Estimating Volume Fractions of Microstructural Constituents in Austempered High Silicon Alloyed GJS 600-10 Ductile Iron through Magnetic Measurements (VSM)

2017 ◽  
Vol 907 ◽  
pp. 50-55
Author(s):  
Yakup Yürektürk ◽  
Murat Baydogan
Keyword(s):  
Heat Treatment ◽  
Ductile Iron ◽  
Retained Austenite ◽  
Volume Fraction ◽  
Magnetic Measurements ◽  
Ferritic Matrix ◽  
Volume Fractions ◽  
High Silicon ◽  
New Generation

In this paper, austempering heat treatment was applied to a new generation high silicon GJS 600-10 grade ductile iron with an initial ferritic matrix. Different austempering temperatures of 270, 330 and 390°C were applied after austenitizing at 975°C for 120 min. Depending on the austempering temperatures, lower and upper ausferritic microstructures were obtained. Results showed that volume fraction of the retained austenite in the ausferritic microstructures, which was estimated by VSM technique is well correlated with those estimated by XRD technique.

scholarly journals Effect of Different Austempering Heat Treatments on Corrosion Properties of High Silicon Steel

Materials ◽  
2021 ◽  
Vol 14 (2) ◽  
pp. 288
Author(s):  
Mattia Franceschi ◽  
Luca Pezzato ◽  
Alessio Giorgio Settimi ◽  
Claudio Gennari ◽  
Mirko Pigato ◽  
...  
Keyword(s):  
Retained Austenite ◽  
Volume Fraction ◽  
Electrochemical Impedance ◽  
Borate Buffer Solution ◽  
X Ray Diffraction ◽  
Buffer Solution ◽  
Corrosion Properties ◽  
Volume Fractions ◽  
Final Microstructure ◽  
High Silicon

A novel high silicon austempered (AHS) steel has been studied in this work. The effect of different austenitizing temperatures, in full austenitic and biphasic regime, on the final microstructure was investigated. Specimens were austenitized at 780 °C, 830 °C, 850 °C and 900 °C for 30 min and held isothermally at 350 °C for 30 min. A second heat treatment route was performed which consisted of austenitizing at 900 °C for 30 min and austempering at 300 °C, 350 °C and 400 °C for 30 min. Scanning electron microscopy (SEM) and X-ray diffraction (XRD) have been used to evaluate the microstructural evolution. These techniques revealed that the microstructures were composed of carbide-free bainite, ferrite, martensite and retained austenite (RA) in different volume fractions (Vγ). An aqueous borate buffer solution with 0.3 M H3BO3 and 0.075 M Na2B4O7∂10H2O (pH = 8.4) was used for corrosion tests in order to evaluate the influence of the different volume fractions of retained austenite on the corrosion properties of the specimens. The results showed that when increasing the austenitization temperatures, the volume fractions of retained austenite reached a maximum value at 850 °C, and decrease at higher temperatures. The corrosion properties were investigated after 30 min and 24 h immersion by means of potentiodynamic polarization (after 30 min) and electrochemical impedance spectroscopy (after both 30 min and 24 h) tests. The corrosion resistance of the samples increased with increases in the volume fraction of retained austenite due to lower amounts of residual stresses.

scholarly journals Heat Treatment Evaluation for the Camshafts Production of ADI Low Alloyed with Vanadium

Metals ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 1036
Author(s):  
Eduardo Colin García ◽  
Alejandro Cruz Ramírez ◽  
Guillermo Reyes Castellanos ◽  
José Federico Chávez Alcalá ◽  
Jaime Téllez Ramírez ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Tensile Strength ◽  
Ductile Iron ◽  
Volume Fraction ◽  
Energy Impact ◽  
Treatment Conditions ◽  
Mold Casting ◽  
Grade 3 ◽  
Good Agreement

