Influence of the Pouring Temperature on the Castability and Microstructure of Elektron 21 and QE22 Magnesium Casting Alloys

2013 ◽  
Vol 197 ◽  
pp. 125-130
Author(s):  
Bartłomiej Dybowski ◽  
Robert Jarosz ◽  
Andrzej Kiełbus
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Magnesium Alloys ◽  
Automotive Industry ◽  
Volume Fraction ◽  
Low Density ◽  
Pouring Temperature ◽  
Casting Alloys ◽  
Magnesium Casting

Magnesium alloys are widely used in aerospace and automotive industry due to their low density, good mechanical properties and good castability. The paper presents results of the castability tests and microstructural investigations on two unmodified magnesium casting alloys, Elektron 21 and QE22. Spirals for the castability test were poured from three temperatures: 755°C, 800°C and 835°C. Volume fraction of eutectic regions and grain size in both alloys were quantitatively evaluated. Castability increased with increasing pouring temperature. Quantity of eutectics and grain size did not show straight correlation with pouring temperature.

Influence of Pouring Temperature on Castability and Microstructure of QE22 and RZ5 Magnesium Casting Alloys

2012 ◽  
Vol 191 ◽  
pp. 137-144 ◽  
Author(s):  
Bartlomiej Dybowski ◽  
Robert Jarosz ◽  
Andrzej Kiełbus ◽  
Jan Cwajna
Keyword(s):  
Mechanical Properties ◽  
Corrosion Resistance ◽  
Rare Earth ◽  
High Temperature ◽  
Magnesium Alloys ◽  
Volume Fraction ◽  
Low Density ◽  
Pouring Temperature ◽  
Casting Alloys ◽  
Magnesium Casting

Magnesium alloys are widely used in automotive and aerospace industries due to their great connection of low density and good mechanical properties. They are also characterized by good castability and weldability. Their weak high temperature properties and corrosion resistance, led to development of magnesium alloys containing rare earth elements. Casting is the most popular way of manufacturing magnesium elements. However, there is a lack of investigations concerning impact of different factors on fluidity of these alloys. This paper presents results of investigations on influence of pouring temperature on castability and microstructure of QE22 and RZ5 magnesium alloys. In case of QE22 alloy, the filling length of the liquid alloy increased with the increasing pouring temperature. In RZ5 no such dependence was noted. This is probably caused by oxide films in the structure of material. Grain refinement and eutectics volume fraction also didn’t present correlation with pouring temperature.

Research on the Microstructures and Mechanical Properties of Annealed Cold Upsetting AZ31 Magnesium Alloy

2009 ◽  
Vol 610-613 ◽  
pp. 826-830
Author(s):  
Tian Mo Liu ◽  
Wei Hui Hu ◽  
Qing Liu
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Magnesium Alloy ◽  
Magnesium Alloys ◽  
Annealing Temperature ◽  
Volume Fraction ◽  
Cold Upsetting ◽  
Cast Magnesium Alloys ◽  
Microstructures And Mechanical Properties ◽  
Cast Magnesium

The microstructures and mechanical properties of cold upsetting magnesium alloys were investigated upon anneal under different conditions. The results show that a large amount of twins were observed in the original grains of cold upsetting AZ31 magnesium alloys. The twins disappeared gradually and recrystal grains formed after anneal. The volume fraction of the recrystal grains increases as the strain of samples rises. Recrystal grain size grows large with the elevated annealing temperature. Recrystal grain size reduces at first and then grows as the annealing time is prolonged. In addition, compared with as-cast magnesium alloys, the yield strength of cold upsetting samples increase apparently due to grain refinement after anneals.

