scholarly journals Frictional properties and microstructural evolution of dry and wet calcite-dolomite gouges

2020 ◽  
Author(s):  
Matteo Demurtas ◽  
Steven A.F. Smith ◽  
Elena Spagnuolo ◽  
Giulio Di Toro
Keyword(s):  
Microstructural Evolution ◽  
Shear Zones ◽  
Slip Zone ◽  
Cyclic Process ◽  
Experimental Conditions ◽  
Slip Rates ◽  
Bearing Faults ◽  
Seismic Slip ◽  
Wide Range ◽  
Dynamic Weakening

Abstract. Calcite and dolomite are the two most common minerals in carbonate-bearing faults and shear zones. Motivated by field examples from exhumed seismogenic faults in the Italian Central Apennines, we investigated the frictional and microstructural evolution of gouge mixtures consisting of 50 wt % calcite and 50 wt % dolomite using a rotary-shear apparatus. The gouges were sheared at a range of slip rates (30 µm s−1–1 m s−1), displacements (0.05–0.4 m), and normal loads (17.5–26 MPa), under both room humidity and water-dampened conditions. The frictional behaviour and microstructural evolution of the gouges were strongly influenced by the presence of water. At room humidity, slip strengthening behaviour was observed up to slip rates of 0.01 m s−1, which was associated with gouge dilation and the development of a 500–900 µm wide slip zone cut by Y-, R-, and R1-shear bands. Above a slip rate of 0.1 m s−1, dynamic weakening accompanied the development of a localised <100 µm thick principal slip zone preserving microstructural evidence for calcite recrystallization and dolomite decarbonation, while the bulk gouges developed a well-defined foliation consisting of organized domains of heavily fractured calcite and dolomite. In water-dampened conditions, evidence of gouge fluidization within a fine-grained principal slip zone was observed at a wide range of slip-rates from 30 µm s−1 to 0.1 m s−1, suggesting that caution is needed when relating fluidization textures to seismic slip in natural fault zones. Dynamic weakening in water-dampened conditions was observed at 1 m s−1, where the principal slip zone was characterised by patches of recrystallized calcite. However, local fragmentation and reworking of recrystallized calcite suggests a cyclic process involving formation and destruction of a heterogeneous slip zone. Our microstructural data show that development of a well-defined gouge foliation at these experimental conditions is limited to high-velocity (>0.1 m s−1) and room humidity, supporting the notion that some foliated gouges and cataclasites may form during seismic slip in natural carbonate-bearing faults.

scholarly journals Frictional properties and microstructural evolution of dry and wet calcite–dolomite gouges

Solid Earth ◽  
2021 ◽  
Vol 12 (3) ◽  
pp. 595-612
Author(s):  
Matteo Demurtas ◽  
Steven A.F. Smith ◽  
Elena Spagnuolo ◽  
Giulio Di Toro
Keyword(s):  
Microstructural Evolution ◽  
Normal Load ◽  
Shear Zones ◽  
Slip Zone ◽  
Cyclic Process ◽  
Experimental Conditions ◽  
Slip Rates ◽  
Bearing Faults ◽  
Seismic Slip ◽  
Dynamic Weakening