Ductile iron camshafts low alloyed with 0.2 and 0.3 wt % vanadium were produced by one of the largest manufacturers of the ductile iron camshafts in México “ARBOMEX S.A de C.V” by a phenolic urethane no-bake sand mold casting method. During functioning, camshafts are subject to bending and torsional stresses, and the lobe surfaces are highly loaded. Thus, high toughness and wear resistance are essential for this component. In this work, two austempering ductile iron heat treatments were evaluated to increase the mechanical properties of tensile strength, hardness, and toughness of the ductile iron camshaft low alloyed with vanadium. The austempering process was held at 265 and 305 °C and austempering times of 30, 60, 90, and 120 min. The volume fraction of high-carbon austenite was determined for the heat treatment conditions by XRD measurements. The ausferritic matrix was determined in 90 min for both austempering temperatures, having a good agreement with the microstructural and hardness evolution as the austempering time increased. The mechanical properties of tensile strength, hardness, and toughness were evaluated from samples obtained from the camshaft and the standard Keel block. The highest mechanical properties were obtained for the austempering heat treatment of 265 °C for 90 min for the ADI containing 0.3 wt % V. The tensile and yield strength were 1200 and 1051 MPa, respectively, while the hardness and the energy impact values were of 47 HRC and 26 J; these values are in the range expected for an ADI grade 3.

scholarly journals Austenitization of FerriticDuctile Iron

2014 ◽  
Vol 14 (4) ◽  
pp. 49-54 ◽  
Author(s):  
A. Krzyńska ◽  
A. Kochański
Keyword(s):  
Heat Treatment ◽  
Ductile Iron ◽  
Starting Material ◽  
Austempered Ductile Iron ◽  
Isothermal Quenching ◽  
Micro Hardness ◽  
Hardness Testing ◽  
Ferritic Matrix ◽  
Rate Of Dissolution ◽  
Nodular Graphite

Abstract Austenitization is the first step of heat treatment preceding the isothermal quenching of ductile iron in austempered ductile iron (ADI) manufacturing. Usually, the starting material for the ADI production is ductile iron with more convenient pearlitic matrix. In this paper we present the results of research concerning the austenitizing of ductile iron with ferritic matrix, where all carbon dissolved in austenite must come from graphite nodules. The scope of research includedcarrying out the process of austenitization at 900° Cusing a variable times ranging from 5 to 240minutes,and then observations of the microstructure of the samples after different austenitizing times. These were supplemented with micro-hardness testing. The research showed that the process of saturating austenite with carbon is limited by the rate of dissolution of carbon from nodular graphite precipitates

Microstructure and Tensile Properties of TRIP-Aided Steel Sheet Subjected to Hot-Rolling and Austempering

2021 ◽  
Vol 1016 ◽  
pp. 732-737
Author(s):  
Junya Kobayashi ◽  
Hiroto Sawayama ◽  
Naoya Kakefuda ◽  
Goroh Itoh ◽  
Shigeru Kuraoto ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Hot Rolling ◽  
Manufacturing Process ◽  
Retained Austenite ◽  
Volume Fraction ◽  
Isothermal Holding ◽  
High Strength ◽  
Isothermal Transformation ◽  
Transformation Process ◽  
Steel Sheets

Various high strength steel sheets for weight reduction and safety improvement of vehicles have been developed. TRIP-aided steel with transformation induced plasticity of the retained austenite has high strength and ductility. Conventional TRIP-aided steels are subjected to austempering process after austenitizing. Generally, elongation and formability of TRIP-aided steel are improved by finely dispersed retained austenite in BCC phase matrix. The finely dispersed retained austenite and grain refinement of TRIP-aided steel can be achieved by hot rolling with heat treatment. Therefore, the improvement of mechanical properties of TRIP-aided steel is expected from the manufacturing process with hot rolling and then isothermal transformation process. In this study, thermomechanical heat treatment is performed by combining hot rolling and isothermal holding as the manufacturing process of TRIP-aided steel sheets. The complex phase matrix is obtained by hot rolling and then isothermal holding. Although the hardness of the hot rolled and isothermal held TRIP-aided steel is decreased, the volume fraction of retained austenite is increased.

scholarly journals Phase Transition Kinetics in Austempered Ductile Iron (ADI) with Regard to Mo Content