Microstructures and Mechanical Properties of Annealed Fe-8Mn-6Al-0.4C Duplex Low-Density Steels

2021 ◽  
Vol 1035 ◽  
pp. 337-343
Author(s):  
Rong Chen ◽  
Peng Chen ◽  
Xiao Wu Li
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Tensile Strength ◽  
Mechanical Stability ◽  
Volume Fraction ◽  
Electron Back Scatter Diffraction ◽  
Low Density ◽  
X Ray Diffraction ◽  
Austenite Grain Size ◽  
The Stability

The cold-rolled Fe-8Mn-6Al-0.4C duplex low-density steel was annealed at different conditions to obtain ferrite + austenite duplex microstructure. The excellent mechanical properties (i.e., elongation of 52%, tensile strength of 785 MPa, and a product of tensile strength and elongation of 40.9 GPa·%) have been obtained by adjusting the volume fraction and the stability of austenite. The microstructure of the experimental steels was analyzed by scanning electron microscopy (SEM) and electron back-scatter diffraction (EBSD), and the volume fraction of austenite was estimated by the X-ray diffraction (XRD). The results show that the distribution of austenite grain size is inhomogeneous, and that the mechanical stability of austenite is mainly affected by the alloying partitioning and the variation of grain size during the annealing process. The increase of elongation is attributed to the degradation in mechanical stability of austenite, which can efficiently promote an occurrence of transformation induced plasticity (TRIP) effect.

The Influence of Section Thickness on Microstructure of Elektron 21 and QE22 Magnesium Alloys

2012 ◽  
Vol 191 ◽  
pp. 145-150 ◽  
Author(s):  
Michał Stopyra ◽  
Robert Jarosz ◽  
Andrzej Kiełbus
Keyword(s):  
Solid Solution ◽  
Grain Size ◽  
Magnesium Alloys ◽  
Statistical Methods ◽  
Wall Thickness ◽  
Light Microscope ◽  
Volume Fraction ◽  
Grain Structure ◽  
Section Thickness ◽  
Gating System

The paper presents analysis of section thickness’ influence on microstructure of Elektron 21 and QE22 magnesium alloys in the form of a stepped casting test. Solid solution grain size and volume fraction of eutectic areas were measured using light microscope and sterological methods. The results showed the significant increase of grain size caused by wall thickness and its slight decrease connected with the distance beetwen analysed section and the gating system. This relationship was confirmed using statistical methods. QE22 alloy demonstrated finer grain structure than Elektron 21 alloy as well as lesser susceptibility of grain size to solidification conditions

scholarly journals Novel grain refinement of AZ91E magnesium alloy and the effect on hot tearing during solidfication

2021 ◽  
Author(s):  
Abdallah Elsayed
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Magnesium Alloy ◽  
Grain Refinement ◽  
Magnesium Alloys ◽  
Hot Tearing ◽  
Grain Refining ◽  
Grain Refiner ◽  
Structural Applications ◽  
Hot Tearing Susceptibility