Abstract. Calcite and dolomite are the two most common minerals in carbonate-bearing faults and shear zones. Motivated by observations of exhumed seismogenic faults in the Italian Central Apennines, we used a rotary-shear apparatus to investigate the frictional and microstructural evolution of ca. 3 mm thick gouge layers consisting of 50 wt % calcite and 50 wt % dolomite. The gouges were sheared at a range of slip rates (30 µm s−1–1 m s−1), displacements (0.05–0.4 m), and a normal load of 17.5 MPa under both room-humidity and water-dampened conditions. The frictional behaviour and microstructural evolution of the gouges were strongly influenced by the presence of water. At room humidity, slip strengthening was observed up to slip rates of 0.01 m s−1, which was associated with gouge dilation and the development of a 500–900 µm wide slip zone cut by Y-, R-, and R1-shear bands. Above a slip rate of 0.1 m s−1, dynamic weakening accompanied the development of a localised < 100 µm thick principal slip zone preserving microstructural evidence for calcite recrystallisation and dolomite decarbonation, while the bulk gouges developed a well-defined foliation consisting of organised domains of heavily fractured calcite and dolomite. In water-dampened conditions, evidence of gouge fluidisation within a fine-grained principal slip zone was observed at a range of slip rates from 30 µm s−1 to 0.1 m s−1, suggesting that caution is needed when relating fluidisation textures to seismic slip in natural fault zones. Dynamic weakening in water-dampened conditions was observed at 1 m s−1, where the principal slip zone was characterised by patches of recrystallised calcite. However, local fragmentation and reworking of recrystallised calcite suggests a cyclic process involving formation and destruction of a heterogeneous slip zone. Our microstructural data show that development of well-defined gouge foliation under the tested experimental conditions is limited to high velocities (>0.1 m s−1) and room humidity, supporting the notion that some foliated gouges and cataclasites may form during seismic slip in natural carbonate-bearing faults.

scholarly journals Hematite (U-Th)/He thermochronometry detects asperity flash heating during laboratory earthquakes

Geology ◽  
2020 ◽  
Vol 48 (5) ◽  
pp. 514-518 ◽  
Author(s):  
Gabriele Calzolari ◽  
Alexis K. Ault ◽  
Greg Hirth ◽  
Robert G. McDermott
Keyword(s):  
High Temperatures ◽  
Temperature Rise ◽  
Thick Layer ◽  
Seismogenic Zone ◽  
Experimental Conditions ◽  
Slip Rates ◽  
Seismic Slip ◽  
Slip Surfaces ◽  
Before And After ◽  
Dynamic Weakening

Abstract Evidence for coseismic temperature rise that induces dynamic weakening is challenging to directly observe and quantify in natural and experimental fault rocks. Hematite (U-Th)/He (hematite He) thermochronometry may serve as a fault-slip thermometer, sensitive to transient high temperatures associated with earthquakes. We test this hypothesis with hematite deformation experiments at seismic slip rates, using a rotary-shear geometry with an annular ring of silicon carbide (SiC) sliding against a specular hematite slab. Hematite is characterized before and after sliding via textural and hematite He analyses to quantify He loss over variable experimental conditions. Experiments yield slip surfaces localized in an ∼5–30-µm-thick layer of hematite gouge with &lt;300-µm-diameter fault mirror (FM) zones made of sintered nanoparticles. Hematite He analyses of undeformed starting material are compared with those of FM and gouge run products from high-slip-velocity experiments, showing &gt;71% ± 1% (1σ) and 18% ± 3% He loss, respectively. Documented He loss requires short-duration, high temperatures during slip. The spatial heterogeneity and enhanced He loss from FM zones are consistent with asperity flash heating (AFH). Asperities &gt;200–300 µm in diameter, producing temperatures &gt;900 °C for ∼1 ms, can explain observed He loss. Results provide new empirical evidence describing AFH and the role of coseismic temperature rise in FM formation. Hematite He thermochronometry can detect AFH and thus seismicity on natural FMs and other thin slip surfaces in the upper seismogenic zone of Earth’s crust.

scholarly journals Dynamic weakening of serpentinite gouges and bare surfaces at seismic slip rates

2014 ◽  
Vol 119 (11) ◽  
pp. 8107-8131 ◽  
Author(s):  
B. P. Proctor ◽  
T. M. Mitchell ◽  
G. Hirth ◽  
D. Goldsby ◽  
F. Zorzi ◽  
...  
Keyword(s):  
Slip Rates ◽  
Seismic Slip ◽  
Dynamic Weakening

Strongly Coupled Redox-Linked Conformational Switching at the Active Site of the Non-Heme Iron-Dependent Dioxygenase, TauD

