Commercial-off-the-Shelf (COTS) 3D Integration using Low Temperature Wafer Bonding

2011 ◽  
Vol 2011 (DPC) ◽  
pp. 000836-000858 ◽  
Author(s):  
Sang Hwui Lee ◽  
Michael Khbeis

This paper reports on a successful 3D integration (3DI) of multi-purpose signal processor (MSP) chips with memory chips using die-to-wafer (D2W) and wafer-to-wafer (W2W) bonding technologies. 3D integration enables compact systems of commercial-off-the-shelf (COTS) parts with high functionality using a wafer-level process for better thinning process uniformity and high yield throughput. The3D system is comprised of commercial Flash memory bare die and MSP bare die. The bare die are face-down aligned to a 150mm diameter silicon handle wafer with alignment marks polished silicon surface. Unique features on the commercial die are detected and used for die registration using a flip-chip bonder with vision automation. An adhesive film between the die and silicon handle wafer are used for temporary bonding. After the die-to-wafer population and bonding, the die substrates are thinned at the wafer-level to a target of 60 microns for the memory die and 25 microns for the MSP die, respectively. The thinned memory die set is permanently transferred onto a 150mm diameter silicon carrier wafer using a low temperature silicon covalent wafer bonding. Following bonding, an adhesive film release process is used to separate the memory die set from the temporary handle wafer. The thinned MSP die on a second handle wafer are then aligned to the thinned memory die set using a wafer-to-wafer alignment tool, and bonded with thin-film polyimide in a high-yield, low temperature wafer bonding process, followed by the release process to separate the MSP die set from the handle wafer. Finally, the MSP/memory stack are electrically connected using a via-last through-silicon-via (TSV) process. One of the key considerations for COTS 3DI is to meet the back-end-of-line (BEOL) thermal budgets of 350–400 Celsius. Plasma-assisted preparation facilitates the reduction in thermal budget for silicon covalent bonding and is performed at 150 Celsius, followed by a long-term annealing process at 175 Celsius. Stacking of thinned die relies on low temperature polyimide bonding that is performed at 200 Celsius. Fluorine and oxygen based plasma surface activation process and CTE-matched polyimide bonding play a critical role in enabling the low temperature bonding for this 3D MSP/memory integration. The thinning and bonding processing details that are presented in this paper are essential for COTS 3DI but can also be applied to several low-profile multi-chip module and packaging applications.

2016 ◽  
Vol 75 (9) ◽  
pp. 345-353 ◽  
Author(s):  
F. Kurz ◽  
T. Plach ◽  
J. Suss ◽  
T. Wagenleitner ◽  
D. Zinner ◽  
...  

2015 ◽  
Vol 2015 (DPC) ◽  
pp. 001847-001884
Author(s):  
Peter Ramm ◽  
Armin Klumpp ◽  
Alan Mathewson ◽  
Kafil M. Razeeb ◽  
Reinhard Pufall

