scholarly journals Authors’ Reply to the Discussion by Crisci et al. (2021) on “Experimental Deformation of Opalinus Clay at Elevated Temperature and Pressure Conditions Mechanical Properties and the Influence of Rock Fabric”

Author(s):  
Valerian Schuster ◽  
Erik Rybacki ◽  
Audrey Bonnelye ◽  
Georg Dresen
Author(s):  
Eleonora Crisci ◽  
Alessio Ferrari ◽  
Lyesse Laloui

AbstractThe testing procedure and results on saturated samples of Opalinus Clay in the work of Schuster et al. (Rock Mech Rock Eng https://doi.org/10.1007/s00603-021-02474-3, 2021) were conducted and presented using strain rates two to four orders of magnitudes higher than the rates needed to allow pore pressure equilibrium in the material, both in drained and undrained conditions. This leads to an erroneous estimation of the mechanical properties in saturated conditions. We discuss this aspect in the context of shale testing. We also discuss the effect of drying-induced fissuring on the mechanical properties of geomaterials tested in dry conditions.


2021 ◽  
Vol 92 (4) ◽  
pp. 043711
Author(s):  
Harm Ridder ◽  
Christoph Sinn ◽  
Georg R. Pesch ◽  
Jan Ilsemann ◽  
Wolfgang Dreher ◽  
...  

Polymers ◽  
2021 ◽  
Vol 13 (9) ◽  
pp. 1473
Author(s):  
Jun Zhao ◽  
Kang Wang ◽  
Shuaibin Wang ◽  
Zike Wang ◽  
Zhaohui Yang ◽  
...  

This paper presents results from experimental work on mechanical properties of geopolymer concrete, mortar and paste prepared using fly ash and blended slag. Compressive strength, splitting tensile strength and flexural strength tests were conducted on large sets of geopolymer and ordinary concrete, mortar and paste after exposure to elevated temperatures. From Thermogravimetric analyzer (TGA), X-ray diffraction (XRD), Scanning electron microscope (SEM) test results, the geopolymer exhibits excellent resistance to elevated temperature. Compressive strengths of C30, C40 and C50 geopolymer concrete, mortar and paste show incremental improvement then followed by a gradual reduction, and finally reach a relatively consistent value with an increase in exposure temperature. The higher slag content in the geopolymer reduces residual strength and the lower exposure temperature corresponding to peak residual strength. Resistance to elevated temperature of C40 geopolymer concrete, mortar and paste is better than that of ordinary concrete, mortar and paste at the same grade. XRD, TGA and SEM analysis suggests that the heat resistance of C–S–H produced using slag is lower than that of sulphoaluminate gel (quartz and mullite, etc.) produced using fly ash. This facilitates degradation of C30, C40 and C50 geopolymer after exposure to elevated temperatures.


2016 ◽  
Vol 61 (2) ◽  
pp. 761-766 ◽  
Author(s):  
A. Zieliński ◽  
M. Sroka ◽  
A. Hernas ◽  
M. Kremzer

Abstract The HR3C is a new steel for pressure components used in the construction of boilers with supercritical working parameters. In the HR3C steel, due to adding Nb and N, the compounds such as MX, CrNbN and M23C6 precipitate during service at elevated temperature, resulting in changes in mechanical properties. This paper presents the results of microstructure investigations after ageing at 650, 700 and 750 °C for 5,000 h. The microstructure investigations were carried out using scanning and transmission electron microscopy. The qualitative and quantitative identification of the existing precipitates was carried out using X-ray analysis of phase composition. The effect elevated temperature on microstructure and mechanical properties of the examined steel was described.


CORROSION ◽  
1959 ◽  
Vol 15 (4) ◽  
pp. 29-32
Author(s):  
M. KRULFELD ◽  
M. C. BLOOM ◽  
R. E. SEEBOLD

Abstract A method of applying the hydrogen effusion method to the measurement of corrosion rates in dynamic aqueous systems at elevated temperature and pressure is described. Data obtained in low carbon steel systems are presented, including (1) reproducibility obtained in measured hydrogen effusion rates at a flow velocity of 1 foot per second at a temperature of 600 F and 2000 psi, and (2) a quantitative comparison between the hydrogen effusion rates in static and in low flow velocity dynamic systems at this temperature and pressure. Some observations are included on corrosion rate measurements in a high flow velocity (30 feet per second) loop by the hydrogen effusion method. Implications of these measurements with regard to the comparison between high flow velocity corrosion and low flow velocity corrosion are mentioned and some data indicating high local sensitivity of the hydrogen effusion method are noted. Some possible difficulties involved in the method are pointed out. 2.3.4


2014 ◽  
Vol 1004-1005 ◽  
pp. 148-153
Author(s):  
Min Hao ◽  
Ji Gang Ru ◽  
Ming Liu ◽  
Kun Zhang ◽  
Liang Wang ◽  
...  

Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) were utilized to study the microstructure and mechanical behavior of an Al-Cu-Mg alloy after tensile test at 125°C, 150°C, 175°C and 200 °C, respectively. The yield strength and ultimate tensile strength decreased with the increase of temperature, while the elongation increased firstly and then decreased. The S and S′ precipitate after tension at elevated temperatures. When the temperature was higher than 175°C, the precipitate coarsens rapidly. The alloys displayed a shear fracture features at elevated temperature. The larger S′ and S phase coarsened and dropped which forming crack in the grain boundaries and precipitate interfaces, resulting in the decrease of the elongation of the alloy.


2015 ◽  
Vol 625 ◽  
pp. 296-302 ◽  
Author(s):  
Mladen-Mateo Primorac ◽  
Manuel David Abad ◽  
Peter Hosemann ◽  
Marius Kreuzeder ◽  
Verena Maier ◽  
...  

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