scholarly journals Parameters Influencing Steady-State Grain Size of Pure Metals Processed by High-Pressure Torsion

2012 ◽  
Vol 706-709 ◽  
pp. 3034-3039 ◽  
Author(s):  
Kaveh Edalati ◽  
Z. Horita
Keyword(s):  
Grain Size ◽  
High Pressure ◽  
Steady State ◽  
High Pressure Torsion ◽  
Electron Back Scatter Diffraction ◽  
Logarithmic Scale ◽  
Transmission Electron ◽  
Nickel Copper ◽  
Iron Nickel ◽  
Copper Zinc

High purity elements such as magnesium, aluminum, silicon, titanium, vanadium, iron, nickel, copper, zinc, zirconium, molybdenum, palladium, silver, indium, tin, hafnium, gold and lead were processed by high-pressure torsion and subsequently evaluated by microstructural examinations and Vickers microhardness measurement. The grain size at the steady state, where the grain size and hardness remain unchanged with straining, was determined using either transmission electron microscopy, electron back-scatter diffraction analysis and/or optical microscopy. It is found that the steady state grain sizes are at the submicrometer level in elements with metallic bonding and at the nanometer level in elements with covalent bonding. The correlations between the steady-state grain size and the physical properties of metals are examined and it is found that the atomic bond energy and the homologous temperature are important parameters influencing the steady-state grain size after processing by HPT. A linear correlation between the hardness and grain size at the steady state is achieved by plotting the hardness normalized by the shear modulus against the grain size normalized by the Burgers vector in the logarithmic scale.

scholarly journals DIFFUSIVE AND DISPLACIVE PHASE TRANSFORMATIONS UNDER HIGH PRESSURE TORSION

2019 ◽  
Vol 25 (4) ◽  
pp. 230 ◽  
Author(s):  
Boris Straumal ◽  
Askar Kilmametov ◽  
Andrey Mazilkin ◽  
Olga Kogtenkova ◽  
Brigitte Baretzky ◽  
...  
Keyword(s):  
Mass Transfer ◽  
Plastic Deformation ◽  
Grain Size ◽  
High Pressure ◽  
Phase Composition ◽  
Steady State ◽  
Phase Transformations ◽  
High Pressure Torsion ◽  
Dynamic Equilibrium ◽  
Initial State

<p class="AMSmaintext"><span lang="EN-GB">Severe plastic deformation (SPD) can induce various phase transformations. After a certain strain, the dynamic equilibrium establishes between defects production by an external force and their relaxation (annihilation). The grain size, hardness, phase composition etc. in this steady-state does not depend on the initial state of a material and is, therefore, equifinal. In this review we discuss the competition between precipitation and dissolution of precipitates, amorphization and (nano)crystallization, SPD-induced accelerated mass-transfer, allotropic and martensitic transitions and formation of grain boundary phases.</span></p>

An Investigation of Hardness Homogeneity and Microstructure in Pure Titanium Processed by High Pressure Torsion

2014 ◽  
Vol 783-786 ◽  
pp. 2701-2706 ◽  
Author(s):  
Chuan Ting Wang ◽  
Alan G. Fox ◽  
Terence G. Langdon
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Grain Size ◽  
High Pressure ◽  
Dislocation Density ◽  
Vickers Microhardness ◽  
High Pressure Torsion ◽  
Pure Titanium ◽  
Commercial Purity ◽  
Transmission Electron

High-pressure torsion (HPT) was conducted on disks of commercial purity Ti under applied pressures of 3 and 6 GPa. Measurements of the Vickers microhardness showed improving hardness homogeneity with increasing numbers of HPT turns. Transmission electron microscopy demonstrated that a higher HPT pressure leads to a smaller grain size after straining and these grains contain a high dislocation density with arrays of twins. This is consistent with the higher hardness of the Ti samples processed by HPT under 6 GPa pressure.