The European 3D heterogeneous integration platform has been established by the consortium of the Integrated Project e-BRAINS [1], where technologies of the following relevant main categories of 3D integration are provided to enable future applications of smart sensor systems:3D System-on-Chip Integration - 3D-SOC: TSV technology for stacking of thinned devices or large IC blocks (global level),3D Wafer-Level-Packaging - 3D-WLP: embedding technology with through-polymer vias (TPV) for stacking of thinned ICs on wafer-level (no TSV), and3D System-in-Package - 3D-SIP: 3D stacking of packaged devices or substrates *definitions according to [2] Regarding TSV performance, the applications do not need ultra-high vertical interconnect densities as for 3D stacked Integrated Circuits – 3D-SIC*. Nevertheless, the lateral sizes of the TSVs are preferably minimized to allow for place and route for small “open” IC areas. Smaller TSVs are also preferred in order to reduce thermo-mechanical stress. e-BRAINS' focus is on how heterogeneous integration and sensor device technologies can be combined to bring new performance levels to targeted applications with high market potentials. The consortium, under coordination of Infineon and technical management by Fraunhofer EMFT, is composed of major European system manufacturers (Infineon, Siemens, SensoNor, 3D PLUS, Vermon and IQE), SMEs (DMCE, Magna Diagnostics, SORIN and eesy-ID), the large research institutions CEA Grenoble, Fraunhofer (EMFT Munich & IIS-EAS Dresden), imec, SINTEF, Tyndall and ITE Warsaw, and universities (EPFL Lausanne, TU Chemnitz and TU Graz). Target applications include automotive, ambient living and medical devices, with a specific focus on wireless sensor systems. Concerning the enabling 3D Heterogeneous Integration Platform, the e-BRAINS partners are working close together, where Infineon, Fraunhofer EMFT, imec and SINTEF are focusing mainly on 3D-SOC and 3D-WLP, and the French system manufacturer 3D PLUS and Tyndall on 3D-WLP and 3D-SIP technologies. The focus of this paper is on low-temperature bonding processes for highly reliable 3D integrated sensor systems. One of the key issues for heterogeneous systems production is the impact of 3D processes to the reliability of the product, i.e. the high built-in stresses caused by e.g. the CTE mismatch of complex layer structures (thin Si, ILDs, metals etc.) in combination with elevated bonding temperatures. As consequence, extensive project work was dedicated in the developments of reliable low-temperature bonding processes. Mainly intermetallic compound (IMC) bonding with Cu/Sn metal systems supported by ultrasonic agitation (Fraunhofer EMFT) was successfully introduced in 3D integration technology (see Fig. 2). A copper/tin solid-liquid interdiffusion (SLID) system was investigated using ultrasonic agitation to reduce the assembly temperature below the melting point of tin. Cleaning procedures are important shortly before joining the samples; dry cleaning has best results due to removal of thin oxide layers. Figure 2 shows a cross section of US supported Cu/Sn bonding at 150C. The intermetallic compounds Cu3Sn and Cu6Sn5 as well as pure tin easily can be identified. Due to low temperature assembly the most stable intermetallic compound (IMC) Cu3Sn has a minor share of the metal system. Most importantly there is no gap between top and bottom part of the joint despite the macroscopic assembly temperature is far away from the melting point of tin. But maybe the ultrasonic agitation brings enough energy to the interfaces, so locally melting can occur. In this way robust IMC bonding technology at 150C could be demonstrated with shear forces of 17 MPa and an alignment accuracy of 3 μm, well-suited for 3D integration. Figure 2: Low-temperature IMC bonding technology using ultrasonic agitation (Fraunhofer EMFT) Reliability for SLID contacts is certainly a very challenging objective especially looking for robust solutions in automotive applications. Thermally induced mechanical stress is the main reason for early fails during temperature cycling. Cross sectioned samples were investigated and methods like nanoindentation, Raman spectroscopy, fibDAC, and high local resolution x-ray scattering were applied to measure the intrinsic stresses. It can be shown that low temperature bonding is the right approach to avoid excessive stress cracking the interface or even fracturing the silicon. Also fatigue of metals can be reduced in a range that plastic deformation is no lifetime limiting factor.


2012 ◽  
Vol 2012 (DPC) ◽  
pp. 1-24
Author(s):  
Michael Gallagher ◽  
Jong-Uk Kim ◽  
Eric Huenger ◽  
Kai Zoschke ◽  
Christina Lopper ◽  
...  

3D stacking, one of the 3D integration technologies using through silicon vias (TSVs), is considered as a desirable 3D solution due to its cost effectiveness and matured technical background. For successful 3D stacking, precisely controlled bonding of the two substrates is necessary, so that various methods and materials have been developed over the last decade. Wafer bonding using polymeric adhesives has advantages. Surface roughness, which is critical in direct bonding and metal-to-metal bonding, is not a significant issue, as the organic adhesive can smooth out the unevenness during bonding process. Moreover, bonding of good quality can be obtained using relatively low bonding pressure and low bonding temperature. Benzocyclobutene (BCB) polymers have been commonly used as bonding adhesives due to their relatively low curing temperature (~250 °C), very low water uptake (<0.2%), excellent planarizing capability, and good affinity to Cu metal lines. In this study, we present wafer bonding with BCB at various conditions. In particular, bonding experiments are performed at low temperature range (180 °C ~ 210 °C), which results in partially cured state. In order to examine the effectiveness of the low temperature process, the mechanical (adhesion) strength and dimensional changes are measured after bonding, and compared with the values of the fully cured state. Two different BCB polymers, dry-etch type and photo type, are examined. Dry etch BCB is proper for full-area bonding, as it has low degree of cure and therefore less viscosity. Photo-BCB has advantages when a pattern (frame or via open) is to be structured on the film, since it is photoimageable (negative tone), and its moderate viscosity enables the film to sustain the patterns during the wafer bonding process. The effect of edge beads at the wafer rim area and the soft cure (before bonding) conditions on the bonding quality are also studied. Alan/Rey ok move from Flip Chip and Wafer Level Packaging 1-6-12.


