Digital light processing 3D printing of multi-materials with improved adhesion using resins containing low functional acrylates

2022 ◽  
Author(s):  
Hyeonwoo Hwangbo ◽  
Seog-Jin Jeon
Keyword(s):  
3D Printing ◽  
Digital Light Processing

scholarly journals Rapid fabrication of MOF-based mixed matrix membranes through digital light processing

2021 ◽  
Author(s):  
Alexey Pustovarenko ◽  
Beatriz Seoane ◽  
Edy Abou-Hamad ◽  
Helen E King ◽  
Bert Weckhuysen ◽  
...  
Keyword(s):  
Additive Manufacturing ◽  
3D Printing ◽  
Processing Speed ◽  
Mixed Matrix Membranes ◽  
Scientific Interest ◽  
Mixed Matrix ◽  
Digital Light Processing ◽  
Additive Manufacturing Technology ◽  
Rapid Fabrication ◽  
Manufacturing Methods

3D printing, also known as additive manufacturing technology, has greatly expanded across multiple sectors of technology replacing classical manufacturing methods by combining processing speed and high precision. The scientific interest...

scholarly journals Mechanical Properties and Biocompatibility of Urethane Acrylate-Based 3D-Printed Denture Base Resin

Polymers ◽  
2021 ◽  
Vol 13 (5) ◽  
pp. 822
Author(s):  
Jy-Jiunn Tzeng ◽  
Tzu-Sen Yang ◽  
Wei-Fang Lee ◽  
Hsuan Chen ◽  
Hung-Ming Chang
Keyword(s):  
Mechanical Properties ◽  
3D Printing ◽  
Flexural Modulus ◽  
Measurement Data ◽  
Uv Exposure ◽  
Control Group ◽  
Urethane Acrylate ◽  
Shore Hardness ◽  
Digital Light Processing ◽  
Denture Base

In this study, five urethane acrylates (UAs), namely aliphatic urethane hexa-acrylate (87A), aromatic urethane hexa-acrylate (88A), aliphatic UA (588), aliphatic urethane triacrylate diluted in 15% HDD (594), and high-functional aliphatic UA (5812), were selected to formulate five UA-based photopolymer resins for digital light processing (DLP)-based 3D printing. Each UA (40 wt%) was added and blended homogenously with ethoxylated pentaerythritol tetraacrylate (40 wt%), isobornyl acrylate (12 wt%), diphenyl (2,4,6-trimethylbenzoyl) phosphine oxide (3 wt%), and a pink acrylic (5 wt%). Each UA-based resin specimen was designed using CAD software and fabricated using a DLP 3D printer to specific dimensions. Characteristics, mechanical properties, and cytotoxicity levels of these designed UA-based resins were investigated and compared with a commercial 3D printing denture base acrylic resin (BB base) control group at different UV exposure times. Shore hardness-measurement data and MTT assays were analyzed using a one-way analysis of variance with Bonferroni’s post hoc test, whereas viscosity, maximum strength, and modulus were analyzed using the Kruskal–Wallis test (α = 0.05). UA-based photopolymer resins with tunable mechanical properties were successfully prepared by replacing the UA materials and the UV exposure times. After 15 min of UV exposure, the 5812 and 594 groups exhibited higher viscosities, whereas the 88A and 87A groups exhibited lower viscosities compared with the BB base group. Maximum flexural strength, flexural modulus, and Shore hardness values also revealed significant differences among materials (p < 0.001). Based on MTT assay results, the UA-based photopolymer resins were nontoxic. In the present study, mechanical properties of the designed photopolymer resins could be adjusted by changing the UA or UV exposure time, suggesting that aliphatic urethane acrylate has good potential for use in the design of printable resins for DLP-type 3D printing in dental applications.

scholarly journals Demonstration of a Polymer-Based Single Step Waveguide by 3D Printing Digital Light Processing Technology for Isopropanol Alcohol-Concentration Sensor

2021 ◽  
Author(s):  
Kankan Swargiary ◽  
Romuald Jolivot ◽  
Waleed Soliman Mohammed
Keyword(s):  
Refractive Index ◽  
3D Printing ◽  
Limit Of Detection ◽  
Optical Power ◽  
Alcohol Concentration ◽  
Single Step ◽  
Gap Size ◽  
Digital Light Processing ◽  
Fused Deposition ◽  
The Core

