Estimating the uncertainty of measurements of thermal conductivity of thin films of thermoelectrics with the 3-omega method

Using the method of computer simulation, the uncertainty of measurements of the thermal conductivity of silicon, which is often used as substrates, and also thin films based on bismuth, is estimated. The influence of the application of an additional dielectric layer between the thermoelectric film and the resistive heater on the measurement results is shown.

Continuous Wave Laser Nanowelding Process of Ag Nanowires on Flexible Polymer Substrates

In this paper we present the laser nanowelding process of silver nanowires (AgNWs) deposited on flexible polymer substrates by continuous wave (CW) lasers. CW lasers are cost-effective and can provide moderate power density, somewhere between nanosecond pulsed lasers and flash lamps, which is just enough to perform the nanowelding process efficiently and does not damage the nanowires or the polymer substrates. Here, an Nd:YAG CW laser (wavelength 532 nm) was used to perform the nanowelding of AgNWs on polyethylene terephthalate (PET) substrates. Key process parameters such as laser power, scan speed, and number of scans were studied and optimized, and mechanisms of observed phenomena are discussed. Our best result demonstrates a sheet resistance of 12 ohm/squ with a transmittance at λ = 550 nm of 92% for AgNW films on PET substrates. A transparent resistive heater was made, and IR pictures were taken to show the high uniformity of the CW laser nanowelded AgNW film. Our findings show that highly effective and efficient nanowelding can be achieved without the need of expensive pulse lasers or light sources, which may contribute to lower the cost of mass producing AgNWs on flexible substrates.

Operation of the Prototype Device for Induction Heating of Railway Turnouts at Various Operating Frequencies

Devices for electric heating of railroad turnouts are elements of the railway infrastructure protecting railroad turnouts against blocking them by snow and ice in winter. They often operate based on the principle of resistance heating but other solutions are also emerging. In this paper, one of such new solutions using the phenomenon of electromagnetic induction was presented and tested under various conditions. In comparison with traditional resistive heaters, the inductive ones offer heat distribution directly to ice and snow without intermediation of rails. Moreover, they can use a wide range spectrum of frequency to shorten the melting time. The resistive and inductive devices were tested with respect to melting time, temperatures and energy consumption. It follows that the induction-based device offers much lower energy consumption at a level of 30%–60% of that by resistive heater. The details depend on frequency used, initial temperature and number of induction devices of action assumed equivalent to the resistive one. Inductive heating of turnouts also offers shorter times of operation, which are obtained for frequencies in the range 40–70 kHz. The inductive device was also tested with respect to magnetic field levels around it to assess its possible influence on nearby infrastructure.

Robotic Multi-Probe-Single-Actuator Inchworm Neural Microdrive

Electrophysiology is one of the major experimental techniques used in neuroscience. The favorable spatial and temporal resolution as well as the increasingly larger site counts of brain recording electrodes contribute to the popularity and importance of electrophysiology in neuroscience. Such electrodes are typically mechanically placed in the brain to perform acute or chronic freely moving animal measurements. The micro positioners currently used for such tasks employ a single translator per independent probe being placed into the targeted brain region, leading to significant size and weight restrictions. To overcome this limitation, we have developed a miniature robotic multi-probe neural microdrive that utilizes novel phase-change-material-filled resistive heater micro-grippers. The microscopic dimensions, gentle gripping action, independent electronic actuation control, and high packing density of the grippers allow for micrometer-precision independent positioning of multiple arbitrarily shaped parallel neural electrodes with only a single piezo actuator in an inchworm motor configuration. This multi-probe-single-actuator design allows for significant size and weight reduction, as well as remote control and potential automation of the microdrive. We demonstrate accurate placement of multiple independent recording electrodes into the CA1 region of the rat hippocampus in vivo in acute and chronic settings. Thus, our robotic neural microdrive technology is applicable towards basic neuroscience and clinical studies, as well as other multi-probe or multi-sensor micro-positioning applications.One Sentence SummaryMiniature robotic multi-probe single-actuator microdrive utilizing phase change material based micro-grippers.

DNA Ligation on a Digital Microfluidic Device

This investigation demonstrates that digital microfluidic platforms are suitable for automated DNA ligation. Multiple DNA ligation steps are required to create DNA products using oligonucleotide synthesis. Unfortunately, traditional methods of oligonucleotide synthesis are unable to create highly accurate, long DNA products. This leads to a supply-side bottleneck that puts a drag on innovation in drug development, organism engineering, and agricultural improvement. Here we demonstrate ligation of two DNA products into one DNA product in digital microfluidic devices that manipulate droplets in air and in oil. Results from the gel electrophoresis imaging confirmed that ligation on digital microfluidics devices was successful in all cases. Silicone oil experiments also verified that on-chip incubation of DNA ligation is possible on these devices using an external resistive heater. This suggests that large-scale DMF automation of DNA synthesis can be used to alleviate the bottleneck created by the lack of efficient, high-volume production of long change DNA products. Such an advancement would be highly valued for a wide variety of biomedical applications.