2013 ◽  
Vol 2013 (1) ◽  
pp. 000516-000522 ◽  
Author(s):  
G. Parès ◽  
A. Attard ◽  
F. Dosseul ◽  
A. N'Hari ◽  
O. Boillon ◽  
...  

3D integration relying on novel vertical interconnection technologies opens the gate to powerful microelectronic systems in ultra-thin packages answering the demand of the mobile market. Among these, die-to-wafer stacking is a key enabling technology for 2.5D as well as for 3D with technological challenges driven by, in one hand, the increase of the die surface and the number of I/Os and, on the other hand, the reduction of the vertical dimensions. In our integration scheme we have achieved flip chip stacking (or Face to Face) of 35 μm ultra-thin dies with low stand-off (< 15 μm) copper micro-bumps and tin-silver-copper solders (SAC). Ultra-thin dies are prepared using dicing before grinding (DBG) technique. After DBG, plasma stress release process is applied to the backside of the singulated chips. Copper μbump technology is challenging with this very low profile stacking since the current flip chip process is no longer adapted to this geometry and that the die flatness tolerance become very critical to obtain a high soldering yield. Process improvements have been achieved on the copper pillar fabrication itself with several metallurgy stack configurations as well as new processes using damascene techniques. Furthermore, innovative technologies have been deployed on the pick and place and collective soldering processes. Intermetallic formation during reflow process is achieved through transient liquid phase (TLP) reaction leading to thorough consumption of the tin layer and to the formation of Cu6Sn5 and Cu3Sn compounds. Capillary underfill is finally successfully applied in the narrow die-to-wafer gap by jetting technique. After optimization, electrical tests show a very high yield close to 100% over a representative number of fully populated wafers. Reliability tests have also been carried out at wafer level exhibiting no significant resistance increase or yield loss over 1000 thermal cycles between −40 and +125°C.


2004 ◽  
Vol 14 (7) ◽  
pp. 884-890 ◽  
Author(s):  
M M V Taklo ◽  
P Storås ◽  
K Schjølberg-Henriksen ◽  
H K Hasting ◽  
H Jakobsen

2019 ◽  
Vol 2019 (NOR) ◽  
pp. 000012-000016
Author(s):  
Henri Ailas ◽  
Jaakko Saarilahti ◽  
Tuomas Pensala ◽  
Jyrki Kiihamäki

Abstract In this study, a low temperature wafer-level packaging process aimed for encapsulating MEMS mirrors was developed. The glass cap wafer used in the package has an antireflective (AR) coating that limits the maximum temperature of the bonding process to 250°C. Copper thermocompression was used as copper has a high self-diffusivity and the native oxidation on copper surfaces can be completely removed with combination of ex situ acetic acid wet-etch and in situ forming gas anneal. Making it suitable for a development of a low temperature bonding process. In this work, bonding on of sputtered and electrodeposited copper films was studied on temperatures ranging from 200°C to 300°C as well as the effect of pretreatment on bond strength. The study presents a successful thermocompression bonding process for sputtered Cu films at a low temperature of 200°C with high yield of 97 % after dicing. The bond strength was recorded to be 75 MPa, well above the MIL-STD-883E standard (METHOD 2019.5) rejection limit of 6.08 MPa. The high dicing yield and bond strength suggest that the thermocompression bonding could be possible even at temperatures below 200°C. However, the minimum bonding temperature was not yet determined in this study.


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