scholarly journals Characterization of micro- to macroscopic response of polymers containing voids under macroscopically uniform deformation

2002 ◽  
Vol 39 (13-14) ◽  
pp. 3409-3428 ◽  
Author(s):  
Yoshihiro Tomita ◽  
Wei Lu
Keyword(s):  
Uniform Deformation ◽  
Macroscopic Response

Quantitative Analysis of Instability for Superplastic Tension

2014 ◽  
Vol 941-944 ◽  
pp. 1505-1508
Author(s):  
Zhi Ping Guan ◽  
Ming Wen Ren ◽  
Pin Kui Ma ◽  
Po Zhao
Keyword(s):  
Strain Rate ◽  
Strain Path ◽  
Superplastic Forming ◽  
Uniform Strain ◽  
Deformation Condition ◽  
Al Alloy ◽  
Uniform Deformation ◽  
Rate Dependent ◽  
Strain And Strain Rate

In conventional analysis of instability, a rough prediction of uniform deformation was obtained due to taking material parameters as constants. In this study, the constitutive equation with varying parameters for Zn-5%Al alloy at 340 °C is employed to predict the critical values of uniform strain in tension based on Considere criterion and Hart criterion, respectively. It should address the factor of strain rate in the characterization of the capability of uniform deformation on superplastic alloys, or for that matter, on any rate-dependent material. Comparison and analysis indicated that the results on Hart criterion have the better predictability of uniform deformation than Considere criterion. The Considere criterion is dependent on strain path, while Hart crtierion is merely dependent on the values of strain and strain rate in tension, and is independent on the strain path or the deformation condition or the deformation history. Therefore, the uniform strain vs. strain rate relation can be taken as a quantitative reference for designing a reasonable strain path during superplastic forming with increase of formability and reduction of forming time.

Characterization of Size-affected Non-uniform Deformation of Polycrystalline Copper

2021 ◽  
pp. 106760
Author(s):  
Makoto Uchida ◽  
Kensho Tsutsumi ◽  
Masashi Sakamoto ◽  
Yoshihisa Kaneko
Keyword(s):  
Polycrystalline Copper ◽  
Uniform Deformation

Structural characterization of unsaturated aggregated soil

2010 ◽  
Vol 47 (3) ◽  
pp. 297-311 ◽  
Author(s):  
A. Koliji ◽  
L. Vulliet ◽  
L. Laloui
Keyword(s):  
Soil Structure ◽  
Mercury Intrusion Porosimetry ◽  
Experimental Studies ◽  
Environmental Scanning Electron Microscopy ◽  
Structural Evolution ◽  
Environmental Scanning ◽  
Comprehensive Understanding ◽  
Soil Fabric ◽  
Macroscopic Response

Despite the recent experimental studies of soil structure, a comprehensive understanding of the macroscopic response of a soil in relation to its structure has not yet been achieved. This lack of understanding reveals the need for further assessments of soil structure and its evolution under loading. In this work, the structure of an aggregated soil under various conditions of saturation and mechanical loading is studied. We also compare the aggregated soil structure, which shows a double porous fabric, with that of the same soil when reconstituted. The experimental methods selected for this study are a combination of mercury intrusion porosimetry (MIP), environmental scanning electron microscopy (ESEM), and neutron computed tomography (CT). Using MIP and ESEM, we first examine the soil fabric at the intra-aggregate scale. Then, we quantify the structural evolution of the soil using neutron tomography and link it to the macroscopic response of the soil. Based on the experimental evidence, the main features of the soil structure and its evolution are outlined for unsaturated aggregated soil under different loading conditions.

Superplastic Forming

2019 ◽  
Author(s):  
Norman Ridley
Keyword(s):  
Mechanical Properties ◽  
Tensile Testing ◽  
Process Development ◽  
Superplastic Forming ◽  
Stretch Forming ◽  
Uniform Deformation ◽  
Forming Simulation ◽  
Structural Applications ◽  
Identification And Characterization

An inherent limitation of conventional aluminum alloys is that they are unstable when plastically deformed by stretching which leads to catastrophic necking when tensile testing and limitations on uniform deformation during stretch forming under tensile stress. This has led to the development of superplastic forming (SPF) process development used for the production of products for structural and non-structural applications in industries such as aerospace, automotive, architecture, transport and others. This article provides a general overview of superplastic forming and addresses: identification and characterization of superplastic alloys, processing of superplastic alloys, cavitation and failure, superplastic forming, simulation, and applications and mechanical properties.

Morphological Characterization of Mycobacteriophage R1

1974 ◽  
Vol 32 ◽  
pp. 254-255
Author(s):  
B. L. Soloff ◽  
T. A. Rado
Keyword(s):  
Carbon Source ◽  
Stationary Phase ◽  
Growth Phase ◽  
Minimal Medium ◽  
Morphological Characterization ◽  
Logarithmic Growth Phase ◽  
Complete Lysis ◽  
Lysogenic Culture ◽  
Logarithmic Growth

Mycobacteriophage R1 was originally isolated from a lysogenic culture of M. butyricum. The virus was propagated on a leucine-requiring derivative of M. smegmatis, 607 leu−, isolated by nitrosoguanidine mutagenesis of typestrain ATCC 607. Growth was accomplished in a minimal medium containing glycerol and glucose as carbon source and enriched by the addition of 80 μg/ ml L-leucine. Bacteria in early logarithmic growth phase were infected with virus at a multiplicity of 5, and incubated with aeration for 8 hours. The partially lysed suspension was diluted 1:10 in growth medium and incubated for a further 8 hours. This permitted stationary phase cells to re-enter logarithmic growth and resulted in complete lysis of the culture.

