Microstructure and Mechanical Properties of Biomedical Ti-27Nb-8Zr Alloy with Low Elastic Modulus

2010 ◽  
Vol 39 (10) ◽  
pp. 1707-1710 ◽  
Author(s):  
Jie Zhao ◽  
Hongtao Duan ◽  
Haitao Li
Metals ◽  
2019 ◽  
Vol 9 (11) ◽  
pp. 1135 ◽  
Author(s):  
Li ◽  
Ma ◽  
Jia ◽  
Meng ◽  
Tang ◽  
...  

The microstructure and mechanical properties of rapidly solidified β-type Ti–Fe–Sn–Mo alloys with high specific strength and low elastic modulus were investigated. The results show that the phases of Ti–Fe–Sn–Mo alloys are composed of the β-Ti, α-Ti, and TiFe phases; the volume fraction of TiFe phase decreases with the increase of Mo content. The high Fe content results in the deposition of TiFe phase along the grain boundary of the Ti phase. The Ti75Fe19Sn5Mo1 alloy exhibits the high yield strength, maximum compressive strength, large plastic deformation, high specific strength, high Vickers hardness, and large toughness value, which is a superior new engineering material. The elastic modulus (42.1 GPa) of Ti75Fe15Sn5Mo5 alloy is very close to the elastic modulus of human bone (10–30 GPa), which indicating that the alloy can be used as a good biomedical alloy. In addition, the large H/Er and H3/Er2 values of Ti75Fe19Sn5Mo1 alloy indicate the good wear resistance and long service life as biomedical materials.


Metals ◽  
2019 ◽  
Vol 9 (6) ◽  
pp. 712 ◽  
Author(s):  
Peiyou Li ◽  
Xindi Ma ◽  
Duo Wang ◽  
Hui Zhang

The microstructural and mechanical properties of β-type Ti85-xNb10+xSn5 (x = 0, 3, 6, 10 at.%) alloys with low elastic modulus were investigated. The experimental results show that the Ti85Nb10Sn5 and Ti75Nb20Sn5 alloys are composed of simple α and β phases, respectively; the Ti82Nb13Sn5 and Ti79Nb16Sn5 alloys are composed of β and α″ phases. The content of martensite phase decreases with the increase of Nb content. The Ti82Nb13Sn5 and Ti79Nb16Sn5 alloys show an inverse martensitic phase transition during heating. The Ti85Nb10Sn5 and Ti82Nb13Sn5 alloys with the small residual strain exhibit the good superelastic properties in 10-time cyclic loading. The reduced elastic modulus (Er) of the Ti75Nb20Sn5 alloy (61 GPa) measured by using the nanoindentation technique is 2–6 times of that of human bone (10–30 GPa), and is smaller than that of commercial Ti-6Al-4V biomedical alloy (120 GPa). The Ti75Nb20Sn5 alloy can be considered as a novel biomedical alloy. The wear resistance (H/Er) and anti-wear capability (H3/Er2) values of the four alloys are higher than those of the CP–Ti alloy (0.0238), which indicates that the present alloys have good wear resistance and anti-wear capability.


2014 ◽  
Vol 18 (sup4) ◽  
pp. S4-212-S4-214
Author(s):  
Y. L. Qi ◽  
L. Y. Zeng ◽  
Z. M. Hou ◽  
Q. Hong ◽  
S. B. Liu ◽  
...  

2007 ◽  
Vol 124-126 ◽  
pp. 1669-1672 ◽  
Author(s):  
Hi Won Jeong ◽  
Seung Eon Kim ◽  
Chang Yong Jo ◽  
Yong Tae Lee ◽  
Joong Kuen Park

The titanium alloys containing the Nb transition elements have been investigated as the Ni-free shape memory and the biomedical alloys with a low elastic modulus. The mechanical properties of the alloys depended upon the meta-stable phases like the α`, α``, ω. To study the martensitic transformations from the β to α`` or α` the Ti-xNb (x=0 to 40 wt%) alloys were melted into the button type ingots using a VAR, and followed by the water-quenching after the soaking at 1000oC for 2hrs. The crystallography of the martensitic phases in the water-quenched alloys was analyzed using a XRD. The diffraction peaks of the orthorhombic martensites were identified by the crystallographic relationship with the bcc matrix. The lattice parameters of the orthorhombic martensites were varied continuously with the contents of the Nb elements. The martensitic transformations of the alloys were studied using the phenomenological theory of Bowles and Mackenzie.


2011 ◽  
Vol 683 ◽  
pp. 103-112 ◽  
Author(s):  
B. Yang

The evolution of the microstructure and mechanical properties of electrodeposited nanocrystalline Ni with different annealing procedures was studied systematically. For the annealed specimens hardness decreases with increasing average grain size but the dependence changes at different grain size ranges. The specimens annealed at a low temperature show higher hardness compared to the as-deposited nanocrystalline Ni, despite an increased measured average grain size. In association with this hardening an increase in elastic modulus and a decrease in microstrain was observed after annealing. With increasing annealing temperature both the tensile strength and the fracture strain were observed to decrease, this is companied with a transition from ductile to brittle in the fracture surfaces. These results indicated that the mechanical behaviour of nanocrystalline Ni depends not only on the average grain size but also on the grain boundary structure. A change in the grain boundary state arising from annealing may be responsible for the observed increase in hardness and elastic modulus as well as the deterioration of tensile properties.


