase ◽  
Dog Bone

Ti-6Al-4V (wt%) alloy samples with dog-bone and box shapes respectively were fabricated by selective laser melting (SLM). The microstructures and mechanical properties of the 3D printed Ti-6Al-4V samples with and without heat treatment were characterized and tested. The microstructures of the as-fabricated dog-bone shaped samples were mainly composed of acicular α’ phase. After annealing at 700°C, the acicular α’ phase changed into an α/β lamellar structure. After solution treatment at 955°C, water quenching and aging at 550°C, the microstructure was mainly composed of primary α phase and α/β lamellar structure. The optimum heat treatment is annealing, and the mechanical properties of the annealed sample are as follows: yield strength: 1015 MPa, ultimate tensile strength (UTS): 1083 MPa and elongation to fracture: 7.9%. The microstructures of the box-shaped samples after annealing mainly consist of α phase and α/β lamellar structure. When stretched along the direction parallel to the crystal growth direction, the yield strength and UTS of the sample are 1054 and 1090 MPa，and its elongation to fracture is 6.3%. When stretched along the direction perpendicular to the crystal growth direction, the yield strength and UTS of the sample are 1019 and 1068 MPa respectively, and its elongation to fracture is 8.7%.

scholarly journals Influence of Microstructural Morphology on Hydrogen Embrittlement in a Medium-Mn Steel Fe-12Mn-3Al-0.05C

Metals ◽  
2019 ◽  
Vol 9 (9) ◽  
pp. 929 ◽  
Author(s):  
Xiao Shen ◽  
Wenwen Song ◽  
Simon Sevsek ◽  
Yan Ma ◽  
Claas Hüter ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
The Other ◽  
Duplex Microstructure ◽  
Ultrafine Grained ◽  
Medium Mn Steel ◽  
Microstructural Morphology ◽  
Cold Rolled ◽  
Mixed Microstructure ◽  
Mn Steel

The ultrafine-grained (UFG) duplex microstructure of medium-Mn steel consists of a considerable amount of austenite and ferrite/martensite, achieving an extraordinary balance of mechanical properties and alloying cost. In the present work, two heat treatment routes were performed on a cold-rolled medium-Mn steel Fe-12Mn-3Al-0.05C (wt.%) to achieve comparable mechanical properties with different microstructural morphologies. One heat treatment was merely austenite-reverted-transformation (ART) annealing and the other one was a successive combination of austenitization (AUS) and ART annealing. The distinct responses to hydrogen ingression were characterized and discussed. The UFG martensite colonies produced by the AUS + ART process were found to be detrimental to ductility regardless of the amount of hydrogen, which is likely attributed to the reduced lattice bonding strength according to the H-enhanced decohesion (HEDE) mechanism. With an increase in the hydrogen amount, the mixed microstructure (granular + lamellar) in the ART specimen revealed a clear embrittlement transition with the possible contribution of HEDE and H-enhanced localized plasticity (HELP) mechanisms.

Structure Evolution of Thermotropic Polymers by Thermal Annealing. A Light and X-Ray Scattering Study

2015 ◽  
Vol 1765 ◽  
pp. 65-70
Author(s):  
Adriana Reyes-Mayer ◽  
Angel Romo-Uribe ◽  
Michael Jaffe
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Thermal Treatment ◽  
Structure Evolution ◽  
Wide Angle ◽  
Extrusion Axis ◽  
X Ray ◽  
X Ray Scattering ◽  
Extruded Films ◽  
Ray Scattering

ABSTRACTSmall-angle light scattering (SALS) and wide-angle X-ray scattering (WAXS) were used to study the influence of heat treatment on the texture and microstructure of extruded films of high-performance thermotropic liquid crystal polymers (LCPs). The microstructure was correlated with tensile mechanical properties. LCPs based on random units of hydroxybenzoic acid (B), hydroxynaphthoic acid (N), terephthalic acid (TA) and biphenol (BP) were supplied by the former Hoechst Celanese Corp. as 50 μm thick extruded films. The LCPs, denoted B-N, COTBP and RD1000, have B and N as common co-monomers and vary the other co-monomers. Thus, this study also enabled the investigation of the influence of monomer composition on microstructure and mechanical properties. Heat treatments were carried out at temperatures close to the solid-to-nematic transition (Ts→n) for periods up to 5 h, under dry air conditions. The thermal treatment produced either two endotherms or a small increase of Ts→n (B-N and RD1000), or Ts→n increased significantly (COTBP). Moreover, when heat treatment was carried out approximately 40°C below the respective Ts→n, the mechanical Young’s modulus, E, along the extrusion axis increased for all LCPs. Strikingly, for COTBP, E increased over 100% relative to the as-extruded film. The results also showed that the optimum treatment time for improving the Young modulus was between 3 and 4 h. Wide-angle X-ray scattering showed a significant sharpening of crystalline reflections and concentration of the 002 meridional reflection as a result of thermal treatment, suggesting the elimination of defects and a better alignment of the molecular chains along the extrusion axis. This would explain the increase in tensile modulus.

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