Effect of As-Rolled Microstructure on Static Recrystallization Characteristics and Texture Evolution during Annealing

2016 ◽  
Vol 879 ◽  
pp. 1876-1881
Author(s):  
Jing Su ◽  
Abu S.H. Kabir ◽  
Steve Yue
Keyword(s):  
Optical Microscopy ◽  
Static Recrystallization ◽  
Texture Evolution ◽  
Az31 Alloy ◽  
Rolling Speed ◽  
X Ray Diffraction ◽  
Electron Backscattered Diffraction ◽  
X Ray ◽  
Magnesium Az31

Magnesium AZ31 alloy sheets were rolled at 100 °C at a high rolling speed of 1000 m/min. After 30% reduction, the microstructure was heavily twinned and shear banded, while a partially dynamically recrystallized and twinned microstructure was seen at the reduction of 49%. The as-rolled specimens were then annealed at 500 °C for increasing times. Microstructure and texture were characterized by optical microscopy, electron backscattered diffraction (EBSD) and X-ray diffraction (XRD). Texture weakening was found during annealing of the specimens at both reductions. However, the texture weakening was more effective in the fully twinned and shear banded specimen than the partially DRXed and twinned specimen. Effects of as-rolled microstructure on static recrystallization characteristics and texture evolution during annealing were studied.

Effect of electroplastic treatment on microstructure and texture changes of a cold rolling AZ31 strip

2009 ◽  
Vol 1170 ◽  
Author(s):  
Lei Guan ◽  
Guoyi Tang
Keyword(s):  
Cold Rolling ◽  
Light Microscopy ◽  
Static Recrystallization ◽  
Texture Evolution ◽  
Dislocation Climb ◽  
Basal Texture ◽  
X Ray Diffraction ◽  
X Ray ◽  
Electropulsing Treatment

AbstractThe effect of the electropulsing on recrystallized microstructure and on texture evolution of a cold rolling (CR) AZ31 strip was studied with the help of light microscopy and X-ray diffraction technique. It was exciting that the completed recrystallization state of sample subjected to the electropulsing treatment (EPT) could be obtained rapidly in ˜7s with the basal texture weakened. The favoring mechanism of static recrystallization (SRX) of MPT could be attributed to the coupled action of the thermal and athermal effects, thereinto, the latter one activated dislocation climb effectively.

Static Recrystallization Characteristic of Low Temperature Rolled AZ31 Magnesium Alloy during Annealing

2015 ◽  
Vol 828-829 ◽  
pp. 239-243
Author(s):  
Jing Su ◽  
Mehdi Sanjari ◽  
Abu Syed Kabir ◽  
In Ho Jung ◽  
Steve Yue
Keyword(s):  
Static Recrystallization ◽  
Shear Bands ◽  
Az31 Alloy ◽  
Rolling Speed ◽  
Stored Energy ◽  
Second Stage ◽  
Recrystallization Kinetics ◽  
Softening Behavior ◽  
Magnesium Az31 ◽  
Kinetics Of

Microstructure evolution and static recrystallization kinetics of a magnesium AZ31 alloy during annealing have been investigated. The Mg alloy sheets were rolled at 100°C at a low rolling speed of 15m/min and a high rolling speed of 1000m/min to reductions of 8%, 23% and 30%. Annealing was then conducted on the as-rolled specimens at 200°C for different times. The microstructure was characterized by optical microscopy and recrystallization kinetics were evaluated by means of Johnson-Mehl-Avrami-Kolmogorov (JMAK) model. The softening behavior was found to be divided into two annealing stages. The first stage was related to the recrystallization on high stored energy regions, such as shear bands and twins, while the second stage was associated to the recrystallization of low stored energy areas.