For the A1-5Ti-1B grain refiner, the addition of 0.1 wt.% provided a 68 % reduction in grain size as compared to the unrefined AZ91E alloy at a holding time of five minutes. Grain growth restriction by TiB₂ particles was the source of grain refinement. With the addition of A1-5Ti-1B, only a small reduction in hot tearing susceptibility ws observed because large TiA1₃ particles bonded poorly with the eutectic and blocked feeding channels.The addition of 1.0 wt.% A1-1Ti-3B provided a grain size reduction of 63% as compared to the unrefined AZ91E alloy at a holding time of five minutes. The grain refinement with A1-1Ti-3B addition was attributed to a combination of TiB₂ grain growth restriction and A1B₂ nucleating sites. A significant reduction in hot tearing susceptibility was observed with A1-1Ti-3B addition as a result of a higher cooling rate and shorter local soldification time as compared to the AZ91E alloy. The reduction in hot tearing susceptibility was attributed to the good interface between eutectic and TiB₂ particles. Both grain refiners demonstrated a good resistance to fading during the holding times investigated. In addition, the AZ91E + A1-5Ti-1B and AZ91E + A1-1Ti-3B castings showed much fewer dislocation networks as compared to the untreated AZ91E casting.The development of efficient A1-Ti-B refiners can also improve castability of magnesium alloys. In addition, the fade resistant A1-Ti-B grain refiners can reduce operating costs and maintain productivity on the foundry floor. Thus, magnesium alloy with A1-Ti-B treatment have the potential for more demanding structural applications in the automobile and aerospace industries. Vehicle weight in the aerospace and automotive industries directly impacts carbon emissions and fuel efficiency. An increase in the use of lightweight materials for structural applications will result in lighter vehicles. Low density materials, such as magnesium (1.74 g/cm³) are a potential alternative to aluminium (2.70 g/cm³), to reduce component weight in structural applications.However, current magnesium alloys still do not have adequate mechanical properties and castability to meet the performance specifications of the automotive and aerospace industries. Grain refinement can significantly improve mechanical properties and reduce hot tearing during permanent mould casting. Recently, Al-Ti-B based grain refiners have shown potential in grain refining magnesium-aluminum alloys such as AZ91E. This study investigates the grain refining efficiency and fading of A1-5Ti-1B and A1-1Ti-3B in AZ91E magnesium alloy and their subsequent effect on hot tearing.The grain refiners were added at 0.1, 0.2, 0.5 and 1.0 wt.% levels. For the grain refinement and fading experiments, the castings were prepared using graphite moulds with holding times of 5, 10 and 20 minutes. For the hot tearing experiments, castings were produced representing the optimal addition level of each grain refiner. The castings were prepared using a permanent mould with pouring and mould temperatures of 720 and 180 ºC, respectively. The castings were characterized using SEM, TEM, optical microscopy and thermal analysis.

Effects of Pulsed Magnetic Field on the Microstructure and Mechanical Properties of Mg97Y2Zn1 Alloy

2014 ◽  
Vol 1004-1005 ◽  
pp. 123-126 ◽  
Author(s):  
Jian Yin ◽  
Xiu Jun Ma ◽  
Jun Ping Yao ◽  
Zhi Jian Zhou
Keyword(s):  
Magnetic Field ◽  
Mechanical Properties ◽  
Grain Size ◽  
Volume Fraction ◽  
Pulsed Magnetic Field ◽  
Second Phase ◽  
Microstructure And Mechanical Properties ◽  
Magnetic Field Treatment ◽  
Semi Solid ◽  
Strength And Plasticity

Effect of pulsed magnetic field treatment on the microstructure and mechanical properties of Mg97Y2Zn1 alloy has been investigated. When the pulsed magnetic field is applied on the alloy in semi-solid state, the α-Mg was modified from developed dendrite to fine rosette, resulting in a refined solidification microstructure with the grain size decreased from 4 mm to 0.5 mm. The volume fraction of the second phase ( X phase) increased by about 10 %. The yield strength, fracture strength and plasticity were improved by 21 MPa, 38 MPa and 2.4 %, respectively. The improvement of mechanical properties was attributed to the refined grain size and increased volume fraction of X phase.

The Influence of the Ferrite and Pearlite Grain Size on the S-N Fatigue Characteristics of Steel

2014 ◽  
Vol 224 ◽  
pp. 3-8 ◽  
Author(s):  
Sebastian Kamiński ◽  
Marcel Szymaniec ◽  
Tadeusz Łagoda
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Volume Fraction ◽  
Fatigue Properties ◽  
Phase Volume ◽  
Bending Tests ◽  
Phase Volume Fraction ◽  
Similar Chemical ◽  
Fatigue Characteristics ◽  
Ferrite Grain Size

In this work an investigation of internal structure influence on mechanical and fatigue properties of ferritic-pearlitic steels is shown. Ferrite grain size and phase volume fraction of three grades of structural steel with similar chemical composition, but different mechanical properties, were examined. Afterwards, samples of the materials were subjected to cyclic bending tests. The results and conclusions are presented in this paper

scholarly journals Statistical Analysis of Grain-Scale Effects of Twinning Deformation for Magnesium Alloys under Cyclic Strain Loading