2019 ◽  
Author(s):  
Christopher John ◽  
Greg M. Swain ◽  
Robert P. Hausinger ◽  
Denis A. Proshlyakov
Keyword(s):  
Active Site ◽  
Structural Model ◽  
Heme Iron ◽  
Chemical Transformations ◽  
Experimental Conditions ◽  
Strongly Coupled ◽  
Non Heme Iron ◽  
Reversible Redox ◽  
Wide Range ◽  
Complex Structural

2-Oxoglutarate (2OG)-dependent dioxygenases catalyze C-H activation while performing a wide range of chemical transformations. In contrast to their heme analogues, non-heme iron centers afford greater structural flexibility with important implications for their diverse catalytic mechanisms. We characterize an <i>in situ</i> structural model of the putative transient ferric intermediate of 2OG:taurine dioxygenase (TauD) by using a combination of spectroelectrochemical and semi-empirical computational methods, demonstrating that the Fe (III/II) transition involves a substantial, fully reversible, redox-linked conformational change at the active site. This rearrangement alters the apparent redox potential of the active site between -127 mV for reduction of the ferric state and 171 mV for oxidation of the ferrous state of the 2OG-Fe-TauD complex. Structural perturbations exhibit limited sensitivity to mediator concentrations and potential pulse duration. Similar changes were observed in the Fe-TauD and taurine-2OG-Fe-TauD complexes, thus attributing the reorganization to the protein moiety rather than the cosubstrates. Redox difference infrared spectra indicate a reorganization of the protein backbone in addition to the involvement of carboxylate and histidine ligands. Quantitative modeling of the transient redox response using two alternative reaction schemes across a variety of experimental conditions strongly supports the proposal for intrinsic protein reorganization as the origin of the experimental observations.

scholarly journals Low-Energy Electron Damage to Condensed-Phase DNA and Its Constituents

2021 ◽  
Vol 22 (15) ◽  
pp. 7879
Author(s):  
Yingxia Gao ◽  
Yi Zheng ◽  
Léon Sanche
Keyword(s):  
Condensed Phase ◽  
Genetic Material ◽  
High Energy ◽  
Dna Lesions ◽  
Low Energy ◽  
Experimental Investigations ◽  
Experimental Conditions ◽  
Strand Breaks ◽  
Sequence Of Events ◽  
Wide Range

The complex physical and chemical reactions between the large number of low-energy (0–30 eV) electrons (LEEs) released by high energy radiation interacting with genetic material can lead to the formation of various DNA lesions such as crosslinks, single strand breaks, base modifications, and cleavage, as well as double strand breaks and other cluster damages. When crosslinks and cluster damages cannot be repaired by the cell, they can cause genetic loss of information, mutations, apoptosis, and promote genomic instability. Through the efforts of many research groups in the past two decades, the study of the interaction between LEEs and DNA under different experimental conditions has unveiled some of the main mechanisms responsible for these damages. In the present review, we focus on experimental investigations in the condensed phase that range from fundamental DNA constituents to oligonucleotides, synthetic duplex DNA, and bacterial (i.e., plasmid) DNA. These targets were irradiated either with LEEs from a monoenergetic-electron or photoelectron source, as sub-monolayer, monolayer, or multilayer films and within clusters or water solutions. Each type of experiment is briefly described, and the observed DNA damages are reported, along with the proposed mechanisms. Defining the role of LEEs within the sequence of events leading to radiobiological lesions contributes to our understanding of the action of radiation on living organisms, over a wide range of initial radiation energies. Applications of the interaction of LEEs with DNA to radiotherapy are briefly summarized.

scholarly journals Review of the Upright Balance Assessment Based on the Force Plate

2021 ◽  
Vol 18 (5) ◽  
pp. 2696
Author(s):  
Baoliang Chen ◽  
Peng Liu ◽  
Feiyun Xiao ◽  
Zhengshi Liu ◽  
Yong Wang
Keyword(s):  
Postural Balance ◽  
Force Plate ◽  
Assessment Method ◽  
Balance Assessment ◽  
Experimental Conditions ◽  
Methodological Research ◽  
Assessment Tests ◽  
Wide Range ◽  
Foot Posture ◽  
Plate System