The Processing of Ultrafine-Grained Materials Using High-Pressure Torsion

2007 ◽  
Vol 558-559 ◽  
pp. 1283-1294 ◽  
Author(s):  
Cheng Xu ◽  
Z. Horita ◽  
Terence G. Langdon
Keyword(s):  
Plastic Deformation ◽  
Grain Size ◽  
High Pressure ◽  
High Pressure Torsion ◽  
Metallic Materials ◽  
Grain Sizes ◽  
Ultrafine Grained ◽  
Wide Range ◽  
Ultrafine Grained Materials ◽  
Thin Disks

It is now well-established that processing through the application of severe plastic deformation (SPD) leads to a significant reduction in the grain size of a wide range of metallic materials. This paper examines the fabrication of ultrafine-grained materials using high-pressure torsion (HPT) where this process is attractive because it leads to exceptional grain refinement with grain sizes that often lie in the nanometer or submicrometer ranges. Two aspects of HPT are examined. First, processing by HPT is usually confined to samples in the form of very thin disks but recent experiments demonstrate the potential for extending HPT also to bulk samples. Second, since the strains imposed in HPT vary with the distance from the center of the disk, it is important to examine the development of inhomogeneities in disk samples processed by HPT.

Thermal Stability of Ultrafine-Grained Pure Titanium Processed by High-Pressure Torsion

2021 ◽  
Vol 1016 ◽  
pp. 338-344
Author(s):  
Wan Ji Chen ◽  
Jie Xu ◽  
De Tong Liu ◽  
De Bin Shan ◽  
Bin Guo ◽  
...  
Keyword(s):  
Activation Energy ◽  
Thermal Stability ◽  
Grain Size ◽  
High Pressure ◽  
Annealing Temperature ◽  
High Pressure Torsion ◽  
Stored Energy ◽  
Ultrafine Grained ◽  
Average Grain Size ◽  
Thermal Stability Of

High-pressure torsion (HPT) was conducted under 6.0 GPa on commercial purity titanium up to 10 turns. An ultrafine-grained (UFG) pure Ti with an average grain size of ~96 nm was obtained. The thermal properties of these samples were studied by using differential scanning calorimeter (DSC) which allowed the quantitative determination of the evolution of stored energy, the recrystallization temperatures, the activation energy involved in the recrystallization of the material and the evolution of the recrystallized fraction with temperature. The results show that the stored energy increases, beyond which the stored energy seems to level off to a saturated value with increase of HPT up to 5 turns. An average activation energy of about 101 kJ/mol for the recrystallization of 5 turns samples was determined. Also, the thermal stability of the grains of the 5 turns samples with subsequent heat treatments were investigated by microstructural analysis and Vickers microhardness measurements. It is shown that the average grain size remains below 246 nm when the annealing temperature is below 500 °C, and the size of the grains increases significantly for samples at the annealing temperature of 600 °C.

scholarly journals Exceptional Strengthening of Biodegradable Mg-Zn-Ca Alloys through High Pressure Torsion and Subsequent Heat Treatment

Materials ◽  
2019 ◽  
Vol 12 (15) ◽  
pp. 2460 ◽  
Author(s):  
Jelena Horky ◽  
Abdul Ghaffar ◽  
Katharina Werbach ◽  
Bernhard Mingler ◽  
Stefan Pogatscher ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Grain Size ◽  
High Pressure ◽  
Tensile Strength ◽  
High Pressure Torsion ◽  
Type Equation ◽  
Subsequent Heat Treatment ◽  
Strength Increase ◽  
Dislocation Loops ◽  
High Concentration

In this study, two biodegradable Mg-Zn-Ca alloys with alloy content of less than 1 wt % were strengthened via high pressure torsion (HPT). A subsequent heat treatment at temperatures of around 0.45 Tm led to an additional, sometimes even larger increase in both hardness and tensile strength. A hardness of more than 110 HV and tensile strength of more than 300 MPa were achieved in Mg-0.2Zn-0.5Ca by this procedure. Microstructural analyses were conducted by scanning and transmission electron microscopy (SEM and TEM, respectively) and atom probe tomography (APT) to reveal the origin of this strength increase. They indicated a grain size in the sub-micron range, Ca-rich precipitates, and segregation of the alloying elements at the grain boundaries after HPT-processing. While the grain size and segregation remained mostly unchanged during the heat treatment, the size and density of the precipitates increased slightly. However, estimates with an Orowan-type equation showed that precipitation hardening cannot account for the strength increase observed. Instead, the high concentration of vacancies after HPT-processing is thought to lead to the formation of vacancy agglomerates and dislocation loops in the basal plane, where they represent particularly strong obstacles to dislocation movement, thus, accounting for the considerable strength increase observed. This idea is substantiated by theoretical considerations and quenching experiments, which also show an increase in hardness when the same heat treatment is applied.