Materials ◽  
2020 ◽  
Vol 13 (11) ◽  
pp. 2454
Author(s):  
Damin Lu ◽  
Shuai Wang ◽  
Yongting Lan ◽  
Keshi Zhang ◽  
Wujun Li ◽  
...  
Keyword(s):  
Grain Size ◽  
Statistical Analysis ◽  
Magnesium Alloys ◽  
Probability Function ◽  
Volume Fraction ◽  
Scale Effects ◽  
Low Cycle Fatigue ◽  
Cyclic Strain ◽  
Statistical Distribution ◽  
Twin Thickness

To reveal the relationship between grain size and twinning deformation of magnesium alloys under cyclic strain, this study carried out a group of strain-controlled low-cycle fatigue experiments and statistical analysis of microstructures. Experimental results show that the shape of the hysteresis loop exhibits significant asymmetry at different strain amplitudes, and the accumulation of residual twins plays an important role in subsequent cyclic deformation. For the different strain amplitudes, the statistical distribution of the grain size of magnesium alloy approximately follows the Weibull probability function distribution, while the statistical distribution of twin thickness is closer to that of Gaussian probability function. The twin nucleation number (TNN) increases with the increase of grain size, but there is no obvious function relationship between twin thickness and grain size. Twin volume fraction (TVF) increases with the increase of grain size, which is mainly due to the increase of TNN. This work can provide experimental evidence for a more accurate description of the twinning deformation mechanism.

scholarly journals Microstructure, and Mechanical and Wear Properties of Grp/AZ91 Magnesium Matrix Composites

Materials ◽  
2019 ◽  
Vol 12 (7) ◽  
pp. 1190 ◽  
Author(s):  
Chang-rui Wang ◽  
Kun-kun Deng ◽  
Yan Bai
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Tensile Strength ◽  
Friction Coefficient ◽  
Wear Rate ◽  
Yield Strength ◽  
Wear Mechanism ◽  
Thermal Deformation ◽  
Volume Fraction ◽  
Az91 Alloy

Based on semi-solid mixing technology, two kinds of as-cast Grp (Graphite particles)/AZ91 composites with different Grp volume fractions (5 vol %, 10 vol %) were prepared; these are called 5 vol % Grp/AZ91 composites and 10 vol % Grp/AZ91 composites, respectively. In order to eliminate casting defects, refine grains, and improve mechanical properties, thermal deformation analysis of these composites was conducted. The effect of the addition of Grp and thermal deformation on the microstructure, mechanical properties, and wear resistance of AZ91 composite was explored. The results showed that after 5 vol % Grp was added into the as-cast AZ91 alloy, Mg17Al12 phases were no longer precipitated reticularly along the grain boundary, and Al4C3 phases were formed inside the composite. With the increase in the volume fraction of Grp, the grains of the AZ91 composites were steadily refined. With the increase of forging pass, the grain size of 5% Grp/AZ91 composites decreased first, and then increased. Additionally, the Grp size decreased gradually. There was little change in the yield strength, and the tensile strength and elongation were improved to a certain extent. After forging and extrusion of 5% Grp/AZ91 composites once, the grain size and Grp size were further reduced, and the yield strength, tensile strength, and elongation were increased by 23%, 30%, and 65%, respectively, compared with the composite after forging. With the increase of the number of forging passes before extrusion, the grain size decreased little by little, while the Grp size remained unchanged. The average yield strength, tensile strength, and elongation of the composites after forging and extrusion six times were increased by 3%, 3%, and 23%, respectively, compared with the composite after forging and extrusion once. The wear rate and friction coefficient of the 5% Grp/AZ91 composites decreased after forging once, and the wear mechanism was mainly due to ploughing wear. By comparison, the wear rate and friction coefficient of the 5% Grp/AZ91 composites increased in the extrusion state, and the main wear mechanism was from wedge formation and micro-cutting wear.

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