Texture Evolution Under Fast Heating and Cooling Rates of Zirconium Alloys Studied In-Situ by Synchrotron X-Ray Diffraction

2020 ◽  
Author(s):  
Chi-Toan Nguyen ◽  
Alistair Garner ◽  
Javier Romero ◽  
Antoine Ambard ◽  
Michael Preuss ◽  
...  
Keyword(s):  
Texture Evolution ◽  
Zirconium Alloys ◽  
X Ray Diffraction ◽  
Fast Heating ◽  
Cooling Rates ◽  
X Ray ◽  
Heating And Cooling

Synthesis and Properties of Thermotropic Liquid Crystalline Polyesters with Flexible Polymethylene Spacer

2010 ◽  
Vol 428-429 ◽  
pp. 126-131
Author(s):  
Wei Zhong Lu ◽  
Chun Wei ◽  
Qui Shan Gao
Keyword(s):  
Optical Microscopy ◽  
Liquid Crystalline ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Structure Morphology ◽  
Temperature Ranges ◽  
Ft Ir ◽  
Diffraction Peaks ◽  
Ubbelohde Viscometer

Polymethylene bis(p-hydroxybenzoates) were prepared from methyl p-hydroxybenzoate and different diols by melted transesterification reaction. Three liquid crystalline polyesters were synthesized from terephthaloyl dichloride and polymethylene bis(p-hydroxybenzoates). Its structure, morphology and properties were characterized by Ubbelohde viscometer, Fourier transform infrared spectroscopy (FT-IR), Differential scanning calorimetry (DSC), polarized optical microscopy (POM) with a hot stage, and wide-angle X-ray diffraction (WAXD). Results indicated that the intrinsic viscosities were between 0.088 and 0.210 dL/g. Optical microscopy showed that the TLCP has a highly threaded liquid crystalline texture and a high birefringent schlieren texture character of nematic phase and has wider mesophase temperature ranges for all polyesters. DSC analysis were found that the melting point (Tm), isotropic temperature (Ti) of TLCPs decreased and the temperature range of the liquid crystalline phase became wider with increased number of methylene spacers in the polyester. The WAXD results showed that TLCPs owned two strong diffraction peaks at 2θ near 19° and 23°.

Dependence of hydrogen embrittlement on annealing time in medium-Mn steels

2021 ◽  
Vol ahead-of-print (ahead-of-print) ◽  
Author(s):  
Juanping Xu ◽  
Jinxu Li ◽  
Zheng Wang ◽  
Hao Fu ◽  
Ming Wu
Keyword(s):  
Hydrogen Embrittlement ◽  
Annealing Time ◽  
Martensite Transformation ◽  
Design Methodology ◽  
Warm Rolling ◽  
X Ray Diffraction ◽  
Electron Backscattered Diffraction ◽  
Content Type ◽  
X Ray ◽  
Two Samples

Purpose The purpose of this paper is to investigate the effect of the soft annealing time on the microstructure and hydrogen embrittlement (HE) of Fe-0.22C-11.54Mn-2.05Al steels. Design/methodology/approach Steels A and B with different morphologies were prepared by cold rolling after warm rolling, long/short softening annealing and finally annealing at 700 °C for 30 min. Uncharged and charged samples were subjected to tensile, and HE behavior was studied by electron backscattered diffraction, scanning electron microscopy and X-ray diffraction. Findings The two samples exhibited similar tensile strengths. The homogeneous equiaxed microstructure of steel B was found to be more conducive to relieve its HE sensitivity. Steel A exhibited bimodal-grained microstructures – blocky and lath. The formation of crack in the blocky grains of steel A resulted in a significant reduction in its plasticity and tensile strength. Originality/value The high HE susceptibility of steel A is mainly connected with the inhomogeneity of martensite transformation.

scholarly journals Mössbauer study of Fe phases in terrestrial olivine basalts from southern Egypt

Mineralogia ◽  
2013 ◽  
Vol 44 (1-2) ◽  
pp. 3-12 ◽  
Author(s):  
Kamaleldin M. Hassan ◽  
Julius Dekan
Keyword(s):  
Optical Microscopy ◽  
Crystal Chemistry ◽  
Mössbauer Spectra ◽  
Mossbauer Spectroscopy ◽  
X Ray Diffraction ◽  
Mössbauer Study ◽  
Hyperfine Parameters ◽  
X Ray ◽  
Mossbauer Spectra ◽  
Oxidized Iron

AbstractOlivine basalts from southern Egypt were studied by 57Fe Mössbauer spectroscopy at 297 and 77 K, and by optical microscopy and X-ray diffraction. The 57Fe Mössbauer spectra show three-magnetic sextets, three doublets of ferrous (Fe2+), and a weak ferric (Fe3+) doublet that is attributable to a nanophase oxide (npOx). The magnetic sextets relate to titanomagnetite and the Fe2+ doublets to olivine, pyroxene, and ulvöspinel. Variations in the hyperfine parameters of the various Fe components are attributed to changes in the local crystal chemistry. The intensity of oxidation (Fe3+/ΣFe) in the rocks varies from 20-27% with the oxidized iron largely residing in the titanomagnetite.