scholarly journals Grain size and microhardness evolution during annealing of a magnesium alloy processed by high-pressure torsion

2015 ◽  
Vol 4 (1) ◽  
pp. 14-17 ◽  
Author(s):  
Livia Raquel C. Malheiros ◽  
Roberto Braga Figueiredo ◽  
Terence G. Langdon
Keyword(s):  
Grain Size ◽  
High Pressure ◽  
Magnesium Alloy ◽  
High Pressure Torsion

Microstructure Development and Precipitation Effects in Ultra Fine Grained Mg-3Tb-2Nd Alloy Prepared by High Pressure Torsion

2008 ◽  
Vol 584-586 ◽  
pp. 591-596 ◽  
Author(s):  
Jakub Čížek ◽  
Ivan Procházka ◽  
Bohumil Smola ◽  
Ivana Stulíková ◽  
Martin Vlach ◽  
...  
Keyword(s):  
High Pressure ◽  
Positron Lifetime ◽  
High Pressure Torsion ◽  
Creep Properties ◽  
Fine Grained ◽  
Transmission Electron ◽  
Highly Sensitive ◽  
Ideal Tool ◽  
Increasing Temperature

Mg-Tb-Nd ternary alloy represents a novel hardenable Mg-based alloy with enhanced strength and favorable creep properties. In the present work we studied microstructure of ultra fine grained (UFG) Mg-Tb-Nd alloy prepared by high pressure torsion (HPT). Lattice defects introduced into the specimen by the severe plastic deformation play a key role in physical properties of UFG specimens. It is known that positron lifetime (PL) spectroscopy is highly sensitive to open volume defects (like vacancies, dislocations, etc.). Therefore, PL spectroscopy is an ideal tool for defect characterizations in the HPT deformed specimens. In the present work we combined PL studies with transmission electron microscopy and microhardness measurements. After detailed characterization of the as-deformed structure, the specimens were step-by-step isochronally annealed and we investigated the development of microstructure with increasing temperature.

Fabrication of Ultrafine Grained Copper Alloy by 3-Layers Accumulative Roll-Bonding Process

2010 ◽  
Vol 443 ◽  
pp. 158-163
Author(s):  
Cha Yong Lim ◽  
Hyoung Wook Kim ◽  
Seong Hee Lee
Keyword(s):  
Grain Size ◽  
Accumulative Roll Bonding ◽  
Copper Alloy ◽  
Electron Back Scatter Diffraction ◽  
Bonding Process ◽  
Accumulative Roll Bonding Process ◽  
Roll Bonding ◽  
Ultrafine Grains ◽  
Transmission Electron ◽  
Average Grain Size

The 3-layers accumulative roll bonding process (ARB) has been attempted to increase the strength of copper alloy (Cu-0.02wt.%P) by refining grain size. The 3-layers accumulative roll bonding was conducted up to 7 cycles at room temperature without lubrication. Microstructural evolution of the copper alloy with the number of the 3-layers ARB cycles was investigated by optical microscopy (OM), transmission electron microscopy (TEM), and electron back scatter diffraction (EBSD). The average grain size has been refined from 20 μm before ARB to 170 nm after 7 cycles of 3-layers ARB. More than 70% of ultrafine grains formed by 3-layers ARB were composed of high angle grain boundaries. The average misorientation angle of ultrafine grains was 30.7 degrees in the center of the specimen. Tensile strength after 7 cycles of 3-layers ARB was 605 MPa, which is about 3.2 times higher than the initial value.

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