2010 ◽  
Vol 660-661 ◽  
pp. 176-181
Author(s):  
José Hélio Duvaizem ◽  
Gabriel Souza Galdino ◽  
Ana Helena A. Bressiani ◽  
Rubens Nunes de Faria Jr. ◽  
Hidetoshi Takiishi

The effects of the hydrogenation stage on microstructure and mechanical properties of Ti-13Nb-13Zr alloy produced by powder metallurgy have been studied. Powder alloys have been produced by hydrogenation with 250 MPa or 1 GPa and via high energy planetary ball milling. Samples were isostatically pressed at 200 MPa and sintered at 1150 °C for 7, 10 and 13 hours. Elastic modulus and microhardness were determined using a dynamic mechanical analyzer (DMA) and a Vickers microhardness tester. Density of the samples was measured using a liquid displacement system. Microstructure and phases presents were analyzed employing scanning electron microscopy (SEM). Elastic modulus was 81.3  0.8 and 62.6  0.6 GPa for samples produced by 250 MPa and 1 GPa hydrogenation, respectively when sintered for 7h.


2010 ◽  
Vol 154-155 ◽  
pp. 1659-1663
Author(s):  
Zheng Bing Qi ◽  
Peng Sun ◽  
Fang Ping Zhu ◽  
Ruo Xuan Huang ◽  
Zhou Cheng Wang ◽  
...  

The influence of working pressure on microstructure and mechanical properties of magnetron sputtered ZrN coatings were systemically investigated. The results reveal that a decreased working pressure results in preferred orientation evolution from (111) to (200) and cross-sectional morphologies transition from columnar structure to equiaxed grains. These microstructural changes are considered responsible for an increase in hardness and modulus with decreasing working pressure. Chip spallation and plastic deformation failure modes are observed during scratch testing, and the increased critical loads are attributed to higher hardness and elastic modulus, as well as moderate compressive stress at lower working pressure.


Materials ◽  
2021 ◽  
Vol 15 (1) ◽  
pp. 137
Author(s):  
Elena N. Sheftel ◽  
Valentin A. Tedzhetov ◽  
Eugene V. Harin ◽  
Philipp V. Kiryukhantsev-Korneev ◽  
Galina S. Usmanova ◽  
...  

The paper presents results of investigation of Fe65.3–100Zr34.7–0N7.5–0 films prepared by dc magnetron deposition on glass substrates and subsequent 1-hour annealing at temperatures of 300–600 °C. The influence of the chemical and phase compositions and structure of the films, which were studied by TEM, SEM, XRD, and GDOES, on their mechanical properties determined by nanoindentation and static magnetic properties measured by VSM method is analyzed. The studied films exhibit the hardness within a range of 14–21 GPa, low elastic modulus (the value can reach 156 Gpa), and an elastic recovery of 55–83%. It was shown that the films are strong ferromagnets with the high saturation induction Bs (up to 2.1 T) and low coercive field Hc (as low as 40 A/m). The correlations between the magnetic and mechanical properties, on one hand, and the chemical composition of the films, their phase, and structural states as well, on the other hand, are discussed.


2021 ◽  
Author(s):  
Jürgen Peter Gross ◽  
Jürgen Malzbender ◽  
Enkhtsetseg Dashjav ◽  
Frank Tietz ◽  
Ruth Schwaiger

Abstract LATP sheets with LiF and SiO2 addition prepared by tape casting as electrolytes for solid-state batteries were characterized regarding conductivity, microstructure and mechanical properties aiming towards an optimized composition. The use of additives permitted a lowering of the sintering temperature. As general trend, higher LiF to SiO2 ratios led to lower porosities. This decrease in the porosity corresponds to an increase of the ionic conductivity as well as higher values of elastic modulus and hardness determined by indentation testing. Micro-pillar testing was used to assess the crack growth behavior, revealing weak grain boundaries.


2011 ◽  
Vol 409 ◽  
pp. 170-174
Author(s):  
A. Ramarolahy ◽  
Philippe Castany ◽  
Thierry Gloriant ◽  
Frédéric Prima ◽  
P. Laheurte ◽  
...  

Ti-Nb based alloys are well known to their good mechanical properties, shape memory effect, superelasticity, as well as good biocompatibility. The Ti-24Nb (at%) binary alloy presents a shape memory behavior and low elastic modulus. Our study is focused on the improvement of their mechanical properties by adding a third alloying element (oxygen, nitrogen or silicon). Addition of 0.5 at% of N or O modifies drastically the mechanical behavior of Ti-24Nb alloy that exhibits superelastic behavior instead of shape memory one. On the other hand, addition of 0.5 at% of Si increased yield strength of the Ti-24Nb shape memory alloy.


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