Quantitative assessment is crucial for the evaluation of human postural balance. The force plate system is the key quantitative balance assessment method. The purpose of this study is to review the important concepts in balance assessment and analyze the experimental conditions, parameter variables, and application scope based on force plate technology. As there is a wide range of balance assessment tests and a variety of commercial force plate systems to choose from, there is room for further improvement of the test details and evaluation variables of the balance assessment. The recommendations presented in this article are the foundation and key part of the postural balance assessment; these recommendations focus on the type of force plate, the subject’s foot posture, and the choice of assessment variables, which further enriches the content of posturography. In order to promote a more reasonable balance assessment method based on force plates, further methodological research and a stronger consensus are still needed.

scholarly journals Tire/Road Rolling Resistance Modeling: Discussing the Surface Macrotexture Effect

Coatings ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 538
Author(s):  
Malal Kane ◽  
Ebrahim Riahi ◽  
Minh-Tan Do
Keyword(s):  
Slip Rate ◽  
Rolling Resistance ◽  
Friction Model ◽  
Slip Rates ◽  
Wide Range ◽  
Road Surfaces ◽  
Profile Depth ◽  
Experimental Rolling ◽  
Resistance Modeling ◽  
Pavement Friction

This paper deals with the modeling of rolling resistance and the analysis of the effect of pavement texture. The Rolling Resistance Model (RRM) is a simplification of the no-slip rate of the Dynamic Friction Model (DFM) based on modeling tire/road contact and is intended to predict the tire/pavement friction at all slip rates. The experimental validation of this approach was performed using a machine simulating tires rolling on road surfaces. The tested pavement surfaces have a wide range of textures from smooth to macro-micro-rough, thus covering all the surfaces likely to be encountered on the roads. A comparison between the experimental rolling resistances and those predicted by the model shows a good correlation, with an R2 exceeding 0.8. A good correlation between the MPD (mean profile depth) of the surfaces and the rolling resistance is also shown. It is also noticed that a random distribution and pointed shape of the summits may also be an inconvenience concerning rolling resistance, thus leading to the conclusion that beyond the macrotexture, the positivity of the texture should also be taken into account. A possible simplification of the model by neglecting the damping part in the constitutive model of the rubber is also noted.

scholarly journals Towards Reduced CNNs for De-Noising Phase Images Corrupted with Speckle Noise

Photonics ◽  
2021 ◽  
Vol 8 (7) ◽  
pp. 255
Author(s):  
Marie Tahon ◽  
Silvio Montresor ◽  
Pascal Picart
Keyword(s):  
Phase Error ◽  
Speckle Noise ◽  
Experimental Conditions ◽  
Benchmark Data ◽  
Wide Range ◽  
Phase Images ◽  
Different Depths ◽  
Phase Data ◽  
Do So

Digital holography is a very efficient technique for 3D imaging and the characterization of changes at the surfaces of objects. However, during the process of holographic interferometry, the reconstructed phase images suffer from speckle noise. In this paper, de-noising is addressed with phase images corrupted with speckle noise. To do so, DnCNN residual networks with different depths were built and trained with various holographic noisy phase data. The possibility of using a network pre-trained on natural images with Gaussian noise is also investigated. All models are evaluated in terms of phase error with HOLODEEP benchmark data and with three unseen images corresponding to different experimental conditions. The best results are obtained using a network with only four convolutional blocks and trained with a wide range of noisy phase patterns.

scholarly journals Creep Behaviour and Microstructural Characterization of VAT 36 and VAT 32 Superalloys

Metals ◽  
2018 ◽  
Vol 8 (11) ◽  
pp. 877 ◽  
Author(s):  
Vagner Gobbi ◽  
Silvio Gobbi ◽  
Danieli Reis ◽  
Jorge Ferreira ◽  
José Araújo ◽  
...  
Keyword(s):  
Failure Analysis ◽  
Creep Resistance ◽  
High Performance ◽  
Creep Behaviour ◽  
Ductile Failure ◽  
Microstructural Characterization ◽  
Dislocation Slip ◽  
Creep Tests ◽  
Experimental Conditions ◽  
Wide Range

