Microstructural aspects of new grade ODS alloy consolidated by rotary swaging

2021 ◽  
pp. 111477
Author(s):  
Alice Chlupová ◽  
Ivo Šulák ◽  
Lenka Kunčická ◽  
Radim Kocich ◽  
Jiří Svoboda
Keyword(s):  
Materials ◽  
2020 ◽  
Vol 13 (22) ◽  
pp. 5217
Author(s):  
Jiří Svoboda ◽  
Lenka Kunčická ◽  
Natália Luptáková ◽  
Adam Weiser ◽  
Petr Dymáček

New-generation oxide dispersion-strengthened (ODS) alloys with a high volume fraction of nano-oxides of 5% are intended to become the leading creep- and oxidation-resistant alloys for applications at 1100–1300 °C. Hot consolidation of mechanically alloyed powders by intensive plastic deformation followed by heat treatment of the alloys are the key aspects for achieving top creep properties, typically ensured by a coarse-grained microstructure strengthened with homogeneously dispersed, very stable yttrium nano-oxides. The rotary swaging method proves to be favourable for hot consolidation of the new-generation ODS alloy presented. Compared to specimens consolidated by hot rolling, consolidation by hot rotary swaging predetermines the formation of coarse grains with a very high aspect ratio during subsequent secondary recrystallization. Such a grain morphology increases the creep strength of the new-generation ODS alloy considerably.


2019 ◽  
Author(s):  
Francesco D’Elia ◽  
Philipp Hiester ◽  
Carlo Zimmermann ◽  
Igor Schestakow ◽  
Jelena Horky ◽  
...  

Metals ◽  
2020 ◽  
Vol 10 (11) ◽  
pp. 1478 ◽  
Author(s):  
Luděk Stratil ◽  
Vít Horník ◽  
Petr Dymáček ◽  
Pavla Roupcová ◽  
Jiří Svoboda

The aim of the paper is to evaluate the effect of aluminum content on the oxidation resistance of new-generation of oxide dispersion strengthened (ODS) alloy at 1200 °C. Three grades of the alloy of chemical composition Fe-15Cr-xAl-4Y2O3 with different Al contents x = 0.3 wt.%, 2.0 wt.% and 5.5 wt.% are prepared by mechanical alloying. The alloys are consolidated by high temperature rolling followed by heat treatment. To study the oxidation resistance the samples are isothermally aged in the air for 1 h, 4 h, 16 h and 64 h at 1200 °C. The oxidation kinetics, composition and formation mechanism of the oxide layers are analyzed. The weight gain of prepared steels is estimated. The kinetics of oxidation is studied on metallographic cross-sections of the exposed samples by scanning electron microscopy (SEM) and energy dispersive spectrometer (EDS) analysis. The oxides on the surfaces are identified by X‑ray diffraction (XRD) analysis. The Al content significantly enhances the oxidation resistance of the alloy. For a sufficiently high Al content in the alloy a compact oxide layer of α‑Al2O3 on the surface is formed, which significantly suppresses further oxidation process.


Author(s):  
Dhia Charni ◽  
Svetlana Ortmann-Ishkina ◽  
Marius Herrmann ◽  
Christian Schenck ◽  
Jérémy Epp

AbstractThe radial infeed rotary swaging is widely used as a diameter reduction forming process of axisymmetric workpieces, improving the mechanical properties with excellent near net shape forming. In the present study, rotary swaging experiments with different parameter setups were performed on steel tubes and bars under different material states and several resulting property modifications were investigated such as stress-strain curve, hardness, fatigue strength and surface residual stresses. The results show a significant work hardening induced by the rotary swaging process and an improvement in the static and dynamic mechanical properties was observed. Furthermore, the hardness distribution was homogenous in the cross section of the rotary swaged workpieces. Moreover, depending on the process conditions, different residual stresses distribution were generated along the surface.


Author(s):  
Alexander Klumpp ◽  
Alexander Kauffmann ◽  
Sascha Seils ◽  
Stefan Dietrich ◽  
Volker Schulze

AbstractIn this study, the influence of cold rotary swaging on microstructure and mechanical properties of the precipitation-strengthened nickel-based superalloy 718 (Alloy 718) was investigated. The initial stages of work-hardening were characterized by means of microhardness, electron backscatter diffraction (EBSD), and X-ray diffraction (XRD) analyses. Furthermore, attention was devoted to the mechanical behavior at ambient and elevated temperature (550 °C) in uniaxial tension and compression. Rotary swaging to different true strains of maximum $$\varphi = 0.91$$ φ = 0.91 caused a moderate increase of microhardness and enhanced markedly the load-bearing capacity in tension, giving rise to yield strength beyond 2000 MPa. The mechanical strength $$R_{p0.2}$$ R p 0.2 in tension subsequent to rotary swaging perfectly correlates with increasing dislocation density $$\rho $$ ρ estimated from XRD in the form of a Taylor-like relationship $$R_{p0.2} \propto \sqrt{\rho }$$ R p 0.2 ∝ ρ . In compression, transient stress–strain evolution without the occurrence of a clear elastic range and distinct yield phenomenon was observed. Restoration of the elastic range, accompanied by a pronounced increase of microhardness, was obtained by a post-swaging tempering treatment at 600 °C.


2021 ◽  
Vol 9 (6) ◽  
pp. 255-262
Author(s):  
Yue Yang ◽  
Xiang Chen ◽  
Jinfeng Nie ◽  
Kang Wei ◽  
Qingzhong Mao ◽  
...  

2011 ◽  
Vol 213 ◽  
pp. 221-225 ◽  
Author(s):  
Jeong Hwan Jang ◽  
Byeong Don Joo ◽  
Sung Min Mun ◽  
Young Hoon Moon

Studies on the forming characteristics by a rotary swaging process using the sub-scale specimens have been carried out to obtain a shell body nose of desirable quality. To analyze the changes of the nose thickness and length at the respective reduction of inside diameter, the finite element simulations were carried out. As a result, the desired target dimension is satisfied with the diameter reduction of more than 64 % for the given preform. The thickness of nose area increased up to 56.1 % from initial thickness of 2.62 mm to 4.09 mm after swaging. The values of the hardness before and after swaging were 208 HV and 325 HV, respectively. To analyze the dimensional changes (length and thickness) of nose area with decreasing inside diameter, the rotary swaging test was carried out for two different diameter reductions such as 65 % and 67 %. The lengths of nose area for the diameter reductions are 11.79 mm in 65 % and 12.53 mm in 67 %, respectively. At the diameter reduction of more than 67%, the crack occurs when the localized strain hardening reduces ductility in internal area. Therefore, the nose area should be formed from 64% to 67% reduction in target inner diameter.


2015 ◽  
Vol 651-653 ◽  
pp. 627-632 ◽  
Author(s):  
Svetlana Ishkina ◽  
Bernd Kuhfuss ◽  
Christian Schenck

Rotary swaging is a well established cold forming process e.g. in the automotive industry. In order to modify the material properties by swaging systematically, a new process of swaging with asymmetrical strokes of the forming dies is investigated. The newly developed tools feature flat surfaces and do not represent the geometry of the formed part as in conventional swaging. Numerical simulation and physical tests are carried out with special regard to the resulting geometry, mechanical properties and the microstructure. During these tests copper wires with diameter d0=1 mm are formed. Regarding the microstructure in the longitudinal section of formed specimens, elongation of grains in the central part and grain size reduction in the boundary area are observed. Furthermore, this approach opens up new possibilities to configure the geometry of wires. 2D-simulation is applied and discussed in the paper to investigate change of the processed geometry (cross-section) and shear strain distribution during the rotary swaging process.


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