scholarly journals Titania powder activation and rutile ceramics structure formation

2009 ◽  
Vol 41 (1) ◽  
pp. 27-33 ◽  
Author(s):  
I.R. Ziganshin ◽  
S.E. Porozova ◽  
A.E. Stolina ◽  
M.F. Torsunov
Keyword(s):  
Raman Spectroscopy ◽  
Porous Materials ◽  
Optical Microscopy ◽  
Aqueous Medium ◽  
Structure Formation ◽  
Mechanochemical Activation ◽  
Organic Additives ◽  
X Ray Diffraction ◽  
X Ray ◽  
Titania Powder

Impact of mechanochemical activation (MCA) in aqueous medium with various organic additives on commercial titania powder and products made of it has been investigated by X-ray diffraction, optical microscopy and Raman spectroscopy. Agar-agar additive has been shown to offer promise for activation of titania powders used in obtaining both dense and porous materials.

scholarly journals Effect of Supra-Transus Deformation Conditions on Recrystallization of Beta Ti Alloy

Metals ◽  
2021 ◽  
Vol 11 (8) ◽  
pp. 1278
Author(s):  
Chao Voon Samuel Lim ◽  
Yang Liu ◽  
Chen Ding ◽  
Aijun Huang
Keyword(s):  
Hot Deformation ◽  
Static Recrystallization ◽  
Dynamic Recovery ◽  
Texture Evolution ◽  
High Strength ◽  
Ex Situ ◽  
Mechanical Processing ◽  
Ti Alloy ◽  
Electron Backscattered Diffraction ◽  
Beta Ti Alloy

There is increasing usage of high strength Beta Ti alloy in aerospace components. However, one of the major challenges is to obtain homogeneous refined microstructures via the thermo-mechanical processing. To overcome this issue, an understanding of the hot deformation conditions effect on the microstructure, prior to and after annealing, is needed. In this work, the effect of strain levels, which is more precise than percentage of reduction, and strain rate under supra-transus deformation temperature on beta annealing are studied using a double cone sample. The Electron Backscattered Diffraction (EBSD) is used to determine the deformed microstructure and texture evolution, as well as the static recrystallized grains evolution using the ex situ annealing approach. This work provides evidence that the mechanisms of dynamic recovery and recrystallization, along with texture evolution, are affected by the deformation conditions, which in turn affected the subsequent static recrystallization during annealing. It will also be shown that high levels of strain do not necessarily lead to an increase in the rate of recrystallization. Finally, the results obtained provided several examples of guidance in designing the TMP processes for obtaining not only a refine microstructure, but a more homogeneous beta microstructure during the beta processing of Beta Ti alloy.

Structural study of cokes using optical microscopy and X-ray diffraction

Fuel ◽  
1983 ◽  
Vol 62 (3) ◽  
pp. 274-278 ◽  
Author(s):  
Asao Ōya ◽  
Zhanfen Qian ◽  
Harry Marsh
Keyword(s):  
Optical Microscopy ◽  
Structural Study ◽  
X Ray Diffraction ◽  
X Ray

Microstructural Evaluation of Clayey Ceramic Incorporated with Sludge from Paper Manufacturing

2016 ◽  
Vol 881 ◽  
pp. 422-426
Author(s):  
Carlos Maurício Fontes Vieira ◽  
Regina Maria Pinheiro ◽  
Sergio Neves Monteiro
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Optical Microscopy ◽  
X Ray Diffraction ◽  
X Ray ◽  
Paper Making ◽  
Paper Manufacturing ◽  
Microstructural Evaluation ◽  
Calcium Compounds ◽  
Scanning Electron

This work has for objective to evaluate the microstructure of clayey ceramic incorporated with a waste in the form of sludge generated during treatment of effluent of a paper making industry. The microstructure of ceramics incorporated with 0 and 10 wt.% of waste, and then fired at 600°C, was evaluated by optical microscopy, scanning electron microscopy and X-ray diffraction. The results showed that the waste changes the microstructure of the clayey ceramic increasing the porosity, as well as forming new crystalline phases, mainly with calcium compounds.

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