Materials ◽  
2020 ◽  
Vol 13 (22) ◽  
pp. 5266
Author(s):  
Martin Landesberger ◽  
Robert Koos ◽  
Michael Hofmann ◽  
Xiaohu Li ◽  
Torben Boll ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Phase Transformation ◽  
Neutron Diffraction ◽  
Ductile Iron ◽  
Retained Austenite ◽  
Length Change ◽  
Atom Probe ◽  
Carbon Accumulation ◽  
Austempered Ductile Iron ◽  
Mo Content

The phase transformation to ausferrite during austempered ductile iron (ADI) heat treatment can be significantly influenced by the alloying element Mo. Utilizing neutron diffraction, the phase transformation from austenite to ausferrite was monitored in-situ during the heat treatment. In addition to the phase volume fractions, the carbon enrichment of retained austenite was investigated. The results from neutron diffraction were compared to the macroscopic length change from dilatometer measurements. They show that the dilatometer data are only of limited use for the investigation of ausferrite formation. However, they allow deriving the time of maximum carbon accumulation in the retained austenite. In addition, the transformation of austenite during ausferritization was investigated using metallographic methods. Finally, the distribution of the alloying elements in the vicinity of the austenite/ferrite interface zone was shown by atom probe tomography (APT) measurements. C and Mn were enriched within the interface, while Si concentration was reduced. The Mo concentration in ferrite, interface and austentite stayed at the same level. The delay of austenite decay during Stage II reaction caused by Mo was studied in detail at 400 °C for the initial material as well as for 0.25 mass % and 0.50 mass % Mo additions.

Effects of Heat Treatment on Microstructure of High-Strength Manganese-Silicon Steels

2017 ◽  
Vol 270 ◽  
pp. 239-245
Author(s):  
Dagmar Bublíková ◽  
Štěpán Jeníček ◽  
Kateřina Opatová ◽  
Bohuslav Mašek
Keyword(s):  
Heat Treatment ◽  
Cooling Rate ◽  
Microstructure Evolution ◽  
Retained Austenite ◽  
Volume Fraction ◽  
High Strength ◽  
Quenching And Partitioning ◽  
Alloying Additions ◽  
New Procedures ◽  
Strength And Ductility

Today’s advanced steels are required to possess high strength and ductility. This can be accomplished by producing appropriate microstructures with a certain volume fraction of retained austenite. The resulting microstructure depends on material’s heat treatment and alloying. High ultimate strengths and sufficient elongation levels can be obtained by various methods, including quenching and partitioning (Q&P process). The present paper introduces new procedures aimed at simplifying this process with the use of material-technological modelling. Three experimental steels have been made and cast for this investigation, whose main alloying additions were manganese, silicon, chromium, molybdenum and nickel. The purpose of manganese addition was to depress the Ms and Mf temperatures. The Q&P process was carried out in a thermomechanical simulator for better and easier control. The heat treatment parameters were varied between the sequences and their effect on microstructure evolution was evaluated. They included the cooling rate, partitioning temperature and time at partitioning temperature. Microstructures including martensite with strength levels of more than 2000 MPa and elongation of 10–15 % were obtained.

Microstructure Evolution during Strain-Induced Transformation of Austenite in an Austempered Ductile Iron (ADI)

2021 ◽  
Vol 1016 ◽  
pp. 1199-1204
Author(s):  
R. Raghavendran ◽  
Anil Meena ◽  
Murugaiyan Amirthalingam
Keyword(s):  
Phase Transformation ◽  
Thermomechanical Treatment ◽  
Ductile Iron ◽  
Retained Austenite ◽  
Volume Fraction ◽  
Thermomechanical Processing ◽  
Base Material ◽  
High Volume ◽  
Austempered Ductile Iron ◽  
Conventional Heat Treatment

Microstructural evolution during the strain-induced phase transformation of austenite in an Austempered ductile iron (ADI) under various thermomechanical processing conditions is studied in the present study. An alloyed ductile iron is taken as the base material, and thermomechanical treatment is carried out on a Gleeble 3800 thermomechanical simulator coupled with dilatometry. The effect of deformation on the austempering process has been studied by microstructure characterization using optical microscopy (OM), scanning electron microscopy (SEM), and X-ray diffraction (XRD) techniques. The variations in retained austenite volume fraction and its carbon content with respect to different austempering times are analyzed to study the effect of strain-induced transformation of austenite. It has been observed that the thermomechanical treatment significantly influences the phase transformation kinetics during the austempering process. The thermomechanical treatment produced a martensite free ausferritic microstructure for all austempering times with a high volume fraction of carbon enriched retained austenite as compared to the conventional heat treatment.