In-Plane and Out-of-Plane MEMS Piezoresistive Cantilever Sensors for Nanoparticle Mass Detection

In this study, we investigate the performance of two piezoresistive micro-electro-mechanical system (MEMS)-based silicon cantilever sensors for measuring target analytes (i.e., ultrafine particulate matters). We use two different types of cantilevers with geometric dimensions of 1000 × 170 × 19.5 µm3 and 300 × 100 × 4 µm3, which refer to the 1st and 2nd types of cantilevers, respectively. For the first case, the cantilever is configured to detect the fundamental in-plane bending mode and is actuated using a resistive heater. Similarly, the second type of cantilever sensor is actuated using a meandering resistive heater (bimorph) and is designed for out-of-plane operation. We have successfully employed these two cantilevers to measure and monitor the changes of mass concentration of carbon nanoparticles in air, provided by atomizing suspensions of these nanoparticles into a sealed chamber, ranging from 0 to several tens of µg/m3 and oversize distributions from ~10 nm to ~350 nm. Here, we deploy both types of cantilever sensors and operate them simultaneously with a standard laboratory system (Fast Mobility Particle Sizer, FMPS, TSI 3091) as a reference.

Wirelessly powered and remotely controlled valve-array for highly multiplexed analytical assay automation on a centrifugal microfluidic platform

In this paper we present a wirelessly powered array of 128 centrifugo-pneumatic valves that can be thermally actuated on demand during spinning. The valves can either be triggered by a predefined protocol, wireless signal transmission via Bluetooth, or in response to a sensor monitoring parameters like temperature or homogeneity of the dispersion. Upon activation of a resistive heater, a low-melting membrane (ParafilmTM) is removed to vent an entrapped gas pocket, thus letting the incoming liquid wet an intermediate dissolvable film and thus open the valve. The proposed system allows up to 12 heaters to be activated in parallel with a response time below 3 seconds, potentially, resulting in 128 actuated valves in under 30 seconds. We demonstrate with three examples of common and standard procedures how the proposed technology could become a powerful tool for implementing diagnostic assays on Lab-on-a-Disc. First, we implement wireless actuation of 64 valves during rotation in a freely programmable sequence, or upon user input in real time.Then, we show a closed-loop centrifugal flow control sequence where the state of mixing between reagents evaluated from stroboscopically recorded images triggers the opening of valves. In our last experiment valving and closed-loop control are used to facilitate centrifugal processing of whole blood.

Demonstration of a Solid-State Inflation Balloon Deorbiter

This paper updates on the recent development of the novel Solid State Inflation Balloon (SSIB), a simple, reliable, low-cost, non-propulsive deorbit mechanism for the full range of small satellites, defined by NASA as less than 180 kg. It aims to focus on the recent demonstration, for the first time, inflation of a ∼10 cm sized balloon in a vacuum chamber. Small satellites typically rely on aerodynamic drag to deorbit within the FAA’s 25 year requirements. The SSIB will enhance aerodynamic drag by inflating a balloon at the end-of-life of a satellite mission. This technology will provide a scalable and non-existing capability, low-cost deorbit, for applications in the full-range of smallsats, from CubeSats to MicroSats. The SSIB system is composed of three major components: a Micro-Electro-Mechanical Systems (MEMS) Solid-State Gas Generator (SSGG) chip, a balloon structure made of thin film compatible with space environment (i.e. Mylar, Kapton, or Teflon), and a sub-system package suitable for spacecraft integration. The SSGG is composed of a 2D addressable array of sodium azide (NaN3) crystals, confined by Su-8 wells, on a glass substrate. Current versions include 2×2 and 8×8 arrays designed for a full range of small satellites. Under each well is a resistive heater and when heated to above 350 °C, the NaN3 spontaneously decomposes to generate N2 gas in time scales on the order of 10 milliseconds. Each well is designed with a typical volume of 10–15 m3 to 10−6 m3 of NaN3 (i.e. 1,500 μm × 1,500 μm × 150 μm on the larger end of the spectrum). The SSIB system is low power (∼1 W per well for less than 10 seconds) and have low mass (∼100 grams, where mass is dominated by the size of the required balloon). Initial simulations have shown that the SSIB with balloons of 1 m2 cross-section can deorbit small satellites from above 1000 km well within 25 years.