Superalloys are used primarily for the aerospace, automotive, and petrochemical industries. These applications require materials with high creep resistance. In this work, evaluation of creep resistance and microstructural characterization were carried out at two new nickel intermediate content alloys for application in aerospace industry and in high performance valves for automotive applications (alloys VAT 32 and VAT 36). The alloys are based on a high nickel chromium austenitic matrix with dispersion of intermetallic L12 and phases containing different (Nb,Ti)C carbides. Creep tests were performed at constant load, in the temperature range of 675–750 °C and stress range of 500–600 MPa. Microstructural characterization and failure analysis of fractured surfaces of crept samples were carried out with optical and scanning electron microscopy with EDS. Phases were identified by Rietveld refinement. The results showed that the superalloy VAT 32 has higher creep resistance than the VAT 36. The superior creep resistance of the alloy VAT 32 is related to its higher fraction of carbides (Nb,Ti)C and intermetallic L12 provided by the amount of carbon, titanium, and niobium in its chemical composition and subsequent heat treatment. During creep deformation these precipitates produce anchoring effect of grain boundaries, hindering relative slide between grains and therefore inhibiting crack formation. These volume defects act also as obstacles to dislocation slip and climb, decreasing the creep rate. Failure analysis of surface fractures of crept samples showed intergranular failure mechanism at crack origin for both alloys VAT 36 and VAT 32. Intergranular fracture involves nucleation, growth, and subsequent binding of voids. The final fractured portion showed transgranular ductile failure, with dimples of different shapes, generated by the formation and coalescence of microcavities with dissimilar shape and sizes. The occurrence of a given creep mechanism depends on the test conditions. At creep tests of VAT 32 and VAT 36, for lower stresses and higher temperature, possible dislocation climb over carbides and precipitates would prevail. For higher stresses and intermediate temperatures shear mechanisms involving stacking faults presumably occur over a wide range of experimental conditions.

scholarly journals Partitional calorimetry

2019 ◽  
Vol 126 (2) ◽  
pp. 267-277 ◽  
Author(s):  
Matthew N. Cramer ◽  
Ollie Jay
Keyword(s):  
Heat Balance ◽  
Estimation Error ◽  
Fluid Replacement ◽  
Whole Body ◽  
Exposure Limits ◽  
Experimental Conditions ◽  
Direct Calorimetry ◽  
Fundamental Properties ◽  
Wide Range ◽  
Partitional Calorimetry

For thermal physiologists, calorimetry is an important methodological tool to assess human heat balance during heat or cold exposures. A whole body direct calorimeter remains the gold standard instrument for assessing human heat balance; however, this equipment is rarely available to most researchers. A more widely accessible substitute is partitional calorimetry, a method by which all components of the conceptual heat balance equation—metabolic heat production, conduction, radiation, convection, and evaporation—are calculated separately based on fundamental properties of energy exchange. Since partitional calorimetry requires relatively inexpensive equipment (vs. direct calorimetry) and can be used over a wider range of experimental conditions (i.e., different physical activities, laboratory or field settings, clothed or seminude), it allows investigators to address a wide range of problems such as predicting human responses to thermal stress, developing climatic exposure limits and fluid replacement guidelines, estimating clothing properties, evaluating cooling/warming interventions, and identifying potential thermoregulatory dysfunction in unique populations. In this Cores of Reproducibility in Physiology (CORP) review, we summarize the fundamental principles underlying the use of partitional calorimetry, present the various methodological and arithmetic requirements, and provide typical examples of its use. Strategies to minimize estimation error of specific heat balance components, as well as the limitations of the method, are also discussed. The goal of this CORP paper is to present a standardized methodology and thus improve the accuracy and reproducibility of research employing partitional calorimetry.

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