The Application of Analysis of Variance to Phase Transformation of an Austempered Ductile Iron

2015 ◽  
Vol 1128 ◽  
pp. 338-343
Author(s):  
Flavius Aurelian Sarbu ◽  
Ioan Milosan
Keyword(s):  
Phase Transformation ◽  
Analysis Of Variance ◽  
Ductile Iron ◽  
Repeated Measures ◽  
Retained Austenite ◽  
Volume Fraction ◽  
Austempered Ductile Iron ◽  
The One

The paper presents an example of calculation for the one-way repeated measures applied for the results of an austempered ductile iron. This research has a number of objectives which can be started as follows: 1. to determine of the volume fraction of retained austenite (Vγr); 2. the calculation for the one-way repeated measures applied for the results of the volume fraction of retained austenite (Vγr).

scholarly journals High Versatility of Niobium Alloyed AHSS

2017 ◽  
Vol 62 (3) ◽  
pp. 1485-1491 ◽  
Author(s):  
L. Kučerová ◽  
K. Opatová ◽  
J. Káňa ◽  
H. Jirková
Keyword(s):  
Heat Treatment ◽  
Retained Austenite ◽  
Volume Fraction ◽  
High Strength ◽  
Processing Parameters ◽  
High Ductility ◽  
Processing Strategies ◽  
Cooling Schedules ◽  
Final Microstructure ◽  
Steel Processing

AbstractThe effect of processing parameters on the final microstructure and properties of advanced high strength CMnSiNb steel was investigated. Several processing strategies with various numbers of deformation steps and various cooling schedules were carried out, namely heat treatment without deformation, conventional quenching and TRIP steel processing with bainitic hold or continuous cooling. Obtained multiphase microstructures consisted of the mixture of ferrite, bainite, retained austenite and M-A constituent. They possessed ultimate tensile strength in the range of 780-970 MPa with high ductility A5mmabove 30%. Volume fraction of retained austenite was for all the samples around 13%. The only exception was reference quenched sample with the highest strength 1186 MPa, lowest ductility A5mm= 20% and only 4% of retained austenite.

The Microstructures and Hardness Analysis of a New Hypereutectoid Mn-Cr-Mo-V Steel

2013 ◽  
Vol 58 (2) ◽  
pp. 563-568
Author(s):  
R. Dabrowski ◽  
E. Rozniata ◽  
R. Dziurka
Keyword(s):  
Heat Treatment ◽  
Chemical Composition ◽  
Liquid Nitrogen ◽  
Retained Austenite ◽  
Volume Fraction ◽  
Chemical Compositions ◽  
Tool Steels ◽  
Maximum Hardness ◽  
Hypereutectoid Steel ◽  
Tempering Temperature

The results of a microstructure and hardness investigations of a new hypereutectoid Mn-Cr-Mo-V steel, imitating by its chemical composition tool steels, are presented in the paper. The microstructure as well hardness changes, caused by austenitising and tempering temperatures were assessed, for samples quenched and sub-quenched in liquid nitrogen, directly after the quenching treatment. Additionally, the influence of the tempering temperature on the volume fraction of the retained austenite was estimated. New hypereutectoid steel, after an appropriate heat treatment obtained the relevant hardness of the tools used in the cold and hot working proces. It was indicated that the steel hardness increases with the increases of the austenitising temperature. At 800ºC the hardness of the quenched samples were equal 895HV, and for the sub-quenched samples 937HV. The maximum hardness, after tempering (746HV), was found at a temperature of 520ºC. It will be possible, in future, to apply this obtained investigation results in designing chemical compositions and microstructures of the new hypereutectoid alloyed steels of properties required by their users.

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