Dislocation Microstructure in Copper Multicrystals Deformed under the Sequences: Rolling - Tension and Tension - Rolling

2006 ◽  
Vol 514-516 ◽  
pp. 589-593 ◽  
Author(s):  
Nataliya A. Sakharova ◽  
José Valdemar Fernandes

The microstructure evolution of copper multicrystalline sheets, undergoing plastic deformation in the sequences of strain paths rolling – tension and tension – rolling, was studied in the present work. For both sequences, two different types of change of strain path were studied: the tensile and rolling directions were parallel and normal to each other. Samples submitted to these four complex strain paths were investigated by transmission electron microscopy (TEM). TEM observations have shown the typical dislocations microstructures for the prestrain paths in tension and rolling. The dislocation microstructures observed during the second path were analysed and discussed as a function of the sequence and of the type of strain path change (parallel and normal sequential paths). Special microbands features were observed during the second path, for both sequences, rolling – tension and tension – rolling. The appearance of such microstructural features is discussed in terms of the sequence and type of strain path change and it is linked with the slip activity during the second deformation mode.

2007 ◽  
Vol 550 ◽  
pp. 363-368
Author(s):  
R.L. Higginson

The effect of strain path on an aluminium-manganese alloy has been studied using single pass rolling and simple compression tests. Strain paths of 0, 90 and180° have been studied in terms of texture development and recrystallisation behaviour and compared with equivalent positions in the rolled slab. The effects of the individual deformations on the dislocation sub-structure have been studied using transmission electron microscopy. The study has shown that although samples can be deformed to the same strain via nominally the same stain path change the deformation mode can fundamentally influence the sub-structure developed during each deformation stage.


1995 ◽  
Vol 10 (4) ◽  
pp. 791-794 ◽  
Author(s):  
S. Stemmer ◽  
S.K. Streiffer ◽  
W-Y. Hsu ◽  
F. Ernst ◽  
R. Raj ◽  
...  

We have used conventional and high-resolution transmission electron microscopy to investigate the microstruture of epitaxial, ferroelectric PbTiO3 films grown by pulsed laser ablation on (001) MgO single crystals, and on MgO covered with epitaxial Pt or SrTiO3. Pronounced variations are found in the widths and lengths of a-axis-oriented domains in these films, although the volume fraction of a-axis-oriented material varies only weakly for the different types of samples. In addition, the films deposited onto Pt-coated MgO have a larger grain size than those deposited onto bare MgO or SrTiO3/MgO. Possible reasons for the variations in the distribution of a-axis-oriented material in these samples include differences in the elastic properties and electrical conductivities of the different substrate combinations.


2010 ◽  
Vol 18 (4) ◽  
pp. 10-13 ◽  
Author(s):  
Kuniaki Nagayama ◽  
Radostin Danev ◽  
Hideki Shigematsu ◽  
Naoki Hosogi ◽  
Yoshiyuki Fukuda ◽  
...  

Theoretically, transmission electron microscopy (TEM) is compatible with three different types of phase plate: thin-film, electrostatic, and magnetic. However, designing functional phase plates has been an arduous process that has suffered from unavoidable technical obstacles such as phase-plate charging and difficulties associated with micro-fabrication of electrostatic and magnetic phase plates. This review discusses phase-contrast schemes that allow visualization of transparent objects with high contrast. Next it deals with recent studies on biological applications ranging from proteins and viruses to whole cells. Finally, future prospects for overcoming the problem of phase-plate charging and for designing the next generation of phase-plates to solve the problem of electron loss inherent in thin-film phase plates are discussed.


1985 ◽  
Vol 58 ◽  
Author(s):  
A.R. Bhatti ◽  
J.C. Barry ◽  
B Cantor

ABSTRACTAmorphous and partially crystalline Fe7 8B1 3 Si9 alloys have been examined by high resolution transmission electron microscopy at 200kV. In lattice imaging mode, the as-quenched alloy shows small regions, with a mean size of - 20Å, consisting of well defined patterns of fringes. Three different types of crystals can be identified at the very earliest stages of crystallisation of the alloy.


Minerals ◽  
2021 ◽  
Vol 11 (9) ◽  
pp. 1018
Author(s):  
Sejin Jung ◽  
Takafumi Yamamoto ◽  
Jun-ichi Ando ◽  
Haemyeong Jung

Amphibole peridotite samples from Åheim, Norway, were analyzed to understand the deformation mechanism and microstructural evolution of olivine and amphibole through the Scandian Orogeny and subsequent exhumation process. Three Åheim amphibole peridotite samples were selected for detailed microstructural analysis. The Åheim amphibole peridotites exhibit porphyroclastic texture, abundant subgrain boundaries in olivine, and the evidence of localized shear deformation in the tremolite-rich layer. Two different types of olivine lattice preferred orientations (LPOs) were observed: B- and A-type LPOs. Electron backscatter diffraction (EBSD) mapping and transmission electron microscopy (TEM) observations revealed that most subgrain boundaries in olivine consist of dislocations with a (001)[100] slip system. The subgrain boundaries in olivine may have resulted from the deformation of olivine with moderate water content. In addition, TEM observations using a thickness-fringe method showed that the free dislocations of olivine with the (010)[100] slip system were dominant in the peridotites. Our data suggest that the subgrain boundaries and free dislocations in olivine represent a product of later-stage deformation associated with the exhumation process. EBSD mapping of the tremolite-rich layer revealed intracrystalline plasticity in amphibole, which can be interpreted as the activation of the (100)[001] slip system.