AbstractA polymer based horizontal single step waveguide for the sensing of alcohol is developed and analyzed. The waveguide is fabricated by 3-dimensional (3D) printing digital light processing (DLP) technology using monocure 3D rapid ultraviolet (UV) clear resin with a refractive index of n = 1.50. The fabricated waveguide is a one-piece tower shaped ridge structure. It is designed to achieve the maximum light confinement at the core by reducing the effective refractive index around the cladding region. With the surface roughness generated from the 3D printing DLP technology, various waveguides with different gap sizes are printed. Comparison is done for the different gap waveguides to achieve the minimum feature gap size utilizing the light re-coupling principle and polymer swelling effect. This effect occurs due to the polymer-alcohol interaction that results in the diffusion of alcohol molecules inside the core of the waveguide, thus changing the waveguide from the leaky type (without alcohol) to the guided type (with alcohol). Using this principle, the analysis of alcohol concentration performing as a larger increase in the transmitted light intensity can be measured. In this work, the sensitivity of the system is also compared and analyzed for different waveguide gap sizes with different concentrations of isopropanol alcohol (IPA). A waveguide gap size of 300 µm gives the highest increase in the transmitted optical power of 65% when tested with 10 µL (500 ppm) concentration of IPA. Compared with all other gaps, it also displays faster response time (t = 5 seconds) for the optical power to change right after depositing IPA in the chamber. The measured limit of detection (LOD) achieved for 300 µm is 0.366 µL. In addition, the fabricated waveguide gap of 300 µm successfully demonstrates the sensing limit of IPA concentration below 400 ppm which is considered as an exposure limit by “National Institute for Occupational Safety and Health”. All the mechanical mount and the alignments are done by 3D printing fused deposition method (FDM).

Relationship of Electrical Properties and Partical Size of Piezoelectric Ceramics Fabricated by Digital Light Processing 3D Printing

2021 ◽  
Author(s):  
Kai Liu ◽  
Jiaming Hu ◽  
Yusheng Shi ◽  
Chenyang Zhou ◽  
Yunfei Sun ◽  
...  
Keyword(s):  
Particle Size ◽  
Electrical Properties ◽  
3D Printing ◽  
Piezoelectric Sensor ◽  
Piezoelectric Ceramics ◽  
Particle Sizes ◽  
Digital Light Processing ◽  
Relationship Of ◽  
Partical Size ◽  
Functional Ceramics

Abstract To improve electrical properties of BaTiO3 piezoelectric ceramics fabricated by 3D printing, effects of particle sizes was investigated on rheological and curing properties of ceramic slurries, electrical properties of BaTiO3 fabricated by Digital Light Processing 3D printing method. It was found that the curing ability of ceramic slurries decreased first and then increased with the increase of particle size from 136 nm to 1486 nm, while the viscosity of the slurries kept decreasing. When the particle size in a range of submicron, the grain size of sintered ceramics decreased from 13.27 μm to 6.84 μm as particle size increasing. Immediately, the relative density, piezoelectric constant, relative permittivity and remanent polarization of sintered ceramics were measured and it turns out to reach 95.32%, 161.4 pC/N, 1512 and 7.59 uC/cm2 respectively while using the BaTiO3 powder with particle sizes of 993 nm. Finally, a cellular structural BaTiO3 ceramics was fabricated by using optimized powder and process parameters and packaged as a piezoelectric sensor, showing a good function of force-electricity conversion. These results demonstrated the feasibility of fabricating high-quality functional ceramics with designed geometry by Digital Light Processing.

Manufacture of Lenses and Diffraction Gratings Using DLP As an Additive Manufacturing Technology

2018 ◽  
Author(s):  
Laura Daniela Vallejo Melgarejo ◽  
Jose García ◽  
Ronald G. Reifenberger ◽  
Brittany Newell
Keyword(s):  
Additive Manufacturing ◽  
3D Printing ◽  
Diffraction Grating ◽  
Diffraction Gratings ◽  
Optical Microscope ◽  
Manufacturing Technology ◽  
Manufacturing Processes ◽  
Digital Light Processing ◽  
Additive Manufacturing Technology ◽  
Potential Use