AEM analysis of crystallization in Ti-based amorphous alloys

1983 ◽  
Vol 41 ◽  
pp. 270-271
Author(s):  
A.R. Pelton ◽  
A.F. Marshall ◽  
Y.S. Lee
Keyword(s):  
Magnetic Properties ◽  
Amorphous Alloys ◽  
Amorphous Materials ◽  
Isothermal Annealing ◽  
Amorphous Matrix ◽  
Nucleation And Growth ◽  
Current Interest ◽  
Amorphous Films ◽  
Electrical And Magnetic Properties

Amorphous materials are of current interest due to their desirable mechanical, electrical and magnetic properties. Furthermore, crystallizing amorphous alloys provides an avenue for discerning sequential and competitive phases thus allowing access to otherwise inaccessible crystalline structures. Previous studies have shown the benefits of using AEM to determine crystal structures and compositions of partially crystallized alloys. The present paper will discuss the AEM characterization of crystallized Cu-Ti and Ni-Ti amorphous films.Cu60Ti40: The amorphous alloy Cu60Ti40, when continuously heated, forms a simple intermediate, macrocrystalline phase which then transforms to the ordered, equilibrium Cu3Ti2 phase. However, contrary to what one would expect from kinetic considerations, isothermal annealing below the isochronal crystallization temperature results in direct nucleation and growth of Cu3Ti2 from the amorphous matrix.

Characterization of Coherent, Ordered Precipitates in Nickel-Base Alloys

1973 ◽  
Vol 31 ◽  
pp. 144-145
Author(s):  
B. H. Kear ◽  
J. M. Oblak
Keyword(s):  
Stable Phase ◽  
Nickel Base Superalloy ◽  
Alloy 718 ◽  
Commercial Alloy ◽  
Precipitate Morphology ◽  
Continuous Precipitation ◽  
Nickel Base ◽  
Base Superalloy ◽  
Strengthening Precipitate

A nickel-base superalloy is essentially a Ni/Cr solid solution hardened by additions of Al (Ti, Nb, etc.) to precipitate a coherent, ordered phase. In most commercial alloy systems, e.g. B-1900, IN-100 and Mar-M200, the stable precipitate is Ni3 (Al,Ti) γ′, with an LI2structure. In A lloy 901 the normal precipitate is metastable Nis Ti3 γ′ ; the stable phase is a hexagonal Do2 4 structure. In Alloy 718 the strengthening precipitate is metastable γ″, which has a body-centered tetragonal D022 structure.Precipitate MorphologyIn most systems the ordered γ′ phase forms by a continuous precipitation re-action, which gives rise to a uniform intragranular dispersion of precipitate particles. For zero γ/γ′ misfit, the γ′ precipitates assume a spheroidal.

The Use of Advanced Analytical Techniques for Characterization of the Chemical, Physical, and Crystallographic Nature of a Surface

1973 ◽  
Vol 31 ◽  
pp. 132-133 ◽  
Author(s):  
R. E. Herfert
Keyword(s):  
Surface Characterization ◽  
Analytical Techniques ◽  
X Ray Diffraction ◽  
Depth Of Penetration ◽  
X Ray ◽  
The Past ◽  
Transmission Electron ◽  
Scanning Electron

Studies of the nature of a surface, either metallic or nonmetallic, in the past, have been limited to the instrumentation available for these measurements. In the past, optical microscopy, replica transmission electron microscopy, electron or X-ray diffraction and optical or X-ray spectroscopy have provided the means of surface characterization. Actually, some of these techniques are not purely surface; the depth of penetration may be a few thousands of an inch. Within the last five years, instrumentation has been made available which now makes it practical for use to study the outer few 100A of layers and characterize it completely from a chemical, physical, and crystallographic standpoint. The scanning electron microscope (SEM) provides a means of viewing the surface of a material in situ to magnifications as high as 250,000X.

Skeletal elements of crinoid echinoderms: High-resolution structural and microanalytical results

1983 ◽  
Vol 41 ◽  
pp. 194-195
Author(s):  
D. F. Blake ◽  
L. F. Allard ◽  
D. R. Peacor
Keyword(s):  
High Resolution ◽  
Marine Invertebrates ◽  
Sea Urchins ◽  
Structural Features ◽  
Sea Stars ◽  
High Resolution Tem ◽  
Relationship Of ◽  
The Relationship ◽  
Insight Into

Echinodermata is a phylum of marine invertebrates which has been extant since Cambrian time (c.a. 500 m.y. before the present). Modern examples of echinoderms include sea urchins, sea stars, and sea lilies (crinoids). The endoskeletons of echinoderms are composed of plates or ossicles (Fig. 1) which are with few exceptions, porous, single crystals of high-magnesian calcite. Despite their single crystal nature, fracture surfaces do not exhibit the near-perfect {10.4} cleavage characteristic of inorganic calcite. This paradoxical mix of biogenic and inorganic features has prompted much recent work on echinoderm skeletal crystallography. Furthermore, fossil echinoderm hard parts comprise a volumetrically significant portion of some marine limestones sequences. The ultrastructural and microchemical characterization of modern skeletal material should lend insight into: 1). The nature of the biogenic processes involved, for example, the relationship of Mg heterogeneity to morphological and structural features in modern echinoderm material, and 2). The nature of the diagenetic changes undergone by their ancient, fossilized counterparts. In this study, high resolution TEM (HRTEM), high voltage TEM (HVTEM), and STEM microanalysis are used to characterize tha ultrastructural and microchemical composition of skeletal elements of the modern crinoid Neocrinus blakei.

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