2014 ◽  
Vol 44 (4) ◽  
pp. 660-665 ◽  
Author(s):  
Marlúcia Souza Pádua ◽  
Luciano Vilela Paiva ◽  
Luciano Coutinho da Silva ◽  
Kalynka Gabriella do Livramento ◽  
Eduardo Alves ◽  
...  

The aim of this research was to characterize and compare two types of calli from leaf explants of Coffea arabica (cultivar Catiguá). Cells of different types of callus were successfully characterized regarding viability and internal and external morphological characteristics. It was obtained two morphologically distinct types of callus: (i) yellow friable and (ii) transparent watery. The yellow friable calli showed higher cell viability and embryogenic characteristics. Scanning and transmission electron microscopy showed embryogenic characteristics in cells of the yellow friable calli evidenced by the presence of small and isodiametric cells, while transparent watery calli showed elongated cells and large cytoplasm vacuolization.


2007 ◽  
Vol 340-341 ◽  
pp. 883-888 ◽  
Author(s):  
Ichiro Shimizu ◽  
Naoya Tada

Biaxial compression tests with an abrupt strain path change have been performed on polycrystalline aluminum to investigate the plastic deformation behavior under complex strain histories. Attentions are paid especially to the rapid change in the normal stresses due to the abrupt strain path change. The influences of the prestrain amplitude and the angular relation of sequential strain paths on the stress changes were also studied. The results showed that the transient increase of the normal stresses related to the latent hardening phenomenon with strain path change as well as the plastic anisotropy increase with the pre-straining amplitude. The transient increase in the stress was also affected by the strain histories in the sequential compression tests with the strain path change. The transient stress increment became large to the maximum then decreases with the angle between the sequential paths.


Polymers ◽  
2020 ◽  
Vol 12 (9) ◽  
pp. 1984
Author(s):  
Chun Yan Gao ◽  
Min Hwan Kim ◽  
Hyoung-Joon Jin ◽  
Hyoung Jin Choi

Conducting graphene oxide/polydiphenylamine (GO/PDPA) microsheet nanocomposite particles were fabricated via in-situ oxidative polymerization using diphenylamine in the presence of GO. The morphological structures and dimensions of the fabricated GO/PDPA composites were evaluated using transmission electron microscopy and scanning electron microscopy. Electrorheological (ER) responses and creep behaviors of an ER fluid consisting of the GO/PDPA composites when suspended in silicone oil were evaluated using a rotational rheometer under input electric field. Three different types of yield stresses were examined along with dielectric analysis, demonstrating their actively tunable ER behaviors.


1983 ◽  
Vol 61 (5) ◽  
pp. 1062-1070 ◽  
Author(s):  
Barbara M. MacKinnon ◽  
Michael D. B. Burt

The mature cysticercoid of Ophryocotyle insignis, from Patella vulgata, was examined using transmission electron microscopy. Eight different types of microtriches were present over the tegument of the larval body and microvilli covered the caudal bladder, or cercomer. Rounded, modified microtriches were present on the external surface of the bladder enclosing the cysticercoid. Microtriches lining the retraction chamber ranged from small triangular projections having an electron-dense ridge along the anterior margin but having no shaft, to more typically shaped, larger microtriches having a cytoplasmic base, electron-dense shaft, and an electron-dense ridge along the anterior margin of the base. The scolex tegument had large robust microtriches which, in transverse section, had many projecting flanges. The microtriches on the rostellum were long and slender. Long, thin microtriches were present amongst the small spines on the suckers and short microtriches were found on the unspined areas of the suckers. Possible functions for the different types of microtriches are suggested and the significance of microvilli on the cercomer is discussed.


2005 ◽  
Vol 495-497 ◽  
pp. 1067-1072
Author(s):  
Henryk Paul ◽  
Adam Morawiec ◽  
Emmanuel Bouzy ◽  
Jean-Jacques Fundenberger ◽  
Andrzej Piątkowski

The local crystallography within shear bands (SB) has been examined in a single crystal of {112}<111> orientation of pure copper deformed at 77K by channel-die compression to strains of about 1. Setting up a system for making high-resolution orientation maps using transmission electron microscopy (TEM) has opened new advantageous circumstances for the analysis of orientation changes within SB. This method with spatial resolution higher than 10nm allows the examination of microstructure images composed of nanoscale subcells forming SB. It has been found that for well-developed shear bands, a crystal lattice rotation about <112> direction tends to dominate and this process is usually accompanied by activation of new slip systems. The present work shows that despite the plane strain deformation mode, the mechanism of lattice rotation within emerging SBs may lead to Goss and Brass texture components.


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