This document condenses the results obtained when 3D printing lenses and their potential use as diffraction gratings using Digital Light Processing (DLP), as an additive manufacturing technique. This project investigated the feasibility of using DLP additive manufacturing for producing custom designed lenses and gratings. DLP was identified as the preferred manufacturing technology for gratings fabrication. Diffraction gratings take advantage of the anisotropy, inherent in additive manufacturing processes, to produce a collated pattern of multiple fringes on a substrate with completely smooth surfaces. The gratings are transmissive and were manufactured with slit separations of 10, 25 and 50 μm. More than 50 samples were printed at various build angles and mechanically treated for maximum optical transparency. The variables of the irradiance equation were obtained from photographs taken with an optical microscope. These values were used to estimate theoretical irradiance patterns of a diffraction grating and compared against the experimental 3-D printed grating. The resulting patterns were found to be remarkably similar in amplitude and distance between peaks when compared to theoretical values.

scholarly journals Cost-Effectively 3D-Printed Rigid and Versatile Interpenetrating Polymer Networks

Materials ◽  
2021 ◽  
Vol 14 (16) ◽  
pp. 4544
Author(s):  
Osman Konuray ◽  
Arnau Sola ◽  
Jordi Bonada ◽  
Agnieszka Tercjak ◽  
Albert Fabregat-Sanjuan ◽  
...  
Keyword(s):  
3D Printing ◽  
Polymer Networks ◽  
Complex Form ◽  
Interpenetrating Polymer Networks ◽  
Dual Processing ◽  
Digital Light Processing ◽  
Superior Mechanical Properties ◽  
3D Printed ◽  
Acrylate Resin ◽  
Printed Materials

Versatile acrylate–epoxy hybrid formulations are becoming widespread in photo/thermal dual-processing scenarios, especially in 3D printing applications. Usually, parts are printed in a stereolithography or digital light processing (DLP) 3D printer, after which a thermal treatment would bestow the final material with superior mechanical properties. We report the successful formulation of such a hybrid system, consisting of a commercial 3D printing acrylate resin modified by an epoxy–anhydride mixture. In the final polymeric network, we observed segregation of an epoxy-rich phase as nano-domains, similar to what was observed in a previous work. However, in the current work, we show the effectiveness of a coupling agent added to the formulation to mitigate this segregation for when such phase separation is undesired. The hybrid materials showed significant improvement of Young’s modulus over the neat acrylate. Once the flexible, partially-cured material was printed with a minimal number of layers, it could be molded into a complex form and thermally cured. Temporary shapes were readily programmable on this final material, with easy shape recovery under mild temperatures. Inspired by repairable 3D printed materials described recently, we manufactured a large object by printing its two halves, and then joined them covalently at the thermal cure stage with an apparently seamless union.

scholarly journals 3D Printing of Thermo-Sensitive Drugs

Pharmaceutics ◽  
2021 ◽  
Vol 13 (9) ◽  
pp. 1524
Author(s):  
Sadikalmahdi Abdella ◽  
Souha H. Youssef ◽  
Franklin Afinjuomo ◽  
Yunmei Song ◽  
Paris Fouladian ◽  
...  
Keyword(s):  
3D Printing ◽  
Three Dimensional ◽  
Fused Deposition Modelling ◽  
Future Directions ◽  
Digital Light Processing ◽  
Fused Deposition ◽  
Printing Technique ◽  
3D Printed ◽  
Semi Solid ◽  
Selection Of

Three-dimensional (3D) printing is among the rapidly evolving technologies with applications in many sectors. The pharmaceutical industry is no exception, and the approval of the first 3D-printed tablet (Spiratam®) marked a revolution in the field. Several studies reported the fabrication of different dosage forms using a range of 3D printing techniques. Thermosensitive drugs compose a considerable segment of available medications in the market requiring strict temperature control during processing to ensure their efficacy and safety. Heating involved in some of the 3D printing technologies raises concerns regarding the feasibility of the techniques for printing thermolabile drugs. Studies reported that semi-solid extrusion (SSE) is the commonly used printing technique to fabricate thermosensitive drugs. Digital light processing (DLP), binder jetting (BJ), and stereolithography (SLA) can also be used for the fabrication of thermosensitive drugs as they do not involve heating elements. Nonetheless, degradation of some drugs by light source used in the techniques was reported. Interestingly, fused deposition modelling (FDM) coupled with filling techniques offered protection against thermal degradation. Concepts such as selection of low melting point polymers, adjustment of printing parameters, and coupling of more than one printing technique were exploited in printing thermosensitive drugs. This systematic review presents challenges, 3DP procedures, and future directions of 3D printing of thermo-sensitive formulations.

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